SPDT加工对KDP晶体表面温度及应力的影响

KDP晶体作为优质的非线性光学材料,具有脆性高、对温度敏感等特性,在单点金刚石切削(SPDT)超精密加工中,微小的温度和应力变化有可能对晶体造成损伤,但是一直未有相关实验报道.本文采用红外热成像仪对SPDT加工过程进行监测,结合Raman光谱技术,研究KDP晶体在SPDT加工前后表面温度和应力的分布变化.大尺寸KDP晶体经过快速微区切削后,在给定的切削工艺条件下,测量出切削部分最高瞬态温度比附近未切削部分高出将近8℃.通过Raman测量,显示切削后晶体表面存在残余拉应力.结合热力耦合模拟仿真,进一步分析了SPDT加工过程动态切削温度对晶体质量的影响,为优化加工参数提供依据.     

新型铜粉导电复合物的合成

以Bi_2O_3与Sn(OH)_4为原料、NaBH_4为还原剂,成功在3.5μm球形铜粉表面包覆了Sn-Bi合金层,将铜粉与高分子基体(聚乙烯吡咯烷酮、丙烯酸树脂、环氧树脂)复合制备了导电复合物。采用场发射扫描电镜(SEM)、能谱仪(EDS)与差示扫描量热仪(DSC)表征包覆铜粉的组成与结构,采用刮板细度计测试复合物的分散与稳定性能,并用万用电表测试其导电性能。结果表明,包覆铜粉复合物的导电性能较纯铜粉复合物明显提高。     

某乘用车加速工况车内轰鸣声诊断分析及控制方法

该文针对某乘用车加速工况出现的轰鸣声进行诊断分析与控制。首先通过主观评价确定问题工况,通过实车测试发现2400 r/min左右车内存在明显轰鸣声。利用阶次分析、模态分析及错频验证可知,发动机激励经悬置传递副车架,引起副车架的共振,进而传递到车内引起轰鸣声。最后通过传递分析及柔性连接点导纳法,优化副车架橡胶衬套结构。结果表明,优化后在2400 r/min声压总级与2阶声压差值为7.5 dB(A);声压总级较原状态降低2 d B(A),2阶噪声降低7.8 d B(A),声压总级和2阶噪声声压差值增大,轰鸣声明显减小,主观评价可接受。     

五种常见重金属的电化学检测研究进展

电化学检测是重金属快速检测的热门研究方向,在重金属离子的检测领域具有良好的应用前景。阐述了电化学分析法及其传感器在重金属检测中的优势,重点介绍了Cd,Cr,Hg,Pb,As 5种金属的电化学研究进展,根据电极修饰的研究方向进行归纳总结,并对电化学检测技术在重金属检测中存在的问题和应用进行了总结与展望。     

Iterative blind deconvolution of adaptive optics images

Adaptive optics (AO) technique has been extensively used for large ground-based optical telescopes to overcome the effect of atmospheric turbulence. But the correction is often partial. An iterative blind deconvolution (IBD) algorithm based on maximum-likelihood (ML) method is proposed to restore the details of the object image corrected by AO. IBD algorithm and the procedure are briefly introduced and the experiment results are presented. The results show that IBD algorithm is efficient for the restoration of some useful high-frequency of the image.     

Rapid detection of chlorpheniramine maleate by an electrochemical sensor based on metal-organic frameworks CHP@Cu3（BTC）2 /MWCNTsEI北大核心CSCD

Copper hydroxyphosphate@metal-organic frameworks/multi-wall carbon nanotube composites （CHP@Cu3 （BTC）2 /MWCNTs）were prepared by a new in-situ template method and then an electrochemical sensor was developed based on the composites. The crystal structure and morphology of the material were characterized by X-ray diffraction and scanning electron microscope. Cyclic voltammetry and linear sweep voltammetry were used to study the electrochemical catalytic performance，and the determination conditions were optimized. The rapid and sensitive detection of chlorphenamine maleate was realized. There was a good linear relationship between the oxidation peak current and concentration of chlorphenamine maleate in the ranges from 5 to 100 µμmol/L and from 150 to 800 µμmol/L，and the linear equations were as Ipa （µμA）=0.1559c（µμmol/L）-0.3533 （R2 =0.9973）and Ipa （µμA）=0.02328c（µμmol/L）+16.63（R2 =0.9594），and the detection limit was 1.67 µμmol/L. The recoveries of the actual drug ranged from 91.0% to 109.1%. © 2023, Youke Publishing Co.,Ltd. All rights reserved.