Variation of supramolecular structure of heat-resistant polyimide films during thermal treatment

Variation of the supramolecular structure of heat-resistant polymide films in the course of high-temperature treatment was studied by X-ray diffraction analysis and NMR spectroscopy in solids.     

Structuring of polyacrylonitrile solutions

Mechanisms of orientation for the solutions of polyacrylonitrile synthesized under conditions of radical and anionic polymerization were studied. The effect of the fractal-matrix structuring agent developed by the AIRES foundation on the correlation parameters of the solution density and average squared fluctuation polarizability, which can be used to determine how the supramolecular structure changes by “self-orientation” and “induced orientation” mechanisms, was analyzed.     

Changes in the supramolecular structure of heat-resistant polyimide fibers in the course of thermal treatment

Changes in the supramolecular structure of heat-resistant fibers based on polyimide PM were studied by X-ray diffraction analysis and NMR spectroscopy.     

Silver Intercalation into Cellulose Matrix. An X-Ray Scattering,Solid-State 13C NMR,IR, X-Ray Photoelectron,and Raman Study

Diffusion of silver ions into a cellulose matrix and their subsequent reduction both with the matrix itself and with specific reducers lead to preparation of cellulose materials containing silver(0). Most silver metal is intercalated into the cellulose matrix when glycerol is used as solvent and potassium hypophosphite or sodium boron hydrate are used as reducers.     

Thermochemical aspects of interaction of polyimide composites with organic sorbents

Interaction of ITA-31 polyimide binder with a series of industrial sorbents based on styrene and vinylpyridine derivatives was studied.     

Prospects for Using Polyacrylonitrile for Preparing Carbonized Polymeric Composites

The thermochemical cyclization of different polyacrylonitrile samples prepared by radical and anionic polymerization was studied by thermal analysis, spectroscopy, and AM1 semiempirical calculations. The possibility of using polyacrylonitrile as a cocarbonizate for preparing mixed carbon composites with nitrogen-containing polysaccharides was examined.__________Translated from Zhurnal Prikladnoi Khimii, Vol. 78, No. 5, 2005, pp. 810–813.Original Russian Text Copyright © 2005 by Sazanov, Novoselova, Amsharov, Ugolkov, Andreeva, Gribanov.     

Colorimetric and test determination of tetracycline and doxycycline in milk and milk products after sorption concentration at chemically modified aluminosilicate

A technique of colorimetric and test determination through reaction with iron(III) on the surface of chemically modified aluminosilicate for tetracycline and doxycycline was developed. The advantages of the technique are its rapidity, ease of performance, affordability, and good metrological characteristics. The method could be used in laboratories that perform chemical analysis of foodstuffs.     

Problems of solubility of hydrolysis lignin

Interaction of hydrolysis lignin with polyacrylonitrile in water-dimethyl sulfoxide solution in the presence of an activator was studied, and the properties of the products were examined.