背景磁场下Y系超导带材临界电流的测量

高温超导电力装置一般工作于低磁场情况下,测量超导带材在低场下的临界电流特性非常重要.文中通过自行设计的实验平台,采用四引线法对Y系超导带材低场下的临界电流特性进行了测量,得到了带材临界电流随外加磁场变化的曲线,并与Bi系带材低场下的临界电流特性进行比较.     

Flame‐retardant and mechanical properties of phenolic foams toughened with polyethylene glycol phosphates

Three kinds of polyethylene glycol phosphates (PEGPs) toughening agents were synthesized by esterification of phosphorus pentoxide (P₂O₅) with polyethylene glycol and characterized by Fourier transform infrared spectra and ³¹P nuclear magnetic resonance. A series of lightweight phenolic foams toughened with different loadings of PEGPs were prepared. Optical microscopy results show that the addition of PEGPs with small molecular weight PEG improves the structural homogeneity of phenolic foams obviously. The flame retardancy of toughened phenolic foams was evaluated by using UL 94, limiting oxygen index, and cone calorimeter. The results indicate that the incorporation of PEGPs not only increases the toughness of phenolic foams but also improves their flame retardancy. Moreover, the thermal stability of PEGPs and the toughened foams was investigated by thermogravimetric analysis. Copyright © 2013 John Wiley & Sons, Ltd.     

Fire properties of silylated α‐zirconium phosphate composites based on polystyrene

α‐zirconium phosphate (ZrP) (prepared by both reflux and hydrothermal methods) is silylated with chlorotrimethylsilane and characterized by X‐ray diffraction, Fourier transform infrared spectroscopy and scanning electron microscopy. Polystyrene/silylated‐ZrP composites show higher thermal stability as the ZrP content increases. Cone calorimetry suggests that the reduction of the peak heat release rate of polystyrene (PS)/ZrP composites does not increase as the ZrP loading increases; the aspect ratio of ZrP has little effect in fire performance of PS/ZrP composites. Copyright © 2013 John Wiley & Sons, Ltd.     

DEGENERATE OPTIMAL BASIS GRAPHS IN LINEAR PROGRAMMING

§ 1　IntroductionA graph-theoretic approach for investigating basis transformations in a linear pro-gramming has been historically developed.Let V be the setof all bases with respectto thecolumn vectors of a matrix A.Two bases are called adjacentifthey can be transformed intoeach other by a pivot operation.Denote by E the set of edges each of which is incidentwith a pair of adjacentbases.Then G=(V,E) is called the basisgraph of matrix A(or ofthe corresponding LP) .Tucker[1 ] first called…     

一种新的结合NCP函数的SQP滤子算法

对于SQP滤子算法,本文提出了一种新方法来构造滤子,目的是为了使滤子的接受条件更宽松,降低进行可行性恢复的机率.另外,本文通过一些数值例子对这种新算法进行了检验,事实证明这种算法是有效的.最后还证明这种算法具有超线性收敛性.     

EDGEWORTH EXPANSION FOR NEAREST NEIGHBOR- KERNEL ESTIMATE AND RANDOM WEIGHTING APPROXIMATION OF CONDITIONAL DENSITY

§ 1　 IntroductionThere are many discussions on the estimate of density,for example,the kernel andnearest neighbor estimates.Reference [1 ] gave the nearest neighbor-kernel estimate ofconditional density.[2 ] discussed the properties on the nearest neighbor-kernel estimateand bootstrap approximation of conditional density.[3 ] studied some asymptotical proper-ties on kernel estimate and random weighting approximation of density.In this paper,wewill discuss the properties of the nearest neighb…     

氟电极测定铝的新方法——Apple Ⅱ-ISE智能离子计的应用

本文提出一种氟电极测铝的新方法,即二次回归校正曲线法及分段抛物插值法。由于汇集了1.该法依据的数学模型与实验数据相符;2.AppleⅡ-ISE智能离子计具有较强的数据处理功能;3.氟电极性能良好等三个特点,故本法准确可靠,快速方便,具有一定理论意义和较大实用价值。     

宁波大桥主墩墩址软弱带成因机制研究

通过对宁波大桥主墩墩址软弱带详细的地质勘测和综合方法研究，内中包括粘土泥质物Ｘ射线衍射分析，软弱带岩石化学成分和不同成因砂和砾石的成分和特征研究，特别是软弱带的显微构造和物质来源的研究，本文对这一软弱带的成因机制着重进行了探讨。研究发现，这一软弱带在结构上可划分为三部分或三层结构，下部为挤压破碎带、中部为风化产物、上部为地表水贯入充填堆积。它表明这一软弱带经历了三种不同的地质作用的演化过程或具有三种物质来源。这一研究结论对大桥的设计和施工有重要的影响和意义。     

光电直读光谱法测定稀土铝合金中La,Ce,Pr,Nd,Sm ,Si,Fe,Cu

本文报道了稀土铝合金中La,Ce,Pr,Nd,Sm,Si,Fe,Cu的光电直读光谱测定，对光源的激发方式及最佳工作条件进行了选择，应用KH－5高能预火花光源，采用单向全功率放电，先冲洗3秒，然后预燃5秒，曝光10秒。各元素谱线间无干扰，。使用固体试样，样品处理简单。经试验验证该法简便快速，精密度准确度高，含量在0．001％－0．002％之间RSD＜6％，0．02％－0．3％之间RSD＜3％，标准样品的测定值与准确值吻合较好，结果令人满意。     

极性非质子溶剂与甲醇或1,2-二氯乙烷的汽液平衡

使用双沸点仪测定了丙酮、乙酸乙酯、对二氧六环、乙腈或三乙胺与甲醇或1,2→二氯乙烷以及二者混合物等十一组二元体系在99.3 kPa下的汽液平衡数据(T,x,p), 计算了有关体系的过量吉布斯自由能。结果表明, 六种非质子溶剂与甲醇组成的二元系GE>0; 乙腈或三乙胺与1,2-二氯乙烷组成的二元系GE>0, 而丙酮、乙酸乙酯或对二氧六环与1,2-二氯乙烷的二元混合物GE<0。从同种分子间或不同种分子间的缔合作用对上述结果进行了讨论。本文还在固定极性非质子溶剂(第三组分)物质的量浓度的条件下, 测定了非质子溶剂+1,2-二氯乙烷+甲醇三元混合物的汽液平衡数据, 考察了非质子溶剂的加入对甲醇+1,2-二氯乙烷二元系GE的影响。