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在酸氧化后的多壁碳纳米管上化学还原镀钯,用水将镀钯后的碳管清洗至中性并配制成悬浊液,将悬浊液旋涂在真空溅射的叉指金电极表面,干燥后作为气敏膜,把气敏膜暴露于一定浓度的苯气体中,检测传感器的电流变化,并计算其灵敏度。镀钯后的多壁碳管在室温下对苯响应和回复迅速,电导变化与苯气体的浓度呈良好的线性关系,其线性回归方程y=0.0041x 0.1288,r=0.9546。Pd颗粒对苯分子和碳管壁结构缺陷间的电子转移的促进作用可能是多壁碳管镀钯后产生良好气敏响应的原因。 相似文献
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The Δ-scaling method has been applied to ultra-relativistic p p,C C and Pb Pb collision data simulated using a high-energy Monte Carlo package,LUCIAE 3.0.The Δ-scaling is found to be valid for some physical variables,such as charged particle multiplicity,strange particle multiplicity and number of binary nucleon-nucleon-nucleon collisions from these simulated nucleus-nucleus collisions over an extended energy ranging from E1ab=20 to 200A GeV.In addition we derive the information entropy from the multiplicity distribution as a function of beam energy for these collisions. 相似文献
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The Langevin equation is used to simulate the fission process of ^112Sn ^112Sn and ^116Sn ^116Sn. The mass distribution of the fission fragments are given by assuming the process of symmetric fission or asymmetric fission with the Gaussian probability sampling. The isoscaling behaviour has been observed from the analysis of fission fragments of both the reactions, and the isoscaling parameter α seems to be sensitive to the width of fission probability and the beam energy. 相似文献
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The isoscaling behaviour is investigated in a frame of isospin-dependent quantum molecular dynamics models. The isotopic yields ratio Y2/Y1 for reactions ^48Ca ^48Ca and ^40 Ca ^4oCa at different entrance channels are simulated and presented, the relationship between the isoscaling parameter and the entrance channel is analysed, the results show that a and β reduce with the rise of incident energies and increase with the impact parameter b, which can be attributed to the temperature varying of the pre-fragments in different entrance channels. The relation of a and symmetry-term coefficient Csym reveals that the chemical potential difference △μ is sensitive to thesymmetry-term coefficient Csym, and raises with the increasing Csym. 相似文献
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对QuEChERS前处理方法从提取、分离、净化等方面进行优化以减弱样本中的基质效应,提高灵敏度;使用提取试剂(含0.1%甲酸的乙腈:甲醇=70:30,V/V)进行提取,加入无水硫酸镁、硼酸钠、研磨珠进行提取分离,使用混合净化剂(十八烷基硅烷(C18):乙二胺-N-丙基硅烷(PSA)=1:2,m/m)进行净化,UPLC-MS/MS测定,外标法定量。结果表明:在优化条件下,苯丙胺类及其相关9种物质的色谱峰分离良好,且各标准化合物的线性相关系数均大于0.991,检出限(LODs)为0.3~1.0 ng/mL,定量限(LOQs)均为2.5 ng/mL;血液添加标准品样本在低(20 ng/mL)、中(100 ng/mL)、高(400 ng/mL)3个浓度的加标回收率为80.1%~103.1%,精密度相对标准偏差(RSD)为1.5%~8.6%;临床4份检测样本中有3份检出苯丙胺类阳性,准确率为71.5%~99.1%。所建立的QuEChERS方法与UPLC-MS/MS结合的分析方法可应用于血液样本中苯丙胺类及其相关9种药物的同时检测分析。 相似文献
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根据Ho3+在Ho :YVO4 晶体的吸收谱和 0 6~ 2 1μm波段的荧光谱 ,用J O理论计算了Ho3+的强度参数Ωλ ,并由此计算了激发能级的振子强度、自发辐射跃迁几率、荧光分支比和积分发射截面等光谱参数 ,讨论了Ho :YVO4 晶体作为红外激光材料的可能性。 相似文献
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BLUE-GREEN UP-CONVERSION LUMINESCENCE OF NONCHYSTALLINE HoP5O14 INDUCED BY PULSE DCM DYE LASER 总被引:1,自引:0,他引:1 下载免费PDF全文
This paper reports the up-conversion luminescence phenomenon in blue-green wave-range of noncrystalline HoP5O14 induced by pulse DCM dye laser and gives some simple analyses. 相似文献
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正交多项式最小二乘曲线拟合法求光源色温的经验公式 总被引:4,自引:0,他引:4
本文报道用正交多项式最小二乘曲线拟合法,首次获得精确计算光源色温的经验公式Tc,色温Tc≤2000K,2000~20000K和10000~100000K范围的标准偏差分别为1.852×10-2,1.439×10-3和3.536×10-3。应用拟合公式计算了黑体辐射、标准光源以及重组日光的色温值,结果令人满意。 相似文献