Improving the impact property and heat‐resistance of PLA/PC blends through coupling molecular chains at the interface

The influences of both the molecular structure and the melt viscosity differences between Poly(lactic acid) (PLA) and polycarbonate (PC) on the interpenetration of molecular chains at the interface were investigated by comparing the dynamic mechanical properties and morphologies of the as‐prepared PLA/PC solution‐casting blends with those of their corresponding annealed (180°C, 8 h) samples or PLA/PC melt blends. Additionally, two chain extenders containing epoxy groups (ADR and TGDDM) were used to improve the interfacial strength. Subsequently, the interpenetration of PLA and PC molecular chains at the interface was also surveyed. Finally, the effects of the morphology formed by after adding ADR or TGDDM on the impact property, and heat resistance were discussed. The results showed that there was no interpenetration of molecular chains at the interface in PLA/PC melt blends because of the serious hindrance of the molecular structure and the melt viscosity differences. Although the interfacial strength achieved significant increase after adding ADR or TGDDM, the increase of the interfacial strength should be caused by the connection of ADR or TGDDM molecules with PLA and PC molecules at the interface through chemical bonds rather than the entanglements of PLA and PC molecular chains because of no interpenetration of PLA and PC molecular chains at the interface. Thus, the morphology formed after adding ADR or TGDDM is still the type of complete phase separation, which may be the most suitable morphology for achieving high impact and heat resistance PLA/PC blends because these two properties strongly depend on the crystallinity of PLA phase. Copyright © 2015 John Wiley & Sons, Ltd.     

在封闭结构中水对爆炸冲击波的削波、减压作用

采用数值方法计算了封闭矩形空间中布置在炸药周围的水对爆炸冲击波的削波作用以及对于气室压力的削减作用。计算结果显示 ,在各种不同的载荷密度和水 /药质量比参数条件下 ,冲击波峰值压力和气室压力均得到明显的削减。还计算了一个具有开口的模型隧道中水的削波作用 ,并将计算结果与实验测量数据进行了比较。     

氟化氙(C-A蓝绿激光技术研究进展

 综述了XeF(C-A)激光的产生原理，表面放电光泵浦源的结构，激光器装置， XeF(C-A)激光实验研究以及XeF(C-A)激光理论模拟；介绍了XeF₂浓度的监测，以及表面放电光泵浦源技术研究的最新进展。     

BBO，LBO，KDP晶体光参量啁啾脉冲放大特性的比较研究

 对BBO，LBO，KDP晶体I类非共线匹配下的光参量啁啾脉冲放大的相位匹配、参量范围、增益特性等进行了理论分析，重点对BBO和LBO的光参量啁啾脉冲放大特性进行了比较。结果表明对于以光参量啁啾脉冲放大系统代替800nm中心波长的Ti:sappire再生放大系统，用BBO晶体可获得更宽的增益带宽，而对1 053nm中心波长的种子光用LBO晶体更好。     

关于图的下完美邻域数的上界一些结果

本文主要讨论了图的下完美邻域数 ,并给出了θ(G) =γ(G)的充分必要条件 ,并讨论了一些特殊图类的下完美邻域数的上界 ,特别对于树采用了对所有点分层的方法进行了较细致的讨论 ,给出了紧上界θ(T)≤ [n3] .     

PbTe的高温高压合成

 以高温高压为手段，在4～5GPa压力和700～1 200 K温度条件下，成功地合成出了PbTe。对合成样品进行了X射线测试分析，结果表明，合成的PbTe样品是具有NaCl结构的多晶，而PbTe的取向随着合成压力的升高发生变化。扫描电镜分析结果显示：高压合成的PbTe样品，其晶粒有了明显的取向；电阻率比常压样品低1～2个数量级，并随合成压力的升高而降低；热导率也同时低于常压合成的PbTe样品。以上结果说明，高压合成方法是改善材料性能的重要手段。     

μs级充电时水介质同轴电容击穿实验研究

 研制了水介质同轴电容的实验装置，在此装置上进行了大量的实验。测得μs级充电时，水介质同轴电容分别在正脉冲和负脉冲充电时的击穿电压，负击穿电压的理论值与测量值相差较大，正击穿电压的理论值大于测量值的18%左右，对此实验结果进行了分析。此外，当去离子水的电阻率从13MΩ·cm降到5 MΩ·cm时，水介质同轴电容器的击穿电压基本不变。     

A difference scheme for a parabolic system modelling the thermoelastic contacts of two rods

In this article, we study a sequence of finite difference approximate solutions to a parabolic system, which models two dissimilar rods that each rod is fixed at one end and is free to expand or contact at the other end. A finite difference scheme is derived by the method of reduction of order on nonuniform mesh. The unique solvability, unconditional stability, and convergence of the difference scheme are proved. The convergence order is of order two in both time and space. The convergence of iterative algorithm for the difference scheme are also discussed. A numerical example is presented to demonstrate the theoretical results. © 2006 Wiley Periodicals, Inc. Numer Methods Partial Differential Eq, 2007     

激光大气闪烁的间歇特征

 以小波变换法观察了湍流大气中激光光强起伏的间歇特征, 并用奇性测度进行了定量的描述。根据间歇性参量的周日变化规律发现：激光大气闪烁的间歇性存在于所有的时间和起伏条件下,并且保持稳定,间歇性参量约为0.1,基本不随起伏条件和时间变化。