Rapid synthesis and catalytic performance of α‐Mn2O3 single‐crystal nanowires

Single‐crystal α‐Mn₂O₃ nanowires were prepared via a “self‐sacrificing template” route, simply by calcining the prepared α‐MnO₂ nanowire precursors at 550 °C for 1.5 h. XRD, TEM, SEM and HRTEM characterizations show that the as‐prepared α‐Mn₂O₃ samples are all phase pure and the nanowires have uniform diameters of approximately 15‐30 nm and lengths up to several micrometers. The catalytic performances of the prepared α‐Mn₂O₃ nanowires were studied in the degradation of coking wastewater with H₂O₂ as the oxidant, and the technological conditions were optimized by single‐factor and orthogonal experiments. (© 2011 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)     

插值细分曲线有理参数点的精确求值

本文提出了求值插值细分曲线上任意有理参数的算法.通过构造与细分格式相关的矩阵,m进制分解给定有理数以及特征分解循环节对应算子乘积,计算得到控制顶点权值,实现对称型静态均匀插值细分曲线的求值.本文给出了四点细分和四点Ternary细分曲线的求值实例.算法可以推广到求值其他非多项式细分格式中.     

Water-soluble Porphyrin as Temperature Sensor Based on Fluorescent Enhancement

A novel water-soluble porphyrin[5,10,15,20-tetra（3-ethoxy-4-hydroxy-5-sulfonate）phenyl porphyrin, H2TEHPPS] was designed and synthesized, which could be used as a potential fluorescence sensor to detect temperature changes. The studies were performed in solution phase and the concentration of H2TEHPPS was 2.0×10^-5 mol/L. The optical properties of H2TEHPPS were investigated based on the UV and fluorescence spectra. The results show that the fluorescence intensity of H2TEHPPS is directly proportional to temperature in the range of 293-353 K So H,TEHPPS can be used as a molecular temoerature sensor in biomedical and other fields.     

低密度脆性微流星体撞击航天器防护结构损伤效应研究

采用硅酸盐质弹丸模拟低密度脆性微流星体,开展了航天器典型Whipple 防护结构撞击实验研究,获得了低密度微流星体弹丸损伤模式和损伤规律,实验表明,当弹丸撞击速度在1.1~1.4 km/s,前板损伤模式从花瓣式开裂转变为穿孔,当速度为1.4 km/s 时后板鼓包头上出现裂纹;随着弹丸速度的进一步增加,后板出现剥落现象,并形成花瓣撕裂,当弹丸撞击速度达到1.95 km/s 时后板被击穿,导致防护结构受到破坏.     

纳米FinFET器件的单粒子效应研究(英文)

Fin FET器件比主流CMOS技术表现出更多优势,如快速、高集成度、低功耗、多功能性和强扩展性,基于ISE TCAD,考虑迁移率、量子效应、载流子重组、辐射效应等的影响,建立了一种纳米Fin FET器件SEE的3D仿真模型。分析了工艺掺杂浓度、栅压、粒子能量、寄生电容及技术节点等对单粒子瞬态电流的影响,并探讨了其影响机制。基于此分析,找到了一些潜在的工艺加固技术,如降低源极掺杂浓度、增加漏极和衬底的掺杂浓度、减少粒子能量、降低栅压、优化寄生电容等。     

Fabrication of widely tunable ridge waveguide DBR lasers for WDM-PON

We report the fabrication of widely tunable ridge waveguide distributed Bragg reflector(DBR) lasers with InGaAsP butt-joint as grating material. The shape of the butt–joint interface is found to have significant effect on the properties of the lasers. It is shown that irregular mode jumps during wavelength tuning can be avoided by a V-shaped butt–joint interface. From the fabricated device, 23 channels with 0.8 nm spacing and greater than 35 dB side mode suppression ratios are obtained. The different tuning characteristics of the ridge waveguide and the previously reported buried ridge stripe DBR lasers are discussed. Combined with the wide tuning range and the simple structure, the ridge waveguide DBR lasers are promising for use in wavelength division multiplexing passive optical networks(WDM-PONs).     

Coherent crosstalk in passive microring based Optical Networks-on-Chip

Optical Networks-on-Chip (ONoC) is emerging technology for future optical interconnects used in all optical networks. The electrical interconnects face lot of problems due to their inability to support higher data rates used in the System-on-Chip (SoC) technologies. Integrated optical interconnects based on SoC avoid this bottleneck with their support to higher data rates. In this paper for the first time we have studied and analyzed ONoC at physical level for the system performance based on crosstalk, BER, throughput, system frequency, and other related parameters. The investigation of ONoC performance is carried out for the multistage microring optical crossconnect on SoC for coherent WDM signals. The analysis can be used in the design of ultra-high speed photonic routers for reliable data communication and processing. The results show the dependency of a coherent crosstalk on the system frequency of SoC and also illustrate the reduction in throughput with increase in number of WDM signals due to higher probability of packet transmission. Minimum 2 dB signal to noise ratio can be obtained when crosstalk is ?25 dB with 60 wavelengths for probability of packet transmission is 0.5.     

边坡变形的分布式光纤监测模拟试验研究

布里渊散射光时域反射测量技术(BOTDR)作为一项新型光电传感监测技术,因其具有良好的抗干扰、长距离、可植入性和分布式监测的特点而被广泛应用于结构工程健康监测中。而直接将光纤布设在土体中则存在变形协调性差、易折断及空间定位难等问题。本次研究通过室内小比例尺模型试验,分别将光纤植入土工布和土工格栅等柔性复合材料中并一起铺设在边坡模型不同深度处,利用BOTDR监测边坡在外荷作用下的变形特征。试验结果表明,布设在土工格栅中的光纤稳定性最好; 土工布中的光纤变形协调性和敏感性优于土工格栅; 通过合理布置光纤能够对异常应变进行较为准确的识别和定位。试验初步验证了该方法应用于土质边坡变形监测的可行性。     

关于二维光滑线性方程无解的注记

Abstract. A smooth linear complex partial differential equation in two variables which is without solutions is found.     

1-(2-萘基)-3-甲基-5-吡唑啉酮衍生试剂的制备及其在高效液相色谱-质谱法测定糖类化合物中的应用

以1-(2-萘基)-3-甲基-5-吡唑啉酮(NMP)作为柱前衍生试剂,建立了简单、灵敏的糖类组分的反相高效液相色谱测定方法。NMP与糖在氨为催化剂的条件下,于70 ℃下反应可获得稳定的衍生产物。在Hypersil ODS 2反相色谱柱上,实现了8种单糖的基线分离。衍生物线性相关系数均大于0.9985,检出限为0.58～1.1 pmol。利用柱后在线串联质谱的电喷雾电离正离子模式监测,获得了各组分的质谱定性及裂解规律,特别是m/z 473的特征碎片离子可作为单糖NMP衍生物的判定依据。与1-苯基-3-甲基-5-吡唑啉酮(PMP)相比,NMP对糖的衍生化具有灵敏、简单、质谱裂解规律性强、重现性好等优点。该方法用于测定油菜花粉多糖中的单糖组成,结果令人满意。