PdMn/Co多层膜的磁性和磁光特性研究

用磁控溅射法制备了不同Mn含量的PdMn/Co磁性多层膜，通过x射线衍射对该多层膜系列进行结构分析；测定了不同Mn含量系列样品的磁滞回线、垂直各向异性及磁力显微镜图，分析了饱和磁化强度、磁畴和垂直各向异性变化的原因；通过测定该多层膜体系的克尔谱，简要分析了一定波长下克尔角随Mn含量增加而变化的物理机制. 关键词： 多层膜 磁性 磁光     

An investigation of phase separation by magnetic force microscopy in La0.45Sr0.55MnO3-δ(δ≈0.01)

We have found phase separation in La_0.45Sr_0.55MnO_3-δ (LSMO) by means of electron spin resonance, magnetic force microscopy (MFM) and magnetic measurements. Ferromagnetic and antiferromagnetic phases can coexist at low temperatures, and ferromagnetic and paramagnetic phases coexist when the temperature lies between the Néel and Curie temperatures. The size and shape of the ferromagnetic phases (the minority phases) was first observed directly from MFM images. It is suggested that the phase separation in LSMO is not the charge segregation type, but an electroneutral type due perhaps to the nonuniform distribution of oxygen vacancies.     

HDDR过程中三元和多元Nd-Fe-B合金磁畴结构的MFM研究

用磁力显微镜研究了三元Nd-Fe-B合金在HDDR过程的不同阶段(铸态、不充分吸氢歧化、充分吸氢歧化和脱氢再复合)的破畴结构。在铸态样品表面清楚地观察到了易磁化轴互相垂直的柱状晶表面的两类磁畴图型。当样品不充分吸氢歧化和充分吸氢歧化时，破畴结构明显发生变化，反映了Nd-Fe-B的分解产物NdH2，α-Fe和Fe2B及其微晶结构的变化。脱氢再复合后形成的微晶的磁畴结构则表明样品保留了铸态样品柱状晶的构型。此外，还对比研究了多元Nd-Fe-B合金在HDDR过程中的磁畴结构，并根据微磁结构分析，指出过量的Ga元素添加可抑制Nd2(Fe，M)14B相的吸氢歧化，从而导致相应HDDR粘结磁体性能降低。     

Magnetic Agglomeration Among Nd-Fe-B Particles and Its Influence on Field Aligning

There exists strong magnetic agglomeration among Nd-Fe--B particles. Due to this effect, an applied field even up to 1350kAm^-1 still can not make the loose Nd-Fe-B powders to reach saturated magnetization. SEM images of a little amount of Nd-Fe-B powders were used to i11ustrate the agglomeration phenomenon. We believe that the generai existence of misaiignment gains in the magnetic force images of the sintered Nd-Fe-B magnet fabricated by die pressing with 1500kAm^-1 aiignlng field is a confirmation of the magnetic agglomeration.     

Domain structures of Nd13Fe80B7 magnets during HDDR process

The domain structures of Nd13Fe80B7 alloy at different stages of the HDDR process have been revealed using a magnetic force microscope. In the as-cast samples, the columnar crystals with easy axis perpendicular to one another are clearly characterized by their different domain structures. For the insufficient and sufficient HD treatment, an obvious change of domain structure occurs, which is related to the variation of composition and crystalline microstructure during the HD process. And for the samples after sufficient DR processing, it is confirmed that the configuration of the columnar crystals is retained by the detected domain structures.     

Investigation of the magnetic domain structure of （PtCoPt）／Si multilayers by magnetic force microscopy

The domain structure of (PtCoPt)/Si multilayers in the dc demagnetized state has been investigated by magnetic force microscopy.The domain structure is found to change dramatically as the thickness of the non-magnetic Si sublayer (tsi) increases.Together with the analysis of magnetic properties,the variation of the domain period indicates that the domain wall energy decreases.Using the model developed by Draaisma and de Jonge,the domain wall energy is obtained.     

液相烧结对Nd-Fe-B粉末压坯及磁体取向度的影响

XBD，SEM及MFM观察表明，Nd-Fe-B粉末压坯在液相烧结过程中同时存在两种影响主相晶粒取向度的机制：烧结过程中大颗粒吞并吸附在其表面的取向不良的小晶粒并择优长大，使磁体的取向度提高；在液相烧结过程中，被液相所包围的主相晶粒的自由转动，造成磁体的取向度降低。对于取向度较低的DP生坯，烧结中影响Nd-Fe-B磁体取向度的前一种机制是主导的；而对于取向度较高的振动RIP生坯，烧结过程中后一种机制起主导作用。