Statistical mixture design investigation of fractionated and total extracts from Erythrina speciosa Andrews leaves

The simplex centroid mixture design for the ethanol, dichloromethane, hexane and acetone solvents has been applied to the extraction of crude mass and the fiber, organic, neutral and basic fractions as well as the fractionation residues of Erythrina speciosa Andrews leaves. Binary and ternary synergic solvent interactions are seen to provide dominant contributions to the extraction of both crude mass and all the fractions. Quadratic and special cubic mixture models precisely predict the extracted quantities of each fraction and the residue as a function of the proportions of the four solvents. Different solvent mixtures are found to be the most efficient extractors for the different fractions: binary dichloromethane‐hexane mixtures for the fiber fraction, ternary ethanol‐dichloromethane‐acetone mixtures for the neutral fraction, binary ethanol‐dichloromethane mixtures for the organic fraction, crude extract and residue values and ternary ethanol‐dichloromethane‐hexane mixtures for the basic fraction. Principal component analysis shows that the ethanol‐dichloromethane mixtures are important for extracting large quantities of the basic and organic fractions as well as of the residue and crude masses.     

基于虚拟仪器的导弹质心定位系统设计与实现

针对传统导弹质心定位设备精度低,操作繁琐等弊端,从弹体质心定位原理出发,合理选取力矩计算参考点,建立质心定位模型;以基于PCI总线的内插式DAQ虚拟仪器测控平台为依托,突出“通用性、精确性、高效性”的设计理念,制定系统总体设计方案,围绕导弹质量测量与质心定位技术展开研究与工程实现;实际应用表明,本系统可拓展应用于多型导弹和大型圆柱形工件的称重与质心定位,满足导弹飞行控制研究和装配工艺要求。     

素GPI-环的幂零多项式

Ｒ是素ＧＰＩ－环,若多项式ｆ（ｘ_１,…,ｘ_d）在Ｒ上是幂零的,则或ｆ（ｘ_１…,ｘ_d）是Ｒ的恒 等式,或Ｒ是有限域上的有限矩阵环     

素GPI-环广义形心扩张的本原性

类似于中心扩张,本文引入了广义形心扩张的概念,且研究了广义形心扩张的本原性。     

神龙一号电子束质心运动测量研究

 在强流直线感应加速器中,电子束质心位置的控制是一项重要技术,要达到较好的控制效果,前提是对电子束质心位置进行准确的测量和定位。针对具有时间分辨的电子束质心位置的测量和确定,介绍了测量实验系统的建立和数据处理两个方面的研究工作。该处理方法在实际应用时能够将电子束质心位置的误差控制在1～2个像素内。用高速分幅相机以10 ns的时间间隔、3 ns的曝光时间获得了神龙一号加速器在漂移段出口处的电子束质心运动情况。结果表明：束的质心主要在半径为0.5 mm的区域内运动,束斑直径dFWHM值分别为8.4,8.8,8.5,9.3和7.6 mm,测量结果可以为束的调控提供准确参数。     

无衍射光束在CCD像点位置提取算法中的应用

重心法是一种高精度的ＣＣＤ像点位置提取算法。但由于数据量大，采样率低，响应速度受到限制，使它在要求实时响应的小型系统中很难得到应用。光束的光衍射是一种很优越的特性，它能在一定的空间内提供高准直的微小光束。利用无衍射光束的这一特性来缩小像点的尺寸，将它和二值化方法结合在一起，可使数据处理量减小到可以满足实时响应的要求。理论、算法分析和实验都证明了这种方法的可行性。     

Synthesis, Crystal Structure and Luminescence Property of [Co(hmz)2(H2O)4]·2H2O

A new mononuclear Co(Ⅱ) complex, [Co(hmz)2(H2O)4]·2H2O, has been synthesized by the reaction of Co(CH3COO)2·4H2O with 1-(4-hydroxyphenyl)-5-mercaptotetrazole (Hhmz). It crystallizes in the monoclinic system, space group P21/n with a = 13.502(5), b = 6.718(3), c = 13.972(6) (A), β = 117.532(4)°, V = 1123.9(8) (A)3, Z = 2, M r = 553.45, F(000) = 570, Dc = 1.635 g/cm3, μ = 1.008 mm-1, the final R = 0.0272 and wR = 0.0684 for 2194 observed reflections (Ⅰ＞ 2σ(Ⅰ)). The Co(Ⅱ) is six-coordinated by two nitrogen atoms from two hmz-1 ligands and four water molecules, forming an octahedral geometry. The intermolecular hydrogen bonding and offset-panel π-π stacking interactions between the adjacent molecules extend the compound into a three- dimensional supramolecular framework. The title compound emits strong blue fluorescent light (λem(max) = 427 nm) at room temperature and is red-shifted compared with free ligand Hhmz (λem(max) = 342 nm).     

Isotropy of 8-dimensional quadratic forms over function fields of quadrics

Let F be a field of characteristic different from 2 and let ø be an anisotropic 8-dimensional quadratic form over F with trivial deter-minant. We study the remaining open cases in the problem of describing the quadratic forms ψ such that ø becomes isotropic over the function field (ψ).     

转动定律实验拓展问题研究

准确地画出了转动系统各物理量间关系与矢量方向;论述了转动惯量实验方程组的建立与求解的完备性;证明了只有传动滑轮质量m0必须非常小时,才会对实验结果影响忽略不计;论证了转动系统平衡条件为满足质心坐标和惯量系数同时为零。