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The title compound 3,9-bis(pyridin-2-yl)-2,4,8,10-tetraoxaspiro[5.5]undecane 4(C17H18N2O4) has been synthesized by the reaction of 2,2-bis(hydroxymethyl)propane-1,3-diol with pyridine-2-carbaldehyde in the presence of p-toluenesulfonic acid,and characterized by IR,1H-NMR and X-ray single-crystal diffraction.The crystal belongs to monoclinic system,space group C2/c with a = 25.133(2),b = 5.7219(5),c = 21.942(2) ,β = 99.145(2)°,V = 3115.3(5)3,Z = 8,Dc = 1.340 g/cm3,Mr = 314.33,F(000) = 1328,μ = 0.097 mm-1,MoKa radiation(λ = 0.71073),R = 0.0352 and wR = 0.1022 for 2486 observed reflections with I > 2σ(I).X-ray analysis reveals that the two 1,3-dioxane rings passing through the central spiro-C atom both adopt chair conformation.Intermolecular C-H…π,C-H…O and C-H…N weak interactions link the molecules to form a three-dimensional samdwich,which are effective in the stabilization of the crystal structure. 相似文献
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超导接收前端以超导滤波器和高电子迁移率晶体管(HEMT)低温放大器构成核心微波电路,其HEMT放大器在低温下拥有极低的工作噪声,但对偏置供电的要求很高,只有在特定偏置下,系统才拥有最佳的工作稳定度、高增益和低噪声。本文针对多信道超导接收前端,设计了一种多通道、模块化,带程控通讯的超导接收前端用HEMT低噪放电控组件,为设备核心射频通道提供供电、切换和远程控制。其供电偏置可调、供电纹波≤3 mV,并提供多路TTL电平接口,支持RS485数据通讯控制,便于模块化安装,在超导接收前端分机中工作状况良好。 相似文献
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