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The title compound2-p-methyloxyphenyl-3a-(2-phenyl-1,2,3-triazole-4-yl)-3,4- dihydro-1,2,4-oxa-diazolo[4,5-d][1,5] benzothiazepine (C31H25N5O2S, Mr = 531.63) has been syn- thesized and its structure was determined by single-crystal X-ray diffraction. The crystal belongs to triclinic, space group P1 with a = 10.888(2), b = 15.115(3), c = 16.702(3), α = 99.90(3), β = 95.21(3), γ = 100.41(3)o, V = 2642.1(9) nm3, Dc = 1.336 g/cm3, Z = 4, F(000) = 1112, μ = 0.162 mm-1 ,λ(MoKα) = 0.071073 nm, R = 0.0357 and wR = 0.1126 for 10620 observed reflections with I > 2σ(I). X-ray analysis reveals that the molecular backbone consists of a tricyclic system with the central seven- membered ring in a twisted boat-like conformation. 相似文献
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以钛酸甲丁酯和乙酸钡为主要原料,以乙二醇独甲醚为溶剂,采用溶胶凝胶法在(100)低阻硅片上制备了BaTiO3薄膜电容,用XRD分析了该薄膜的结构,发现薄膜在硅片上取向生长,同时又对薄膜的介电性质进行研究,结果表明,薄膜的介电特性在高频范围内随频率的变化比较稳定,并讨论了晶化温度对薄电容的影响。 相似文献
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合成得到钯与苯基羧酸和1,2-二(二苯膦)乙烷配位的四种混配配合物,确定其化学组成为Pd(PCA)2(dppe).用元素分析、红外、紫外和荧光光谱、摩尔电导、质子核磁共振和热重分析等手段对配合物进行了性质表征. 相似文献
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合成得到钯与苯基羧酸和1,2-二9二苯磷)乙烷配位的四种混配配合物,确定其化学组成为Pd(PCA)2(dppe)。用元素分析,红外、紫外和荧光光谱、摩尔电导、质子核磁共振和热重分析等手段对配合物进行了性质表征。 相似文献
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2012年各省市的高考卷中都注重了对抛物线方程与性质的考查,尤其是对过抛物线焦点的弦性质的考查.笔者在研究这类试题中发现除了"方程法"之外,"几何法"也是行之有效的方法.例(2012年安徽卷理科第9题)过抛物线y2=4x的焦点F的直线l交该抛物线于A、B两点, 相似文献
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The complex {[Co(4,4′-bpy)(H2O)4](Fum)·4H2O}n(where 4,4′-bpy = 4,4′-bipyridine and Fum = fumarate) was synthesized and characterized by X-ray diffraction. The complex consists of one-dimensional chains containing cobalt(Ⅱ) ions bridged by 4,4′-bpy molecules. The six-coordination of Co2+ is achieved by means of four water molecules. The fumarate is not coordinated to cobalt ion while it forms hydrogen bonds with coordinated and non-coordinated water molecules and extends the structure into three-dimensional hydrogen bonding network. CCDC: 190488. 相似文献