Reducibly degradable hydrogels of PNIPAM and PDMAEMA: Synthesis,stimulus‐response and drug release

Reducibly degradable hydrogels of poly(N‐isopropylacrylamide) (PNIPAM) and poly(N,N‐dimethylaminoethyl methacrylate) (PDMAEMA) were synthesized by the combination of reversible addition‐fragmentation chain transfer (RAFT) polymerization and click chemistry. The alkyne‐pending copolymer of PNIPAM or PDMAEMA was obtained through RAFT copolymerization of propargyl acrylate with NIPAM or DMAEMA. Bis‐2‐azidyl‐isobutyrylamide of cystamine (AIBCy) was used as the crosslinking reagent to prepare reducibly degradable hydrogels by click chemistry. The hydrogels exhibited temperature or pH stimulus‐responsive behavior in water, with rapid response, high swelling ratio, and reproducible swelling/shrinkage cycles. The loading and release of ceftriaxone sodium proved the feasibility of the hydrogels as the stimulus‐responsive drug delivery system. Furthermore, the presence of disulfide linkage in AIBCy favored the degradation of hydrogels in the reductive environment. © 2010 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 48: 3604–3612, 2010     

Temperature dependent in situ doping of ALD ZnO

This study on ALD grown ZnO layers is aimed at the systematic study of the effect of incorporation of different Al contents on the properties of the layers. An alternate precursor pulse method was used for layer deposition. Optimal doping was achieved at 210 °C at 2 at% Al content. A relationship between crystalline morphology versus temperature and aluminium incorporation was established.     

四苯骈卟啉锌纯化和脱锌的研究

通过系统研究,改进了四苯骈卟啉锌的纯化和脱锌的方法,发现用浓硫酸脱锌时绿色物质的生成与温度有关. 纯化方法经改进,产率和纯度均有所提高.     

高速光脉冲的测量方法

 综述了目前国际上公认的测量高速光脉冲的几种方法，主要包括电光条纹相机（SC）、快速脉冲取样、二次谐波产生（SHG）、频率分辨光学门（FROG）以及光谱相位干涉直接电场重建（SPIDER）等。详细地阐述和分析了这些方法的原理、特点、适用范围以及它们的研究现状。     

HIRFL高频腔体功率耦合匹配实验研究

 介绍了HIRFL主加速器SSC高频腔体功率馈入耦合匹配系统的研究，实验结果表明，通过改变耦合环角度可更好地实现高频腔体和高频发射机之间的匹配，提高了高频腔体电压和高频发射机的工作效率。     

非齐次线性差分方程的Cm解[英文]

设c0,c1,…,cn均为实的常数，F（x)是个从R到R的C^m映射。本文讨论了非齐次线性差分方程∑i=1ncif(x i)=F(x)的C^m(m≥0）的存在性和唯一性。     

毛细管电泳法测定人发中铝

用毛细管离子分析 (CIA)法 ,采用 10mmol·L- 1咪唑为背景电解质 ,4 0 %甲醇为选择性改性剂 ,在 pH 2 .5、分离电压为 2 5kV、柱温为 2 2℃的电泳条件下 ,采用间接紫外检测 (2 14nm ) ,在5min内测定了人发中铝 ,方法简便、快速、灵敏度高、重现性好、测定成本低     

脉冲软X光辐射三种材料的喷射冲量实验研究

 在强光一号脉冲加速器上进行了国内首次的实验室软X光辐射三种材料的喷射冲量研究。结果表明，在能量为(0.2～0.33)keV、平均脉宽为39ns左右的X光辐射下，对灰漆、白漆和硬铝，在能注量分别为(92～152)J/cm²、(115～136)J/cm²和(163～192)J/cm²时，它们的冲量耦合系数分别为(0.61～0.80)Pa·s/(J·cm^-2)、(0.58～0.97)Pa·s/(J·cm^-2)和(0.61～0.84)Pa·s/(J·cm^-2)。     

中子法测量沥青含量

讨论了沥青混合料中沥青含量的中子测量方法，比较了几种测量结构，给出了最佳测量结构及其测量结果与离心分离法的比较．     

Solitary wave solutions for a general Boussinesq type fluid model

The possible solitary wave solutions for a general Boussinesq (GBQ) type fluid model are studied analytically. After proving the non-Painlevé integrability of the model, the first type of exact explicit travelling solitary wave with a special velocity selection is found by the truncated Painlevé expansion. The general solitary waves with different travelling velocities can be studied by casting the problems to the Newtonian quasi-particles moving in some proper one dimensional potential fields. For some special velocity selections, the solitary waves possess different shapes, say, the left moving solitary waves may possess different shapes and/or amplitudes with those of the right moving solitons. For some other velocities, the solitary waves are completely prohibited. There are three types of GBQ systems (GBQSs) according to the different selections of the model parameters. For the first type of GBQS, both the faster moving and lower moving solitary waves allowed but the solitary waves with“middle” velocities are prohibit. For the second type of GBQS all the slower moving solitary waves are completely prohibit while for the third type of GBQS only the slower moving solitary waves are allowed. Only the solitary waves with the almost unit velocities meet the weak non-linearity conditions.