基于物理课堂有效教学的策略浅析

根据有效教学的理念提出了课堂有效教学的基本策略、动力策略和长效策略,并结合基础物理的教学,对这些教学策略的科学掌握和运用进行了探讨.     

Crystal structure of β-cyclodextrin-4-chlorobenzoic acid complex:Unusual C-Cl…π interaction between 4-chlorobenzoic acids in β-cyclodextrin dimer

The inclusion complex ofβ-cyclodextrin（β-CD） with 4-chlorobenzoic acid was synthesized and its crystal structure was determined by single crystal X-ray diffraction under cryogenic condition.The complex contains twoβ-CDs,two 4-chlorobenzoic acids and twenty-nine water molecules in the asymmetric unit,and can be formulated as 2(C₄₂H₇₀O₃₅)·2（C₇H₅O₂Cl）·29（H₂O）.In the crystal lattice,twoβ-CDs form a face-to-face dimer jointed together through hydrogen bonding between the secondary hydroxyl groups ofβ-CDs.Two 4-chlorobenzoic acid molecules which contact by C-Cl…πinteractions are included in theβ-CD dimer cavity.Theβ-CD dimers are arranged in brickwork-like pattern along the crystallographic a-axis.The effect of guest molecule length on the inclusion geometry was discussed by comparative study of someβ-CD complexes containing similar guests.     

异常血红蛋白酶解肽段硅胶薄板指纹图谱法的改良

本文叙述了改进的硅胶薄板指纹图谱法用于异常血红蛋白结构分析中的肽段分离工作。此法设备简单、省时省料,使用比较简陋的实验条件即可获得较好的实验结果,克服了高效液层法(HPLC)和反相高效液层法(RP—HPLC)要求设备昂贵,高压电泳法有害气体严重以及RP—HPLC的某些失活问题等     

Removal of phosphate from aqueous solution by zeolite synthesized from fly ash

Fifteen Chinese fly ashes were converted hydrothermally into zeolites, and phosphate immobilization capacity (PIC) of the synthesized zeolites and the corresponding raw fly ashes were determined using an initial phosphate concentration of 1000 mg/L. Results showed that there was a remarkable increase in PIC (from 1.2 to 7.6 times) following the synthesis process. Fractionation of immobilized phosphorus indicated that Fe+Al-P increased most significantly and consistently among all the phosphorus fractions following the conversion of fly ash to zeolite. The PIC and Ca+Mg-P were closely related to Ca content (with r values of 0.9683 and 0.9651, respectively) rather than Mg content (with r values of 0.3920 and 0.3212, respectively). The r values of PIC and Fe+Al-P with Fe content (with r values of 0.4686 and 0.6385, respectively) were higher than those with Al content (with r values of -0.7857 and -0.3770, respectively). Although calcium and iron components were mainly involved in phosphate immobilization, there was no significant change of Ca and Fe content following the conversion of fly ash to zeolite. Increase in dissociated Fe(2)O(3) and specific surface area probably accounted for the enhancement in PIC of synthesized zeolites compared with corresponding fly ashes. The PIC value of zeolites showed a significant correlation with dissociated Fe(2)O(3) (r=0.6186). The specific surface area increased 26.0-89.4 times as a result of the conversion of fly ash to zeolite. The maximum removal of phosphate occurred within different pH ranges for zeolites which were synthesized from high, medium and low calcium fly ashes and this behavior was explained by the reaction of phosphate with calcium and iron components.     

嗪草酮与脱氧核糖核酸相互作用的研究

采用电化学方法,结合紫外-可见分光光度法、荧光光度法、粘度法和与变性脱氧核糖核酸(DNA)的作用研究了嗪草酮(M)与DNA的作用机制,并通过研究嗪草酮对溴化乙锭-天然DNA体系的影响,以及天然DNA和变性DNA与嗪草酮的作用的不同,得出嗪草酮与DNA分子发生类似溴化乙锭(EB)嵌插作用的结论,形成DNA-M 1∶1型的超分子化合物DNA-M。求得结合常数β=1.8×105L/mol。DNA加入量在1×10-5~1.5×10-4mol/L范围内,DNA浓度与峰电流降低值之间存在线性关系。     

The economic lot scheduling problem under extended basic period and power-of-two policy

The economic lot scheduling problem schedules the production of several different products on a single machine over an infinite planning horizon. In this paper, a nonlinear integer programming model is used to determine the optimal solution under the extended basic period and power-of-two policy. A small-step search algorithm is presented to find a solution which approaches optimal when the step size approaches zero, where a divide-and-conquer procedure is introduced to speed up the search. Further a faster heuristic algorithm is proposed which finds the same solutions in almost all the randomly generated sample cases.     

碘离子选择电极催化动力学法测定钒(V)的研究

本文介绍用碘离子选择电极催化电势动力学法对测定钒(Ⅴ)进行的研究,发现去氢抗坏血酸是钒(Ⅴ)催化BrO_3-氧化I~-体系的一种良好的活化剂,详细地研究了各种因素对测定的影响,找出了测定钒(Ⅴ)的较佳条件。该法测定钒(Ⅴ)浓度的线性范围很宽,检测限为2×10~(-10)mol/l,灵敏度比文献报道的高3个数量级。对几种离子的干扰进行了试验,柠檬酸可以有效地掩蔽这些离子的干扰。此法曾应用于测定自来水和头发中的钒,得到了较好的结果。     

A NEW EXTENSION OF THE HIGH-ORDER VIRASORO ALGEBRA

1 IntroductionVirasoro algebra and W algebra have been widely investigated by both physicists andmahematicians. Virasoro algebra can be thought of as the central extended algebra Of diffeOmorphisms Di$S') on the circle S1. In Ref[1], ftaPpat et al. extended the notion ofloop algebra g(S') to algebra g(M), M being a closed surface with dim M > 1, and gave thefolowing commutation relations:c,[Lk,l, L.,.] = [mp(k -- T) -- ftO(l -- 8)]Lk .,l , ti ll ghO(k -- j) -- fl0(l -- j)lok .,O8l ,,…     

Numerical simulation of control ablation by transpiration cooling

A transient, one-dimensional numerical model is developed to describe the processes of transpiration cooling and ablation of the porous matrix used for the cooling. This model is based on the assumption of local thermal equilibrium. The problem of moving boundary due to ablation of the porous matrix is treated by the front-fixing method. This paper discusses the results of numerical simulations under different conditions and control parameters of ablation process. It was found that cooling effects and ablation processes are influenced by the coolant mass flow rate, the intensity of the heat flux, and the initial temperature at the start of transpiration cooling. In additional to the above three parameters, the Stefan number and the Biot number can also influence the transient cooling process, control ablative thickness of the porous plate by the reduction of ablative speed and duration, respectively.     

带有分段常数变元的时滞微分方程解的稳定性和振动性

本文讨论带有分段常数变元的时滞微分方程解的渐性性质。我们利用Ｒａｚｕｍｉｋｈｉｍ方法证明了零解的稳定性，并且改进了文［１］得到的两上振动定理。