Synthesis and Crystal Structure of Fluoride K2(Ta0.9I0.1)F7 with the Micro-Isomorphic Substitution in the Ta Cationic Position

Crystallography Reports - Fluoride crystals K2(Ta0.9I0.1)F7 (sp. gr. Р21/c) complementary to the K2TaF7 and K2NbF7 fluoride family have been obtained by hydrothermal synthesis. Their...     

Inherent electrochemical activity of TiO2 (anatase,rutile) enhances the charge capacity of cathodes of lithium-sulfur batteries

Journal of Solid State Electrochemistry - The addition of nanocrystalline titanium dioxide (P90) to a cathode of Li/S cell enhances its voltammetric charge capacity by 19%, from which only a small...     

Dislocation Structure Evolution in Low-Stability States of Solid Solutions of Alloys Under Their Deformation

Russian Physics Journal - The results of a study of the dislocation structure evolution in polycrystals of homogeneous solid solutions in low-stability states in Cu-Mn-based alloys with FCC crystal...     

Numerical Simulation of a Multi-Output Radar Orthogonal Waveform Based on a Chaos Optimization Algorithm

Russian Physics Journal - Aiming at problems of low probability of interception and poor anti-jamming performance of the multi-output radar, the numerical simulation based on a chaos optimization...     

Synthesis and characterization of cellulose acetate from cellophane industry residues. Application as acetaminophen controlled-release membranes

Journal of Thermal Analysis and Calorimetry - Cellophane film production generates cellulosic residues from scraps, edges, and low-quality films. In this work, cellophane was used as a raw material...     

Mechanical Characteristics of Diamond-Like Moiré Films

JETP Letters - The mechanical characteristics of diamond-like films, such as Dn21.8, Dn27.8, and Dn29.4 moiré diamanes, formed by the hydrogenation of graphene layers twisted at an angle of...     

Rapid qualitative profiling and quantitative analysis of Juglandis Mandshuricae Cortex and seven flavonoids by ultra-high performance liquid chromatography–quadrupole/orbitrap high-resolution mass spectrometry

Juglandis Mandshuricae Cortex is the bark of Juglans mandshurica Maxim., which has been used as a folk medicine plant in China and India. In this study, an ultra-high performance liquid chromatography–quadrupole/orbitrap high-resolution mass spectrometry method was developed to clarify and quantify the chemical profiling of Juglandis Mandshuricae Cortex rapidly. A total of 113 compounds were characterized. Among them, seven flavonoids were simultaneously quantified in 15 min, including myricetin, myricetrin, taxifolin, kaempferol, quercetin, quercitrin, and naringenin. The method was validated for accuracy, precision, and the limits of detection and quantification. All calibration curves showed a good linear relationship (r > 0.9990) within test ranges. The intra- and inter-day relative standard deviations were less than 2.16%. Accuracy validation showed that the recovery was between 95.6 and 101.3% with relative standard deviation values below 2.85%. The validated method was successfully applied to determine the contents of seven flavones in Juglandis Mandshuricae Cortex from seven sources and the contents of these places were calculated respectively. This method provides a theoretical basis for further developing the medicinal value of Juglandis Mandshuricae Cortex.     

X-ray Diffraction Study of Structural Changes in High-Strength Ceramics Based on Zirconium Oxide with Additions of Ytterbium and Neodymium Oxides after Hydrothermal Treatment

Crystallography Reports - A surface structural analysis of two ceramic samples of zirconium oxide (ZrO2) sintered at 1550°C, stabilized in the tetragonal form, before and after hydrothermal...     

Vaidya’s Method for Convex Stochastic Optimization Problems in Small Dimension

Mathematical Notes - The paper deals with a general problem of convex stochastic optimization in a space of small dimension (for example, 100 variables). It is known that for deterministic problems...     

Magnetoresistance and Quantum Oscillations in WTe2 Semimetal

Physics of the Solid State - The discovery of extreme magnetoresistance (MR) in nonmagnetic materials attracted attention to WTe2 semimetal. We studied MR in a single crystal of tungsten...