激光沉积超导薄膜过程中出射粒子速度的飞行时间谱分析

采用飞行时间谱技术,测量了准分子激光烧蚀沉积高温超导薄膜过程中,由靶面出射粒子的飞行速度。研究了粒子速度与充氧压及其激光能量密度的关系。讨论了高能粒子在薄膜原位低温外延生长中的作用。     

Electro-Magnetic Control of Vortex Shedding Behind a Circular Cylinder

Both open- and closed-loop control algorithms have been developed for suppressing of vortex shedding behind a circular cylinder in an electrically low-conducting fluid. For the open-loop control, the localized Lorentz forces are generated parallel to the cylinder surface, which have the accelerated effect to the fluid. Furthermore, two closed-loop control methods have been derived from the equations of motion capable of determining at all times the intensity of the Lorentz force to control the vortex shedding of a cylinder.     

Simulation of Patterns and Qualitative Analysis of Pattern Rotation in an End-Pumped Nd：YVO4 Laser

We simulate some laser output patterns observed in our previous experiment employing superposition of Laguerre- Gaussian modes. The rotating pattern is qualitatively analysed from the point of contemporary spatial burning hole effect of the lasing crystal.     

猪肉中16种性激素的多残留检测方法

采用安捷仑GC/MS5975N能同时对猪肉中16种性激素残留进行筛选、定量和确证.对5.0g肌肉样品的检出限均在0.25～1.0 μg·kg-1之间.猪肉的平均回收率分别为83.7%～107.9%,平均变异系数为6.8%～19.7%.当添加水平为1.0 μgkg-1时,本方法不同批次猪肉回收率的相对标准偏差为7.7%～21.6%,重复性好.另外,与安捷仑GC/MS5973分析相比,采用GC/MS5975N时,雌三醇衍生物定量离子为m/z 876,比m/z 663峰度强.     

海底掩埋物的目标强度和回声信混比

基于两种流体介质中声散射的修正的Kirchhoff近似,导出计算掩埋物回声的近似公式。应用回声计算的板块元方法和底质的地声模型,能够计算任意形状刚性掩埋物的回声特性。海底沉积层的影响主要反映在声波在底质中传播的衰减。界面的作用主要表现在声波经过两次折射或透射产生的损失。计算结果表明,用常规方式探测掩埋物时回声信混比总是很小, 探测是十分困难的。     

Novel Properties of Photochromic Spirooxazine Nanoparticles

The nanoparticles of a spirooxazine （SPO） and its photomerocyanine （PMC） were prepared through the reprecipitation method. Two distinct features were observed. One is that the decaying lifetime for PMC nanoparticles was 600 times of that for the dispersed molecules, and the other is that the fluorescence intensity of SPO nanoparticles was enhanced by 240 times of that of the dispersed monomer.     

聚(酪氨酸酯对苯二甲酰胺)碳酸酯药物控制释放材料的研究

报道了一类生物可降解聚（酪氨酸酯对苯二甲酰胺）碳酸酯的合成和结构表征，研究了聚合物的性质和体外降解性能，并以５ 氟脲嘧啶和牛血清白蛋为模型，对它们作为药物控制释放材料的性能进行了初步评价．     

网间交联型增韧环氧树脂/蓖麻油聚氨酯互穿网络聚合物的动态力学性能和形态结构

以增韧环氧树脂(TEP)和蓖麻油聚氨酯[PU(CO)]形成的互穿网络聚合物(IPN),两网络间具有一定数量的交联点,在一定组成下,该IPN的tanδ-T曲线半峰宽达100℃,tanδ最大值接近1,阻尼性能良好。形态研究表明,该IPN既有增韧环氧树脂本身的两相结构,又有IPN的两相结构。     

Synthesis and Crystal Structure of Zn(Ⅱ) Complex with 2-Aminopyridine and Acetylacetone

A mixed complex [Zn(C5H6N2)(HL)2] (C5H6N2 = 2-aminopyridine, H2L = acetyl- acetone) has been synthesized and characterized by IR, elemental analysis and X-ray single-crystal diffraction analysis. The crystal belongs to monoclinic, space group P21/c with a = 7.4490(15), b = 8.2650(17), c = 27.615(6)(A),β = 101.69(3)°, V = 1664.9(6)(A)3, Z = 4, Mr = 357.70, Dc = 1.427 g/cm3, F(000) = 744, μ = 1.493 mm-1, R = 0.0309 and wR = 0.0771. The Zn(II) is coordinated by one nitrogen atom from 2-aminopyridine and four oxygen atoms from two acetylacetone anions to furnish a distorted square pyramid geometry. The complex forms a three-dimensional network through intermolecular hydrogen bonds.     

超临界co2中模板法制备氧化铝多孔材料

超临界co2;活性炭;模板;氧化铝;多孔