Experimental Investigation of Strain Rate Dependence of Nanocrystalline Pt Films

A new microscale uniaxial tension experimental method was developed to investigate the strain rate dependent mechanical behavior of freestanding metallic thin films for MEMS. The method allows for highly repeatable mechanical testing of thin films for over eight orders of magnitude of strain rate. Its repeatability stems from the direct and full-field displacement measurements obtained from optical images with at least 25 nm displacement resolution. The method is demonstrated with micron-scale, 400-nm thick, freestanding nanocrystalline Pt specimens, with 25 nm grain size. The experiments were conducted in situ under an optical microscope, equipped with a digital high-speed camera, in the nominal strain rate range 10⁻⁶–10¹ s⁻¹. Full field displacements were computed by digital image correlation using a random speckle pattern generated onto the freestanding specimens. The elastic modulus of Pt, E = 182 ± 8 GPa, derived from uniaxial stress vs. strain curves, was independent of strain rate, while its Poisson’s ratio was v = 0.41 ± 0.01. Although the nanocrystalline Pt films had the elastic properties of bulk Pt, their inelastic property values were much higher than bulk and were rate-sensitive over the range of loading rates. For example, the elastic limit increased by more than 110% with increasing strain rate, and was 2–5 times higher than bulk Pt reaching 1.37 GPa at 10¹ s⁻¹.     

Bulge Testing Transparent Thin Films with Moiré Deflectometry

The problem that is addressed here is the measurement of the mechanical properties of very thin, transparent films using bulge tests. All existing techniques make use of reflection from the film surface, but they can be difficult or impossible to apply to very thin, transparent films. Consequently, a novel approach based on the formation of a lens structure and using transmitted light is developed. In this technique, the focal length of the lens structure formed by the bulged film and the pressurizing medium is determined by moiré deflectometry with a corrected governing equation. The resulting curvature of the bulge film is used in the stress analysis of the bulge-test. By combining circular and rectangular configurations, the Young’s modulus and Poisson’s ratio of a 3 μm PET film were 4.65 ± 0.11 GPa and 0.34 ± 0.01, respectively. Consistent residual stresses were obtained from both configurations.     

Bending analysis of thin functionally graded plates using generalized differential quadrature method

In this paper, the differential quadrature (DQ) method is presented for easy and effective analysis of isotropic functionally graded (FG) and functionally graded coated (FGC) thin plates with constant Poisson’s ratio and varying Young’s modulus in the thickness direction. The bending of FG and FGC plates under transverse loading has been studied using the polynomial differential quadrature (PDQ) and the harmonic differential quadrature (HDQ) methods. A three-dimensional elasticity solution for a moderately thick FG plate with exponential Young’s modulus is used as the benchmark. Two examples, including a thin FG rectangular plate and a thin FGC rectangular plate with sigmoidal Young’s modulus, are investigated. The numerical results of PDQ and HDQ methods reveal good agreement with other solutions. Also, it is shown that the formulations for thin FG plates and homogeneous plates are similar, except that the plane strain components of the middle surface in FG plates are not zero.     

A Methodology for Obtaining Material Properties of Polymeric Foam at Elevated Temperatures

A new methodology to characterise the elastic properties of polymeric foam core materials at elevated temperatures is proposed. The focus is to determine reliable values of the tensile and compressive moduli and Poisson’s ratio based on strain data obtained using digital image correlation (DIC). In the paper a detailed coverage of the source of uncertainties in the experimental procedure is provided. The uncertainties include those associated with the load introduction, the measurement and the data processing. The design of the specimens and loading jigs are developed and assessed in terms of the introduction of uniform strain. It is shown that due to the mismatch in stiffness between the jig material and the foam the introduction of a uniform strain through the cross section of the specimens is difficult to obtain. A means for correcting for the non-uniform strain across the specimen cross section is developed. To validate the methodology, tests are firstly conducted at room temperature on Divinycell PVC H100 foam. It is shown that the material is highly anisotropic with a stiffness of 50% less in the plane of the foam sheet compared to the through-thickness direction. It is also shown that because of the compliance of the foam, jig misalignment causes large errors in the measurement, and a means for correcting for this is defined. Tests are then conducted in a temperature controlled chamber at elevated temperatures ranging from 20°C to 90°C. A nonlinear reduction in Young’s modulus is obtained with significant degradation occurring after 70°C. The Poisson’s ratio remains fairly stable at different temperatures. A strong theme in the paper is the accuracy and precision of the DIC data and the factors which introduce scatter in the data, along with the uncertainties that this introduces. Particular attention is paid to the affect of the correlation parameters on the derived strain data.     

Comparison between Berkovich,Vickers and conical indentation tests: A three-dimensional numerical simulation study

Three-dimensional numerical simulations of Berkovich, Vickers and conical indenter hardness tests were carried out to investigate the influence of indenter geometry on indentation test results of bulk and composite film/substrate materials. The strain distributions obtained from the three indenters tested were studied, in order to clarify the differences in the load–indentation depth curves and hardness values of both types of materials. For bulk materials, the differentiation between the results obtained with the three indenters is material sensitive. The indenter geometry shape factor, β, for evaluating Young’s modulus for each indenter, was also estimated. Depending on the indenter geometry, distinct mechanical behaviours are observed for composite materials, which are related to the size of the indentation region in the film. The indentation depth at which the substrate starts to deform plastically is sensitive to indenter geometry.     

SIZE EFFECT AND GEOMETRICAL EFFECT OF SOLIDS IN MICRO—INDENTATION TEST

Micro-indentation tests at scales of the order of sub-micron show that the measured hardness increases strongly with decreasing indent depth or indent size,which is frequently referred to as the size effect.At the same time,at micron or sub-micron scale,another effect,which is referred to as the geometrical size effects such as crystal grain size effect,thin flim thickness effect,etc.,also influences the measured material hardness.However,the trends are at odds with the size-independence implied by the conventional elastic-plastic theory.In the present research,the strain gradient plasticity theory(Fleck and Hutchinson)is used to model the composition effects(size effect and geometrical effect) for polycrystal material and metal thin film/ceramic substrate systems when materials undergo micro-indenting.The phenomena of the “pile-up“ and “sink-in“ apeared in the indentation test for the polycrystal materials are also discussed.Meanwhile,the micro-indentation experiments for the polycrystal Al and for the Ti/Si3N4 thin film/substrate system are carried out.By comparing the theoretical predictions with experimental measuremtns.the values and the variation trends of the micro-scale parameter included in the strain gradient plasticity theory are predicted.     

On Poisson’s Ratio in Linearly Viscoelastic Solids

Poisson’s ratio in viscoelastic solids is in general a time dependent (in the time domain) or a complex frequency dependent quantity (in the frequency domain). We show that the viscoelastic Poisson’s ratio has a different time dependence depending on the test modality chosen; interrelations are developed between Poisson’s ratios in creep and relaxation. The difference, for a moderate degree of viscoelasticity, is minor. Correspondence principles are derived for the Poisson’s ratio in transient and dynamic contexts. The viscoelastic Poisson’s ratio need not increase with time, and it need not be monotonic with time. Examples are given of material microstructures which give rise to designed time dependent Poisson’s ratios.     

Planar Strain Measurements on Wood Specimens

Wood specimens have been tested for compressive loading in the longitudinal direction. Planar deformation was recorded by means of video extensometry on the specimen surfaces. A post processing routine was developed to calculate stress and strain values from the sampled data. The routine made use of mathematical framework used in the finite element method. Material parameters were detected by means of an optimization algorithm, and the determined linear elastic parameters were in general found to be in good agreement with values given in literature. The utilized method offers simultaneous average values for active, passive and shear strains from the measured area. Moduli of elasticity, Poisson’s ratios and shear deformation can thus be evaluated. In addition, the variation of the three strain components over the area is measured. The results can therefore be used for quantification of material inhomogeneity and are further suitable for direct comparison with numerically computed strains comprising non-uniform strain fields. Since video extensometry does not require any physical contact with the specimen, measurements can be undertaken until failure. The present method offers thus an efficient and relatively accurate way to measure and evaluate the material characteristics of anisotropic and inhomogeneous materials like wood.     

Fourier series based FE analysis of a disc under prescribed displacements–elastic stress study

This paper examines the numerical displacements and stresses developed around a disc under horizontal prescribed displacements and at the interface separating it from the surrounding elastic soil. Since the geometry of the problem exhibits axial symmetry and the loading is non-axisymmetric, the semi-analytical FE approach is used as it proves to be efficient and economical. First, both analytical and numerical expressions for soil reaction are established and compared. Results of comparison show a very good agreement. Then, for different values of the soil Poisson’s ratio, normal radial stresses, orthoradial stresses and shear stresses distributions along radial distance reaching 20r _d (r _d is the disc radius) are presented for a disc that has either perfectly smooth or perfectly rough interfaces with the elastic medium. The paper finishes by showing the effect of the soil Poisson’s ratio as well as the relative soil/interface stiffness on the stresses developed at the interface locations.     

ASYMPTOTIC ANALYSIS OF MODE Ⅱ STATIONARY GROWTHCRACK ON ELASTIC-ELASTIC POWER LAWCREEPING BIMATERIAL INTERFACE

A mechanical model was established for mode Ⅱ interfacial crack static growingalong an elastic-elastic power law creeping bimaterial interface. For two kinds of boundaryconditions on crack faces, traction free and frictional contact, asymptotic solutions of thestress and strain near tip-crack were given. Results derived indicate that the stress andstrain have the same singularity, there is not the oscillatory singularity in the field; thecreep power-hardening index n and the ratio of Young‘s module notably influence the crack-tip field in region of elastic power law creeping material and n only influences distribution ofstresses and strains in region of elastic material. When n is bigger, the creepingdeformation is dominant and stress fields become steady, which does not change with n.Poisson‘s ratio does not affect the distributing of the crack-tip field.     

Flow of electrolytes in a porous medium

A two-scale model of ion transfer in a porous medium is obtained for one-dimensional horizontal flows under the action of a pressure gradient and an external electric field by the method of homogenization. Steady equations of electroosmotic flows in flat horizontal nano-sized slits separated by thin dielectric partitions are averaged over a small-scale variable. The resultant macroequations include Poisson’s equation for the vertical component of the electric field and Onsager’s relations between flows and forces. The total horizontal flow rate of the fluid is found to depend linearly on the pressure gradient and external electric field, and the coefficients in this linear relation are calculated with the use of microequations. __________ Translated from Prikladnaya Mekhanika i Tekhnicheskaya Fizika, Vol. 49, No. 4, pp. 162–173, July–August, 2008.     

Modelling of the interface between a thin film and a substrate within a strain gradient plasticity framework

Interfaces play an important role for the plastic deformation at the micron scale. In this paper, two types of interface models for isotropic materials are developed and applied in a thin film analysis. The first type, which can also be motivated from dislocation theory, assumes that the plastic work at the interface is stored as a surface energy that is linear in plastic strain. In the second model, the plastic work is completely dissipated and there is no build-up of a surface energy. Both formulations introduce one length scale parameter for the bulk material and one for the interface, which together control the film behaviour. It is demonstrated that the two interface models give equivalent results for a monotonous, increasing load. The combined influence of bulk and interface is numerically studied and it is shown that size effects are obtained, which are controlled by the length scale parameters of bulk and interface.     

Dynamic stress intensity factor of a crack perpendicular to the weak-discontinuous interface in a nonhomogeneous coating–substrate structure

A mechanical model was established for the antiplane dynamic fracture problem of a functionally graded coating–substrate structure with a coating crack perpendicular to the weak-discontinuous interface. The problem was reduced to a Cauchy singular integral equation by the methods of Laplace and Fourier integral transforms. Erdogan’s collocation method and the Laplace numerical inversion proposed by Miller and Guy were used to calculate the dynamic stress intensity factors. Three conclusions were drawn through parametric studies: (a) unlike the conclusion drawn for an interfacial crack, reducing the weak discontinuity of the interface will not necessarily decrease the dynamic stress intensity factor (DSIF) of the coating crack perpendicular to the interface; (b) increasing the stiffness of the substrate when that of the coating is fixed, or decreasing the stiffness of coating when that of the substrate is fixed, will be beneficial for the reduction of the DSIF of a coating crack perpendicular to the interface; and (c) the free surface has a greater influence on the DSIF than the interface does, and the effect of the interface on the DSIF is greater than that of the material stiffness in the crack-tip region.     

Subcritical crack growth in an aging plate with variable elastic modulus

The paper addresses subcritical growth of a crack in a thin isotropic plate made of an aging viscoelastic material with time-dependent elastic modulus. The behavior of the material is described by Arutyunyan’s creep theory. To simulate fracture, a modified Leonov–Panasyuk–Dugdale model and a critical crack opening displacement criterion are used. An equation describing the subcritical growth of the crack is derived assuming that Poisson’s ratio is constant. As an example, the critical loads are determined, and curves of subcritical crack growth are plotted for a specific material. The results are compared with the case of constant elastic modulus     

A Two-Scale Model for Coupled Electro-Chemo-Mechanical Phenomena and Onsager’s Reciprocity Relations in Expansive Clays: II Computational Validation

In Part I Moyne and Murad [Transport in Porous Media 62, (2006), 333–380] a two-scale model of coupled electro-chemo-mechanical phenomena in swelling porous media was derived by a formal asymptotic homogenization analysis. The microscopic portrait of the model consists of a two-phase system composed of an electrolyte solution and colloidal clay particles. The movement of the liquid at the microscale is ruled by the modified Stokes problem; the advection, diffusion and electro-migration of monovalent ions Na⁺ and Cl⁻ are governed by the Nernst–Planck equations and the local electric potential distribution is dictated by the Poisson problem. The microscopic governing equations in the fluid domain are coupled with the elasticity problem for the clay particles through boundary conditions on the solid–fluid interface. The up-scaling procedure led to a macroscopic model based on Onsager’s reciprocity relations coupled with a modified form of Terzaghi’s effective stress principle including an additional swelling stress component. A notable consequence of the two-scale framework are the new closure problems derived for the macroscopic electro-chemo-mechanical parameters. Such local representation bridge the gap between the macroscopic Thermodynamics of Irreversible Processes and microscopic Electro-Hydrodynamics by establishing a direct correlation between the magnitude of the effective properties and the electrical double layer potential, whose local distribution is governed by a microscale Poisson–Boltzmann equation. The purpose of this paper is to validate computationally the two-scale model and to introduce new concepts inherent to the problem considering a particular form of microstructure wherein the clay fabric is composed of parallel particles of face-to-face contact. By discretizing the local Poisson–Boltzmann equation and solving numerically the closure problems, the constitutive behavior of the diffusion coefficients of cations and anions, chemico-osmotic and electro-osmotic conductivities in Darcy’s law, Onsager’s parameters, swelling pressure, electro-chemical compressibility, surface tension, primary/secondary electroviscous effects and the reflection coefficient are computed for a range particle distances and sat concentrations.     

Evaluation of the Material Properties of an OFHC Copper Film at High Strain Rates Using a Micro-Testing Machine

The material properties of an oxygen-free high thermal conductivity (OFHC) film with a thickness of 0.1 mm were evaluated at strain rates ranging from 10⁻³/s to 10³/s using a high-speed material micro-testing machine (HSMMTM). The high strain-rate material properties of thin films are important especially for an evaluation of the structural reliability of micro-formed parts and MEMS products. The high strain-rate material testing methods of thin films, however, have yet to be established to the point that the testing methods of larger specimens for electronics, auto-body, train, ship, and ocean structures are. For evaluation, a new type of HSMMTM was developed to conduct high-speed tensile tests of thin films. This machine is capable of testing at a sufficiently high tensile speed with an electromagnetic actuator, a novel gripping mechanism, and an accurate load measurement system. The OFHC copper film shows high strain-rate sensitivity in terms of the flow stress, fracture elongation, and strain hardening. These measures increase as the tensile strain rate increases. The rate-dependent material properties of an OFHC copper film are also compared with those of a bulk OFHC copper sheet with a thickness of 1 mm. The flow stress of an OFHC copper film is relatively low compared to that of a bulk OFHC copper sheet in the entire range of strain rates, while the fracture elongation of an OFHC copper film is much larger than that of a bulk OFHC copper sheet. A quantitative comparison would provide material data at high strain rates for the design and analysis of micro-appliances and different types of micro-equipment.     

Stress and Moisture Effects on Thin Film Buckling Delamination

Deposition processes control the properties of thin films; they can also introduce high residual stresses, which can be relieved by delamination and fracture. Tungsten films with high 1–2 GPa compressive residual stresses were sputter deposited on top of thin (below 100 nm) copper and diamond-like carbon (DLC) films. Highly stressed films store large amounts of strain energy. When the strain energy release rate exceeds the films' interfacial toughness, delamination occurs. Compressive residual stresses cause film buckling and debonding, forming open channels. Profiles of the buckling delaminations were used to calculate the films' interfacial toughness and then were compared to the adhesion results obtained from the superlayer indentation test. Tests were conducted in both dry and wet environments and a significant drop in film adhesion, up to 100 times was noticed due to the presence of moisture at the film/substrate interface.     

Full-Field Strain Measurement and Identification of Composites Moduli at High Strain Rate with the Virtual Fields Method

The present paper deals with full-field strain measurement on glass/epoxy composite tensile specimens submitted to high strain rate loading through a split Hopkinson pressure bar (SHPB) device and with the identification of their mechanical properties. First, the adopted methodology is presented: the device, including an Ultra-High Speed camera, and the experimental procedure to obtain relevant displacement maps are described. The different full-field results including displacement, strain and acceleration maps for two mechanical tests are then addressed. The last part of the paper deals with an original procedure to identify stiffnesses on this dynamic case only using the actual strain and acceleration maps (without the applied force) by using the Virtual Fields Method. The results provide very promising values of Young’s modulus and Poisson’s ratio on a quasi-isotropic glass-epoxy laminate. The load reconstructed from the moduli and strains compares favourably with that from the readings.     

Time-dependent thermoelastic creep analysis of rotating disk made of Al–SiC composite

Time-dependent creep stress redistribution analysis of rotating disk made of Al–SiC composite is investigated using Mendelson’s method of successive elastic solution. All mechanical and thermal properties except Poisson’s ratio are radial dependent based on volume fraction percent of SiC reinforcement. The material creep behavior is described by Sherby’s constitutive model using Pandey’s experimental results on Al–SiC composite. Loading is an inertia body force due to rotation and a distributed temperature field due to steady-state heat conduction from inner to outer surface of the disk. Using equations of equilibrium, stress strain, and strain displacement, a differential equation, containing creep strains, for displacement is obtained. History of stresses and deformations are calculated using method of successive elastic solution. It is concluded that the uniform distribution of SiC reinforcement does not considerably influence on stresses. However, the minimum and most uniform distribution of circumferential and effective thermoelastic stresses belongs to composite disk of aluminum with 0% SiC at inner surface and 40% SiC at outer surface. It has also been found that the stresses, displacement, and creep strains are changing with time at a decreasing rate so that after almost 50 years the solution approaches the steady-state condition.     

Influence of elastic material compressibility on parameters of an expanding spherical stress wave

We investigated the influence of elastic material compressibility on parameters of an expanding spherical stress wave. The material compressibility is represented by Poisson’s ratio, ν, in this paper. The stress wave is generated by a pressure produced inside a spherical cavity surrounded by the isotropic elastic material. The analytical closed form formulae determining the dynamic state of the mechanical parameters (displacement, particle velocity, strains, stresses, and material density) in the material have been derived. These formulae were obtained for surge pressure p(t) = p ₀ = const inside the cavity. From analysis of these formulae, it is shown that the Poisson’s ratio substantially influences the course of material parameters in space and time. All parameters intensively decrease in space together with an increase of the Lagrangian coordinate, r. On the contrary, these parameters oscillate versus time around their static values. These oscillations decay in the course of time. We can mark out two ranges of parameter ν values in which vibrations of the parameters are “damped” at a different rate. Thus, Poisson’s ratio in the range below about 0.4 causes intense decay of parameter oscillations. On the other hand in the range 0.4 < ν < 0.5, i.e. in quasi-incompressible materials, the “damping” of parameter vibrations is very low. In the limiting case when ν = 0.5, i.e. in the incompressible material, “damping” vanishes, and the parameters harmonically oscillate around their static values. The abnormal behaviour of the material occurs in the range 0.4 < ν < 0.5. In this case, an insignificant increase of Poisson’s ratio causes a considerable increase of the parameter vibration amplitude and decrease of vibration “damping”.