Studies on the Synthesis of Morphinan Alkaloid： Preparation of the Key Allylic Silyl Ether Precursor

Morphinan alkaloid consisting of many diverse molecules has been attracting much attention of synthetic chemists because of their biologically significant activities and the intriguing structures1. As shown in the common nucleus 1 of these polycyclic frameworks, there is a unique quaternary carbon center with an aryl substituent representing a central synthetic challenge2. In connection with our constant investigations on the quaternary carbon chemistry3, we proposed a general and conceptually…     

一类微分方程亚纯解的增长级

By meas of the Nevanlinna theory of the value distribution of meromorphic functions,this paper discusses the orders of growth of meromorphic solutions of differential equation and proves that the form of the solution is determined if the order are sufficiently large.     

五象限法声源自动跟踪器

介绍由两同心圆组成的等投影面积五象限声－电测量装置的工作原理。当声波与声－电转换器的主要测象限垂直时，其声波在主要测象限内产生的声－电电压最强。根据声－电电压的变化大小来确定声源的方向，实现自动跟踪。     

用毛细管区带电泳法研究水稻种子胚乳贮藏蛋白

水稻品种鉴别目前常采用种子形态分析、蛋白和同工酶的聚丙烯酸胺凝胶电泳分析等方法，其缺点是试剂有毒，分析时间长，且很难区别亲缘关系接近的同母异父杂交水稻种子．毛细管电泳是一种高效分离技术【‘’‘〕，具有快速、微量、自动化等优点．本文采用毛细管区带电泳（CZE）对国产13种水稻种子胚乳贮藏蛋白进行初步研究，探讨了作为品种鉴别模式的实际可操作性，以期能为品种鉴别提供新的有效手段．仪器：BiofocusTM3000型（Bio－RadUSA）毛细管电泳仪，配紫外可见检测器和恒温装置．13种水稻种子中包括两组同母异父杂交种子（每组…     

低杂波波谱的下移和可近性条件

本文利用改进磁面位移计算的射线轨迹Ｃｏｄｅ，研究在射线轨迹的第圈ｎ的下移以及下移量与各等离子体参量的关系。我们发现等离子体密度越高，波的频度越低，ｎ的下移量越大。计算表明：在射线的第一圈ｎ下移量的最大值大致与ｎ＾－ｅ／「ｆ＾１．５ｑ（ｒｃ）」成正比、也与电流、密度的分布和ｎ的初值等有关。     

随机环境中马氏链的状态的性质

定义了随机环境中马氏链的强π-不可约性；给出了一个非正则本质状态不存在的充分条件；得出了在各种不可约性的条件下，状态的各种性质；研究了随机环境中马氏链的各种特性函数的性质．     

Synthesis and Crystal Structure of a Novel 3D Magnesium(II) Coordination Polymer Constructed by Flexible Benzene-1,4-dioxyacetate

1 INTRODUCTION The coordination chemistry of the alkaline-earth metals has remained a largely underdeveloped area[1, 2]to date. Also calcium(II) and magnesium(II) ions are the essentially biological elements and play an im- portant role in DNA and protein syntheses. Although the transition metal carboxylates have been widely in- vestigated[3, 4], the reports on magnesium complexes with carboxylate ligands are very rare[5]. The flexible phenylenedioxydiacetic acids (BDOAH2), especial…     

基于智能化信息处理的建筑工程造价短期预测

提出了一种新的基于智能化信息处理的建筑工程造价短期预测模型.该模型首次利用数据的高阶统计信息,提出了改进独立分量分析技术.通过构建适用于建筑工程造价的属性重构空间,挖掘出表征能力更强的造价独立属性,用于神经网络的学习和训练,从而建立了全新的建筑工程造价短期预测智能模型.该模型通过发挥独立分量分析强大的信号分离能力,增强了神经网络的学习效率,提高了预测精度.实例数据验证了文中所建模型的有效性.     

Characterization of Er3+-doped Na2O-WO3-TeO2 glass for ion-exchanged waveguide amplifiers and lasers

Er3+-doped Na2O-WO3-TeO2 glass consistent with standard ion-exchange technology has been fabricated and characterized. The measured absorption and emission spectra of the glass were analyzed by the JuddOfelt and McCumber theories. The intensity parameters are Ω2 = 7.01 × 10-20 cm2, Ω4 = 1.80 × 10-20 cm2, Ω6 = 1.03 × 10-20 cm2. The maximum emission cross-section is 0.91 × 10-20 cm2 at 1.533 μm, and a broad 1.5-μm emission spectrum of 65-nm full width at half-maximum (FWHM) is demonstrated. Glass transition temperature, crystallization onset temperature, density, refractive index are also reported for reference in the design and modelling of the ion-exchange process.     

Bi2223／Ag带HTS双饼磁体实验

用国产Bi2223／Ag带（西北有色金属研究院提供）设计的中心场3．0T．贮能35kJ的传导冷却高温超导磁体正在建造中．磁体由绕组内径150mm．外径272mm的32个双饼磁体组成．磁体在温度T=20K下．设计临界电流Ic=132A．额定运行电流I=100A.在T=20K附近进行四双饼组合磁体实验，得到磁体Ic=140A，中心场Bcc=1．14T，相应Bi2223／Ag带上最大轴向场Brmax=1．91T．Bi2223／Ag带上最大垂直场Brmax=1．14T．四双饼组合磁体的实验结果预示：35kJ HTS贮能磁体的设计目标能够达到．