Fe_3O_4 nano-whiskers by ultrasonic-aided reduction in concentrated NaOH solution

Fe 3 O 4 nano-whiskers were synthesized via ultrasonic-aided reduction of FeCl 2 ·4H 2 O with N 2 H 4 ·H 2 O in concentrated NaOH solution. Phase identification and morphology observation were conducted by X-ray diffraction (XRD) analysis, transmission electron microscopy (TEM) and field emission scanning electron microscopy (FE-SEM). Face scanning energy dispersive spectrum (face scanning EDS) and two-dimensional fast Fourier transform (2DFFT) for element distribution were carried out for confirming compos...     

Erratum to "Aerosol pollution in China: Present and future impact on environment"

PARTICUOLOGY regrets that the above paper was mistakenly classified as a ‘Review’ rather than an ‘Invited paper’ when originally published in volume 7, issue 6, 426–431.     

W18Cr4V

The frictionand wear characteristics of the surfa ce compound layer of W18Cr4V steel by combined treatment of ion nitrocarburizing-ion sulphurizing were investigated. The friction coefficient of the compound l ayer against GCr15 steel was determined witha block-ring friction tester. The wear test was carried out with a reciprocating wear tester. The worn surface was analyzedby scanning electron microscopy(SEM). The experimental results reveale d that the friction coefficient was lower for treatedW18Cr4V steel against GCr1 5 steel. The wear resistance of the compound layer was higher because the nitroc arbonide andthe sulphide in the compound layer were capable of friction-reduct ion and adhesion-inhibition.     

Synthesis, Crystal Structure and Antibacterial Activities of 3-[3-Methyl-（2-thienyl）methyl-enehydrazinocarbonyl]-（1H）-1,2,4-triazole

1 INTRODUCTION Azole derivatives, such as the derivatives of pyra- zole, imidazole, triazole including benzotriazole, te- trazole and indole, have extensive biological activi- ties. They have become the central focus of studies of agricultural chemicals, medicines, plant growth regulating agents and so on[1, 2]. Schiff bases also constitute a good type of biologically active sub- structures. Studies on pyrazole Schiff base-type fun- gicides have been reported[3, 4]. However, some struc- …     

Crystal Structure, Energy Band and Optical Properties of Phosphate In（PO3）3

1 INTRODUCTION stand the chemical bonding properties and electronic origins of optical transition for solid In(PO3)3, the During the past decades, many indium phosphates crystal energy band and optical response functions have been reported and researched on their conduc- are also calculated. tivity anisotropy, band structure and optical proper- ties[1, . However, to our current knowledge, the com- 2] 2 EXPERIMENTALAND pounds containing alkaline-earth metals are rarely COMPUTATIO…     

Spectral Parameters of Nd^3＋ Ion in Nd^3＋：KLu（WO4）2 Crystal

1 INTRODUCTION There has been increasing interest in the re-search of diode laser-pumped solid-state lasers in re-cent years because of the rapid development of highpower diode lasers. Nd:YAG and Nd:YVO crystalsare commercially available, but limited to low Nd3 (= 1 at.%) doping concentration and to narrow ab-sorption bands near the diode emission wavelengthof 808 nm. Therefore, it is necessary to explore moreefficient crystal materials for diode-pumped solid-state lasers. The alkali …     

Synthesis and Crystal Structure of the Derivative of Hydroquinone from Mannich Reaction

1 INTRODUCTION Mannich reaction plays an important role in theconstruction of a large variety of nitrogen-containingmolecules, for instance, some pharmaceuticals andnatural products[1, . In practice, phenols and naph- 2]thanols can serve as the substrate of Mannich reac-tion to obtain aminomethylate by the treatment withformaldehyde and amines or nitrogen heterocycliccompounds[3～5]. We report herein the synthesis andcrystal structure of a new nitrogencontaining co…     

DFT Studies on Electronic Structures of Boro-Nitride-Carbon Nanotubes

1 INTRODUCTION Since the discovery of carbon nanotubes (CNTs) by S. Iijima[1] in 1991 as a quasi-one-dimensional nano-material, extensive attention has been paid to CNTs due to their special electric conductivity, me- chanical properties and potential applications in molecular device, complex material and so on. The structures of CNTs could be described as graphite sheet with planar hexagonal network structure cur- ling into a tube having the diameter of only several nanometers. In t…     

金属Al薄膜基微池强制沉积胶体光子晶体的制备

强制沉积法是一种利用自组装原理快速沉积胶体晶体有序阵列的模板方法. 我们利用微机械刻划法加工金属Al薄膜, Al膜厚控制微粒粒径和聚醚砜膜厚控制层数, 成功地制备了用于强制沉积光子晶体的微池装置. 为了检验该微池装置的有效性, 我们分别测试了不同粒径(224, 245和283 nm)单分散聚苯乙烯微球的沉积效果, 并且对其中一种微球(283 nm)进行了不同温度的烘干处理, 检验了烘干温度对该样品表面形貌和光子带隙中心波长的影响. 实验结果表明, 该光子晶体呈面心立方结构, 内部晶格完整, 缺陷较少, 带隙中心波长的实验值与计算值符合得较好. 此外, 烘干处理可以使构成光子晶体的微球发生微观变化, 并导致光子带隙中心波长的蓝移.     

水相中磷钼酸催化三组分合成烯丙基胺

以磷钼酸作为催化剂，芳香醛、胺和三丁基烯丙基锡三组分在水作为溶剂，室温下高产率的得到相应的烯丙基胺。