恒能量同步荧光光谱法测定食用油中多环芳烃

用12%（w/V）的氢氧化钾-乙醇溶液皂化食用油的脂肪酸,以环己烷萃取皂化液中的多环芳烃,经浓缩,柱层析纯化并浓缩,取微量试样液稀释后,通过选择合适能量差,建立了同步荧光法测定食用油中多环芳烃含量的新方法,其线性范围为5—1000ng.mL-1,检出限在0.04—15.21ng.mL-1之间,平均加标回收率在81.94%—90.06%之间。该方法具有快速、简便、准确等特点。     

Design and performance of a composite Tm:YAG laser pumped by VBG-stabilized narrow-band laser diode

A 2-μm composite Tm:YAG laser pumped with a narrow-band laser diode was presented. The temperature distribution and thermal lens in the Tm:YAG were numerically simulated by a finite element method and the results were used to design the special cavity, in order to achieve a high efficiency and stable output. With a 25-W incident pump power, we obtained a maximum output power of 11 W at 2018.5 nm, corresponding to a slope efficiency of 51.3% and an optical-to-optical efficiency of 44.5%, respectively. The beam quality was measured to be M_x~2= 1.8 and M_y~2= 1.6.     

分子印迹电化学传感器检测水杨酸

以水杨酸(SA)为模板分子,邻苯二胺(o-PPD)及吡咯(Py)为复合功能单体,在石墨烯修饰的玻碳电极表面制备分子印迹电化学传感器(MIP/GO/GCE),用扫描电镜(SEM)观察印迹膜的表面形貌,方波伏安法(SWV)和循环伏安法(CV)对分子印迹传感器的性能进行表征。通过优化实验条件,显示SA浓度在1.0×10-8~1.0×10-2 mol/L范围内,分子印迹传感器峰电流与SA浓度负对数具有良好的线性关系,检出限为8.6×10-9 mol/L。该传感器对SA具有良好的选择性,样品回收率为101%~106%,相对标准偏差(RSD)为3.8%。SA分子印迹传感器的制备简单、抗干扰性好、灵敏度高、成本低廉,具有较好实用价值。     

Energy reduction:a technique for seed-injection locking of single-axial-mode Q-switched Nd:YAG laser

A new technique for seed-injection locking of single-axial-mode (SAM) Q-switched Nd:YAG laser is re- ported.The technique called energy reduction (ER) is utilized when SAM operation is locked to design its feedback scheme.This method ensures long-term 100% seed-injection locking performance and the pulsed SAM output energy can reach as high as 200 mJ.Both temporal and spatial interferometric experiments have been executed to confirm the SAM oscillation.     

High peak power first,second, and third order Stokes pulses based on intracavity self-stimulated Raman scattering lasers

<正>We obtain high peak power pulses in megawatt range of the first(1181 nm),second(1321 nm),and third order(1500 nm) Stokes radiation from self-conversion of the 1067-nm laser radiation based on Nd:KGW laser.The maximum output energy of the first order Stokes laser is 35.3 mJ,which is to our knowledge, the highest reported energy in an intracavity Q-switched laser.The third order Stokes pulse is obtained in an intracavity Q-switched laser.     

高功率全正色散锁模掺Yb3+双包层光纤飞秒激光器

以芯径为30 μm的掺Yb³⁺双包层光纤为增益介质, 利用非线性偏振旋转技术以及光栅-小孔结构组成的光谱滤波器提供有效的振幅调制, 实现了稳定的全正色散耗散孤子锁模运转. 激光器直接输出重复频率为76.6 MHz、平均功率达6.3 W的超短脉冲, 单脉冲能量可达82 nJ. 直接输出脉冲宽度为1.33 ps, 经腔外压缩后的宽度为377 fs. 通过调节光栅角度还实现了输出脉冲中心波长在1025—1078 nm范围内的调谐.