激光旋光法监测谷氨酸钠浓度的实验研究

味精精制过程中的谷氨酸钠溶液浓度需控制在一定的范围。本文报道一种可用于在线监测谷氨酸钠浓度的双光束激光旋光差动式检测法,并对该方法的可行性进行了初步的实验研究。实测结果表明本方法有较好的实用性。     

光电检测法在线测控糖液过饱和度的研究

过饱和度是糖液结晶过程中的主要测控参量.本文报道一种新型的光电检测法在线测控糖液过饱和度的原理与方法,给出其理论模型、系统构成和在单晶冰糖结晶工序上的应用结果.     

光象散法测量溶液浓度的研究

本文报道一种用光象散技术测量溶液浓度的新方法。给出其理论解析、测量原理、系统构成与实验结果。从理论研究与初步实验结果表明,本方法用于自动测量溶液浓度有好的可行性与实用性,亦可作为在线监测。     

不同形态SnO2纳米晶的制备

In this paper, we report our research on morphologically selective synthesis of nanocrystalline SnO2 by the combination of hydrothermal preparation and calcinated process. We firstly prepared SnO2 nanocrystals by the hydrothermal method at 140 ℃ for 3 h, using SnCI4 as the reactant. With the initial pH of 1.8 or 1.34, we prepared uniform and well-dispersed SnO2(tetragonal) nanocrystals, with similar size of about 3 nm, as determined by TEM. However, after being calcinated at 500 ℃ for 2 h, specimen 1 prepared at pH＝1.8 showed the rod-like shape with an average size of 5 nm×20 nm, while the other one(specimen 2)prepaed at pH＝1.34 showed a granular shape with an average size of 10 nm. XRD experiments showed that specimen 1 had a new diffraction peak after calcination, which was contributed by the (023) face of orthorhombic SnO2. The experiment results indicated that the morpholgy of SnO2 nanocrystals after calcination was closely related to the initial acidity of the reaction solution, possibly due to the difference in surface properties, e.g. the difference in crystalline faces exposed to the surface of particals, under different hydrothermal conditions.     

光导纤维的观察法电弧熔接

<正> 光导纤维(以下简称光纤维)的芯径一般在2微米(单模)到50～100微米(多模)。要把这样细小的纤维连接起来,并使其连接点损耗低以及确保传输特性不受破坏,一般的连接技术都不能满足要求。光纤维连接形式归纳起来不外乎是两大类:可拆卸连接和不可拆卸连接。一般说来,对光纤维连接点的要求是低损耗、连接强度好、操作简便、效率高。对光缆接头来说还要求互换性好。而其中连接损耗是衡量光纤维连接质量