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41.
lntroductionThesmallolefinslikeethylene,propeneandbutenearethec0mmerciallydesirablepetrochemicalfeedstocksandarefoundincreasingusageinchemicalindustry.Theyareusuallyobtainedfromthepyrolysis0fpetroleumhydrocarb0nswithsteaInatveryhightemPeratUreandarealsoavailablefromFCCprocess.TheimProvedFCCcatalystforeIhancingtheolefinproducthasbeenreportedll].However,FCCisalrnostimPossiblefortheshortchainalkanefeedstockscutfrompetroleum0robtuinedfromrefinerygasornatUralgassincecrackingofhydrocarbonsbeco… 相似文献
42.
一种高性能小周期摇摆器 总被引:1,自引:0,他引:1
介绍一种高性能小周期摇摆器的设计。采用槽型定位的分离状磁块,实现了磁场的半周期调节,对该摇摆器模型进行的测量表明,当摇摆器的周期λ_w=10mm,磁极间隙δ为5mm时,峰值磁场B_w=0.35T,磁场最大偏差δB_w/B_w<1.25%。 相似文献
43.
分析研究了慢跳频/M进制频率键控(SFH/MFSK)通信系统在存在瑞利(Rayleigh)衰落和莱斯(Rician)衰落的多径延时短波信道上的性能,导出了其准确的比特差错率的表达式,表明多径干扰数及其强度对系统性能的影响.同时给出了它们的数值结果和性能曲线. 相似文献
44.
The effect of the properties of PADC nuclear track detectors after exposure to high doses of gamma absorbed doses up to 5×105 Gray (50 Mrad) were studied. The gamma source was a 9.03 PBq (244 KCi), Co-60 source. Results indicate that each of the bulk etch rate (Vb), the tracks etch rate (Vt) and the sensitivity (V) of the detectors increases with the high gamma absorbed dose, but there is a drop in these parameters at the low gamma absorbed dose. Signs of surface roughness were observed by increasing the gamma absorbed doses and changes in color observed for doses larger than 2×105 Gray. The temperature of detectors during irradiation time reached 41°C. The fission fragment tracks (from Cf-252 source) disappeared quickly within the etching time (minutes) for total absorbed doses greater than 3×105 Gray due to their high bulk etch rate. 相似文献
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《Journal of separation science》2017,40(15):3074-3085
Short‐chain aliphatic amines are a class of hazardous impurities in drug substances. A simple method, involving derivatization followed by high‐performance liquid chromatography with diode array detection, has been developed for residue determination of eight aliphatic amines simultaneously in drug substances. Different halonitrobenzenes derivatization reagents were systematically compared. As a result, 1‐fluoro‐2‐nitro‐4‐(trifluoromethyl)benzene was selected since the derivatization effectively shifted the absorption wavelength to the visible region (400–450 nm), where most drug substances, impurities and even the derivatization reagent absorb very weakly. Due to the redshift effect, interference was minimized and adequately low limits of quantitation were reached (0.24–0.80 nmol/mL). Moreover, the derivatization reaction was readily carried out in dimethyl sulfoxide at room temperature for 1 h using N ,N‐diisopropylethylamine as catalyst to achieve the highest yield. Without any pre‐treatment, the derivatives were analyzed by high‐performance liquid chromatography with diode array detection. The high stability of the derivatives within 24 h at room temperature (RSD<1.04%) further facilitated the simultaneous preparation and consecutive analysis of quantities of samples. Finally, the proposed method was successfully applied for residue determination of eight aliphatic amines simultaneously in eight drug substance samples. This study could be helpful for the routine analysis and residue control of aliphatic amines in drug substances. 相似文献
48.
《Mathematische Nachrichten》2017,290(5-6):738-755
We introduce some general classes of pseudodifferential operators with symbols admitting exponential type growth at infinity and we prove mapping properties for these operators on Gelfand–Shilov spaces. Moreover, we deduce composition and certain invariance properties of these classes. 相似文献
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基于局域分析的疲劳短裂纹群体演化随机模型 总被引:4,自引:0,他引:4
采用局域裂纹数密度描述金属材料中不同局部区域的疲劳短裂纹群体损伤的发展情况通过考虑在不同局域存在的材料性质的随机涨落及局部损伤对损伤总量发展的影响,建立了局域裂纹数密度演化随机方程对方程数值求解从而模拟了材料的疲劳短裂纹损伤过程结果显示出主裂纹出现的随机性,并讨论了裂纹总数与最大裂纹尺度在统计意义上的演化特征 相似文献