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A DOUBLE-TEMPERATURE-GRADIENT TECHNIQUE FOR THE GROWTH OF PURE C60 SINGLE CRYSTALS FROM THE VAPOR PHASE 总被引:1,自引:0,他引:1 下载免费PDF全文
Pure C60 single crystals were grown by a sublimation-condensation method in an evacuated dosed quartz tube situated in a double-temperature-gradient furnace. Large C60 single crystals, up to a size of 0.6 mm×1.0 mm×2.0 mm with quite smooth and shiny faces, were obtained. X-ray diffraction, electron diffraction and X-ray morphology were carried out and showed that the quality of large C60 single crystals grown by the double-temperature-gradient technique is excellent. In this paper the experimental results of the growth of large C60 single crystals are reported and the morphological and structural characterizations are discussed in detail. 相似文献
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利用STS测量并结合扫描隧道显微镜(STM)扫描图象,给出一组沿石墨单晶表面原子分辨的STM图象上某一线段各点处的扫描隧道谱.d(lnI)/d(lnV)~eV由测量谱给出的样品表面EF附近局域态密度分布与由体能带结构计算得到的结果在一定程度上相符合,将各条曲线中EF附近的态密度峰能量对相应的空间位置作图,给出石墨表面EF附近能态密度在测量区域内实空间的变化。通过对表面不等价A,B类原子处局域电子结构的分析并利用简单模型进行计算,给出了与实验
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The distribution, morphology and structure of carbon nanotubes and buckyonions produced from an arc discharge were investigated by means of scanning electron mi-croscopy and high-resolution transmission electron microscopy, The nanotubes and nanoonions were found to be located mainly near the porous region of the core in the deposited rods and the transition region between the growth ring-shaped graphite sheets. The tube bundles grew freely from carbon particles. Apart from the straight-line tubes, curved and bent tubes were also found. Studies on the structure of them showed that the carbon atomic sheets in the nanotubes displayed a stepped bending. Transverse sectional study predicted a helical structure of the carbon atomic sheets. In addition, the relationship between the number of pentagonal rings and cone angle at the tips of the tubes, as well as the mechanism of the formation of the steplike structure, were discussed. 相似文献
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A DOUBLE-TEMPERATURE-GRADIENT TECHNIQUE FOR THE GROWTH OF PURE C60 SINGLE CRYSTALS FROM THE VAPOR PHASE 下载免费PDF全文
Pure C60 single crystals were grown by a sublimation-condensation method in an evacuated dosed quartz tube situated in a double-temperature-gradient furnace. Large C60 single crystals, up to a size of 0.6 mm×1.0 mm×2.0 mm with quite smooth and shiny faces, were obtained. X-ray diffraction, electron diffraction and X-ray morphology were carried out and showed that the quality of large C60 single crystals grown by the double-temperature-gradient technique is excellent. In this paper the experimental results of the growth of large C60 single crystals are reported and the morphological and structural characterizations are discussed in detail. 相似文献
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用气相法生长出了毫米尺寸的具有规则晶面和金属光泽的高质量的纯C60单晶.X射线衍射分析表明,C60单晶在室温下具有面心立方(fcc)结构,晶格常数为α=1.4199(4)nm。用扫描电子显微镜和光学显微镜观察了C60单晶的形貌,除观察到fcc结构的晶体所特有的{111}和{200}两种稳定晶面以及非常容易形成的孪晶之外,还发现了在{111}面上的树枝状、垄状和生长丘以及在{200}面上的树枝状、游泳池状和生长丘的生长缺陷。对C60
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