聚合氯化铁中OH／Fe物质的量比的测定

讨论了测定聚合氯化铁中OH/Fe物质的量比的几种方法,确定用过量碱沉淀法测定聚合氯化铁中的OH/Fe物质量比;同时研究了影响测定的各种因素,找出了最佳的测定条件.通过对合成试样和未知试样的测定,结果表明方法无系统误差存在,结果准确、可靠.     

激光窗口热效应对光束发散角的影响

以DF激光器CaF_2输出窗口为例计算了三种输出功率(10~3W,10~4W,10~5W)情况下,窗口材料的温升、波阵面畸变及对光束发散角的影响。计算中窗口直径为40mm,厚度为10mm,光束直径为20mm。     

加权Bergman空间到μ-Bloch空间的复合算子

给定α>-1,p>0和[0,1)上的正规函数μ,得到了Cn中单位球上加权Bergman空间Aαp到μ-Bloch空间βμ的复合算子C(?)为有界算子和紧算子的充要条件,同时也给出了几个推论．     

压电陶瓷带形中Ⅲ型裂纹的精确分析解

分析无限长压电带形中的Ⅲ型裂纹问题，主要讨论了在带形边界受四种机电组合载荷情况下裂纹位于带形中平面上的情形。通过积分变换，与其相的复合边值问题分别转化为对偶积分方程组，使用对偶积分方程的熟知结果，获得了裂纹线上电弹性场的明显的解析表达式及在裂尖处一些量的强度因子和能量释放率公式。与已知的近似解比较，所得结果是以封闭形式给出的精确解。     

Charge collection of single event effects at Bragg's peak

Using Geant4 Monte Carlo code and Technology Computer-Aided Design(TCAD) simulation,energy deposition and charge collection of single event effects(SEE) are studied,which are induced by low-energy protons and α particles in small feature size devices.We analyzed charge collection of SEE especially at Bragg's peak and obtained two types of deposited energy distributions of protons and α particles at different incident energies.The two components of the total charge collected are quantified,which are due to d...     

Sensing system with Michelson-type fiber optical interferometer based on single FBG reflector

A sensing system,with Michelson-type fiber optical interferometer based on single fiber Bragg grating (FBG) as the reflector,is demonstrated.The system used a frequency-matched ring fiber optical laser as the source.The closed Michelson-type fiber optical interferometer system will be helpful in simplifying the developed interferometric sensor by replacing the double reflectors with only one FBG reflecting the doubleside light.The basic sensing properties of the system are demonstrated,with a fiber optic piezoelectric ceramic transducer embedded in the arm of the interferometer simulating the sensing signal.     

原子荧光光谱法测定动物肝中微量砷

建立了测定动物肝中微量砷的原子荧光光谱方法 ,方法灵敏度高 ,准确度好。在选定的试验条件下 ,荧光强度与砷浓度在 0～ 16 0ng·mL- 1 范围内成线性关系 ,相关系数r =0 9996 ,检出限 0 4ng·mL- 1 ,回收率 94 2 %～ 98 5 % ,相对标准偏差不超过 4 6 %。     

Stereoslective Synthesis of （Z）-1, 2-Bis（arylseleno）-1-alkene by Addition of Cesium Arylselenolate to Alkynyl Selenide

Alkynyl selenide reacted with cesium arylselenolate in commercial THF at r.t under N2 to afford (Z)-1, 2-bis(arylseleno)-1-alkene in high yields.     

一类五次系统的赤道极限环问题

本文解决了一类五次系统赤道环的稳定性与极限环分枝问题,所得的结论与三次系统的若干结论形成有趣的对比.     

拟生灭过程几种遍历性的判别准则(Ⅱ)

本文是文[7]的继续,研究了连续时间拟生灭过程,给出了一类连续时间拟生灭过程l-遍历和几何遍历行之有效的判别准则,并证明其不可能是多项式一致遍历和强遍历的.