CoNiZ系列合金的结构和马氏体相变性质

利用X射线衍射研究了CoNiZ(Z=Si,Sb,Sn,Ga等)合金在不同热处理条件下的相组成.当Z元素为Sn,Sb时,材料是完全的B2结构;但Z为Si时,材料变成面心立方的γ相.形成B2还是γ相由电子浓度和原子尺寸效应两种因素共同决定.而CoNiGa的研究结果表明,在合金中除了形成B2结构的同时还容易形成γ相,常表现出两相共存的特性.对材料进行不同方式的热处理可以使合金中两相的含量有所消长,γ相含量的多少对CoNiGa合金的马氏体相变有很大的影响.分析指出,两相共存及其所带来的物性变化是CoNiGa铁磁性形状记忆合金非常有利用价值的物理性质.     

前馈PMD补偿实验中从偏振度椭球获得差分群时延的研究

运用偏振度(DOP)椭球法从实验的有限样点数据中获得了差分群时延和偏振主态方向,这为前馈补偿实验提供了最关键的技术因素.在实验中获得了偏振主态方向和DGD,而且当DGD较小时,从实验所获得的DGD值与理论模拟的变化趋势基本一致.结果表明当DGD较小时,可以用偏振度椭球法从实验上得到正确的DGD和偏振主态方向.     

AN ESTIMATE ON THE DISTRIBUTION AND MOMENTS OF THE LAST EXIT TIME OF AN ELLIPTIC DIFFUSION PROCESS

Let LB be the last exit time from a compact set B of an elliptic diffusion process X. A moderate estimate for the distribution of LB is obtained, and the sufficient and necessary condition for Ex(LBk)<∞is proved.     

动态广义球对称含荷黑洞的统计熵

利用改进了的brickwall膜模型,计算了动态广义球对称含荷黑洞的熵,研究结果表明,对于动态黑洞,将黑洞熵表示为与视界面积成正比时,则比例系数总与动态黑洞的视界速度有关 关键词： 广义球对称黑洞 黑洞熵 brick-wall膜模型 WKB近似     

MOCVD生长的GaN单晶膜透射光谱研究

采用MOCVD技术在Al2O3(0001)衬底上生长了GaN薄膜，使用透射光谱、光致发光光谱和X射线双晶衍射三种技术测试了五类GaN薄膜样品，实验结果表明：GaN薄膜透射谱反映出的GaN质量与X射线双晶衍射测量的结果一致，即透射率越大，半高宽越小，结晶质量越好；而X射线双晶衍射峰半高宽最小的样品，其PL谱的带边峰却很弱，这说明PL谱反映样品的光学性能与X射线双晶衍射获得的结晶质量不存在简单的对应关系，同时还报导了一种特殊工艺生长的高阻GaN样品的RBS／沟道结果。     

Reaction Mechanism Investigation Using Vibrational Mode Analysis for the Multichannel Reaction of CH_3O+CO

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Synthesis for robust synchronization of chaotic systems under output feedback control with multiple random delays

Synchronization under output feedback control with multiple random time delays is studied, using the paradigm in nonlinear physics—Chua’s circuit. Compared with other synchronization control methods, output feedback control with multiple random delay is superior for a realistic synchronization application to secure communications. Sufficient condition for global stability of delay-dependent synchronization is established based on the LMI technique. Numerical simulations fully support the analytical approach, in spite of the random delays.     

Electroless deposition of open-end Cu nanotube arrays

Cu nanotube arrays were fabricated by electroless deposition using porous anodic aluminium oxide membranes as templates. This was accomplished by a four-step procedure, i.e. pore-wall modification, polishing treatment, sensitization-activation and electroless deposition. The as-synthesized Cu nanotubes possess controllable inner diameter and open ends.     

线性流形上矩阵方程BTXB=F的双对称最小二乘解

1引言令R~(n×m)、OR~(n×n)、SR~(n×n)(SR_0~(n×n))分别表示所有n×m阶实矩阵、n阶实正交阵、n阶实对称矩阵(实对称半正定阵)的全体,A~ 表示A的Moore-Penrose广义逆,I_k表示k阶单位矩阵,S_k表示k阶反序单位矩阵。R(A)表示A的列空间,N(A)表示A的零空间,rank(A)表示矩阵A的秩。对A=(a_(ij)),B=(b_(ij))∈R~(n×m),A*B表示A与     

Pd (II)‐catalyzed vinyl addition polymerization of novel functionalized norbornene bearing dimethyl carboxylate groups

Three novel functionalized polynorbornenes (PNB) with pendant dimethyl carboxylate group (carboxylates—acetate, propionate, and butyrate) are synthesized as a vinyl‐type with a palladium (II) catalyst in high yield. The effects of size of substitutents, molar ratio of monomer to catalyst, solvent polarity, reaction time, and temperature on the polymerization of exo‐norbornene dimethyl propionate were systematically investigated. The low molar ratio and temperature, as well as high polarity of solvent, and long reaction time, are favorable for the enhancement of the monomer conversion, especially, the solvent have an obvious effect on the catalyst activity. The resulting poly(cis‐norbornene‐exo‐2,3‐dimethyl carboxylates) (PNB‐dimethyl carboxylates) show good solubility in common organic solvent and high thermal stability up to 360 °C. The glass transition temperature was detected by DMA at 331, 324, and 318 °C for acetate, propionate, and butyrate, respectively. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 3391–3399, 2007