Radiography of a K_α X-ray source generated through ultrahigh picosecond laser–nanostructure target interaction

Laser-driven ultrafast X-ray sources are widely used for diagnostic radiography. However, there is a large divergence of fast electrons when they are generated by an intense short-pulse laser interacting with a foil target.We design a nanowire array target to achieve a more compact point X-ray source. Fast electrons are confined and guided by the nanowire array structure in order to generate a Kαsource with a small spot size. In our work, the smallest measured source size is comparable to the laser spot size, while the conversion efficiency can reach2.4 × 10-4.     

三峡工程中的若干力学问题

简要介绍了三峡水利枢纽工程概况，工程建设中主要技术难点，以及几个主要工程力学问题，包括流体力学、固体力学、二相流及爆破力学等问题．结合三峡工程侧重叙述岩石（体）力学应考虑的新问题．大型岩土工程是庞大的复杂系统，岩石力学涉及众多学科．建议应用系统工程的理论和方法研究岩石（体）力学，使其在国民经济中发挥更大作用，在岩石（体）力学研究中还需针对不同的目标、任务考虑各种非线性问题．因此，岩石（体）力学应与工程问题更紧密地结合．     

Single order soft X-ray diffraction with quasi-random radius pinhole array spectroscopic photon sieves

A novel single order diffraction grating in the soft X-ray region, called quasi-random radius pinhole array spectro- scopic photon sieves （QRSPS）, is proposed in this paper. This new grating is composed of pinholes on a substrate, whose radii are quasi-random, while their centers are regular. Analysis proves that its transmittance function across the grating bar is similar to that of sinusoidal transmission gratings. Simulation results show that the QRSPS can suppress higher-order diffraction effectively. And the QRSPS would still retain its characteristic of single order diffraction when we take the effect of X-ray penetration into account. These properties indicate that the QRSPS can be used in the soft X-ray spectra measurement.     

时间、能量分辨的光电离质谱技术研究气相自由基反应

闪光光解流动管反应器与同步辐射光电离质谱技术两者相结合组成实验平台用于探测气相自由基反应动力学。外触发的脉冲激光光解流动管反应器内的先驱物来产生待反应的自由基;自由基与反应气体发生反应后,由流动管侧壁小孔取样、取样后的混合气体被同步辐射光电离;飞行时间质谱探测光电离产生的离子。同时脉冲信号触发脉冲发生器使其产生一连串的脉冲,间隔40~50μs,此脉冲外触发质谱的采集,连续采集覆盖单次光解反应过程。质谱的时间分辨率为40μs,满足微秒时间内探测反应动力学过程。通过同步辐射光电离反射飞行质谱能直接探测自由基反应产物,并利用光电离效率曲线获得其电离能并区分不同的异构体。实验利用光解产生Cl自由基并与1-丁烯和异丁烯反应,测得反应的加成和消除产物,并获得其加成产物的电离能。     

ICP—AES法顺序测定药液中的钾,钠,钙,镁,铝,铁方法的研究

本文研究了两种药液中钾、钠、钙、镁、铝、铁的测定方法,并讨论了元素间的光谱干扰及非光谱干扰的校正,获得满意结果。其回收率为90-118%,测量精度(RSD%)小于6%。     

金花忍冬中一个新的二聚体环烯醚萜甙的2D NMR研究

从忍冬科药用植物金花忍冬（Lonicera chrysatha）中首次分离得到一 新的二聚体环烯醚萜甙--金花忍冬素（chrysathain）. 采用¹H-¹H COSY、HMQC、HM
BC及NOESY二维谱技术鉴定了此化合物的化学结构及构型，并对其¹H和¹³C NMR的谱峰进行了全归属.     

一层非球形粒子散射的标量辐射传输迭代解的求逆

给出了一层有下垫反射面的非球形粒子散射的标量辐射传输方程一、二阶迭代解,推导了相函数各阶Legendre展开系数与随机小椭球粒子相函数的对应关系,提出了一层随机小椭球粒子介电常数和单位面积粒子数的迭代反演方法.通过两次各方位角上双站散射测量,反演随机小椭球粒子的介电常数和单位面积粒子数.本方法比现有文献的一些反演方法易于实现,可应用于颗粒性复合材料介电与结构特性以及地表背景参数的反演研究 关键词： 辐射传输方程 迭代解 反演 相函数 介电常数     

Antioxidant Activity of Ecdysteroids from Serratula strangulata

One new ecdysteroid,(24R)-24-(2-hydroxyethyl)-20-hydrox-yecdysone(3),as well three known ecdysteroids,has been isolated from Chinese herb serratula strangulata and these compoundsd 1-4 showed effective antioxidant activity on AAPH-induced hemolysis of human RBC and Fe^2 cysteine-induced lipid peroxidation of liver microsome.