广义H non映射的滑模变结构控制同步

基于可线性化的非线性离散变结构跟踪控制方法实现了广义H non映射混沌系统的同步 .广义H non映射的混沌吸引子比H non映射的混沌吸引子要复杂得多 ,对于保密通信来说 ,这种复杂性正是所期望的 .提出的同步方法允许参数有适当的失配程度 ,这对工程实现是非常有利的 ,理论分析和仿真结果证实了该方法的有效性     

ELECTROLUMINESCENCE SPECTRA OF GexSi1-x/Si SINGLE QUANTUM WELL

The electroluminescence of Ge_xSi_1-x/Si single quantum well was measured at temper-atures above room temperature along the growth direction and the direction normal to it. TO and NP peaks were resolved.     

Ge BEAM TREATMENT OF Si SUBSTRATE FOR MOLECULAR BEAM EPITAXY

A new surface cleaning method for Si MBE is described in which a very weak Ge beam flux is deposited on the surface for removing the thin passivative layer of SiO₂ on the Si subetrate. It has proved that the SiO₂ will react with Ge at a relatively low temperature (620℃), and as a result, the oxide layer becomes volatile. Here the high temperature annealing in the conventional Shiraki method is no longer required, and since the oxide layer is removed in ultra high vacuum, only very little carbon contamination may occur. Furthermore, to reduce the excessive Ge on the substrate surface, Ge is deposited at 620℃ and then the sample is annealed at 700℃; the residual Ge atoms on Si substrate can be reduced to less than 0.1 monolay-er (ML). Ge beam treatment turns out to be an effective low-temperature Si surface-cleaning method, especially for the heteroepitaxial growth of Ge_xSi_1-x/Si.     

NON-NEGATIVE SOLUTIONS FOR A CLASS OF NON-POSITONE PROBLEMS

1IntroduInthispaperwestudyill(.)(l}xlsl(.)ll(:()noTI-1)ega,t]v(3s(>1lltionsfort,h(i1,woilo]lit,boundaryvalueproblemsu\ry;l;(:i.t>(v,>\,:t),:j:=fti-i'...ifn(j)>l),A>0isdcollstanta,f,dj'e(!'l,.,ti,fi<,,f(())<0(l.:i)111.of)i(lfllsifs{.1.l:)-(.I.2)havel,ecnsi…     

广义Hénon映射的滑模变结构控制同步

基于可线性化的非线性离散变结构跟踪控制方法实现了广义Hénon映射混沌系统的同步.广义Hénon映射的混沌吸引子比Hénon映射的混沌吸引子要复杂得多,对于保密通信来说,这种复杂性正是所期望的.提出的同步方法允许参数有适当的失配程度,这对工程实现是非常有利的,理论分析和仿真结果证实了该方法的有效性 关键词： 广义Hénon映射 混沌 同步 变结构控制     

牛血清白蛋白在NVP/HEMA无规共聚物水凝胶上的吸附研究

合成了不同含水量的N-乙烯吡咯烷酮(NVP)／甲基丙烯酸-β-羟乙酯(HEMA)共聚物水凝胶．研究了温度、pH值，蛋白质初浓度及离子强度等因素对牛血清白蛋白吸附性能的影响．采用紫外分光光度法测定BSA的吸附量．结果表明，蛋白质初浓度越高．温度越高，离子强度越大；蛋白质内部更多的疏水性氧基酸残基暴露于外部．吸附量增加：在等电点pH=4．7附近蛋白质沉积量最大．     

Imidazole Coordinated Sandwich-type Antimony Polyoxotungstates Na9[ {Na（H=O2}3{M（C3H4N2）}3（ Sb W9O33）2]·xH=O（M=Ni^Ⅱ, Co^Ⅱ, Zn^Ⅱ, Mn^Ⅱ）

The imidazole covalently coordinated sandwich-type heteropolymngstates Na9[ {Na（H=O2}3{M（C3H4N2）}3（ Sb W9O33）2]·xH=O（M=Ni^Ⅱ, Co^Ⅱ, Zn^Ⅱ, Mn^Ⅱ） were obtained by the reaction of Na2WO4·2H2O, SbCl3·6H2O, NiCl2·6H2O [MnSO4·H2O, Co（NO3）2·6H2O, ZnSO4·7H2O] and imidazole at pH≈7.5. The structure of Na9[{Na（H2O）2}3{Ni（C3H4N2）}3（SbW9O33）2]·32H2O was determined by single crystal X-ray diffraction. Polyanion [{Na（H2O）2}3{Ni（C3H4N2）}3（SbW9O33）2}3]^9- has approximate C3v symmetry, imidazole coordinated six-nuclear duster [{Na（H2O）2}3{Ni（C3H4N2）}3]^9＋ is encapsulated between two （α-SbW9O33）^9-, the three rings of imidazole in the polyanion are perpendicular to the horizontal plane formed by six metals （Na-Ni-Na-Ni-Na-Ni） in the central belt, and x-stacking interactions exist between imidazoles of neighboring polyanions with dihedral angel of 60%. The compounds were also characterized by IR, UV-Vis spectra, TG and DSC, and the thermal decomposition mechanism of the four compounds was suggested by TG curves.     

水煤浆添加剂与煤之间的相互作用规律研究 Ⅰ. 复合煤颗粒间的相互作用对水煤浆流变性的影响

使用12种不同分散剂对14种不同变质程度的煤进行了成浆性实验，分析了182个水煤浆(CWS)样品的流变性。结果表明，低变质程度和高灰煤浆多呈屈服假塑性，煤的性质起主导作用；变质程度高且灰分较低煤浆的流变性，主要依赖于分散剂的结构与性质；分子结构单元立体空间效应大，疏水基团与亲水基团呈立体间隔分布的分散剂，易形成屈服假塑性CWS；分子线度长，亲水基团与疏水基团呈线性间隔分布的分散剂，易形成胀塑性CWS。复合煤粒间的相互作用方式是决定CWS流变特性的关键。     

超高效液相色谱-串联四极杆飞行时间质谱法快速分析东革阿里化学成分

应用超高效液相色谱-串联四极杆飞行时间质谱法(UPLC-Q-TOF-MS)对东革阿里提取物的化学成分进行定性分析。采用Agilent Eclipse Plus-C_(18) RRHD色谱柱(2.1 mm×100 mm,1.8μm),以乙腈-0.1%甲酸水为流动相进行梯度洗脱。质谱分析采用电喷雾正离子模式采集,通过对照品比对及高分辨质谱数据解析,鉴定了49种化学成分,包括29种苦木素二萜、4种β-咔巴啉类生物碱、12种铁屎米-6-酮类生物碱、3种联苯新木脂素类及1种角鲨烯型三萜。该方法快速、可靠、高效,能较全面地反映东革阿里的化学成分,可为深入阐明东革阿里的药效物质基础及质量标准研究提供参考。     

铀—2—（3,5—二—2—吡啶偶氮）—5—二乙氨基苯酚—Triton—X—100析相体系…

本研究了铀－２－（３，５－二溴－２－吡啶偶氮）－５－二乙氨基苯酚（３，５－ｄｉＢｒ－ＰＡＤＡＰ）－Ｔｒｉ－ｔｏｎ－Ｘ－１００析相光度体系，建立了矿石中微量铀的测定方法。在ＰＨ７．５三乙醇胺－盐酸介质中，将胶束溶液在９５±１℃。络合物即被Ｔｒｉｔｏｎ－Ｘ－１００相完全富集。