Brittle fracture of precompressed steel as affected by hydrostatic pressure,temperature and strain concentration

Highly precompressed 1020 HR steel, 0.65 prestrain at 400°F (204°C), tested in nominally uniform tension at ?80°F (?62°C) fractures at about 110,000 psi (760 MN/m²) with less than 0.02 plastic strain. Yet the addition of a hydrostatic pressure of less than 7000 psi (48 MN/m²) converts this visually brittle fracture to a ductile one with appreciable necking. The explanation of this surprising experimental result is shown to follow directly and simply from the combination of a tensile stress criterion of fracture, strain concentration and the low tangent modulus of the stress-strain curve in tension beyond the Bauschinger transition region of a few percent of plastic strain. Temperature dependence and strain-rate dependence of brittle fracture similarly are predictable in an almost trivial manner from the appropriate stress-strain curves for different amounts of precompression. So also is the amazingly high ductility or fracture toughness of the most complex of perforated or notched statically loaded structures of mild steel in an undamaged or fully annealed state.     

Thermal stress measurement of quartz oscillator module packaging

The thermal stress of the quartz oscillator module packaging is investigated using digital-image correlation method (DICM), and the experimental results are given. Under the quartz oscillator module packaging, the quartz oscillator and the Fe−Sn−Cu alloy frame are joined together with the electroconductive adhesive (PI), and the electroconductive adhesive needs to be cured twice at 150°C and 275°C respectively. As the quartz oscillator and the Fe−Sn−Cu alloy frame have a distinct difference in both thermal expansion coefficients and mechanical properties and in process of packaging temperature rises or drops, the thermal stress is yielded easily. While temperature drops, the normal stress at the quartz oscillator edge is a tensile stress, which can make the quartz oscillator fracture. Project supported by the Natural Science Foundation of Tianjin (013605211).     

金属材料脆性断裂机理的实验研究

材料的脆性断裂有许多准则和模型,但对脆断机理和变化规律缺乏合理的描述,给工程应用带来不便。本文对典型脆性材料球墨铸铁、灰铸铁分别进行了拉扭双轴断裂实验和常规拉伸、扭转破坏实验;对韧性金属材料合金钢进行了单轴拉伸颈缩破坏实验。通过上述实验分析了脆性材料和韧性材料发生脆性断裂的机理特征并选择应力三维度作为应力状态参数描述危险点的应力状态,同时考察了脆性材料和韧性材料发生脆性断裂的主导因素。结果表明:韧性材料45#钢和14CrNiMoV合金钢在颈缩断面心部应力三维度值较大时发生脆性拉断,而在颈缩断面边缘处应力三维度值较小时发生剪断;脆性材料球墨铸铁在应力三维度值为0.0～0.33之间变化时均发生脆性断裂;灰铸铁在应力三维度值大于0.0时发生脆性拉断,而在应力三维度值小于0.0时发生剪断。因此可以认为,材料的细观组织结构和危险点应力状态是影响断裂机理及变化规律的主要因素。对于同种材料,随着应力三维度代数值从小向大变化材料的断裂机制由塑性剪切断裂逐渐转变为脆性断裂。本文通过对几种材料的脆性断裂危险点和断裂方向的研究给出了脆断宏观破坏条件。     

Numerical prediction of fracture in the Taylor test

A flat-nosed cylinder moving at a sufficiently high impact velocity in the classical Taylor test will always fracture. In this paper, fracture phenomena and fracture mechanisms in the Taylor test are investigated numerically based on a recently developed ductile fracture locus with the cut-off value for the negative stress triaxiality at −1/3. The impact velocity of the projectile ranges from 240 m/s to 600 m/s. The lower velocity is applied to a less ductile 2024-T351 aluminum alloy cylinder while the higher velocity is introduced for more ductile Weldox 460 E steel. Three distinct fracture modes are recreated numerically: the confined fracture inside the cylinder, the shear cracking on the lateral surface, and the petalling, all of which are consistent with experimental results presented in the open literature. It is found that a more ductile cylinder tends to fail by petalling while a less ductile one by shear cracking. Confined fracture is a common failure mode for both materials, which occurs in a wide range of the impact velocity. The ductile fracture criterion with the cut-off value predicts realistic fracture patterns for short cylinders deforming predominantly under compression.     

Molecular dynamics study of deformation and fracture of Bi-segregated copper bicrystals

The microprocesses of deformation and fracture of Bi-segregated copper bicrystals Σ33 ( ) 58.99°, Σ11 ( ) 50.48° and Σ9 ( ) 38.94° have been simulated by molecular dynamics in order to study the relationship between the grain boundary embrittlement (GBE) and grain boundary (GB) structure. It is shown that GBE is related to the segregated concentration and distribution of Bi atoms, while Bi segregation is related to the GB structure. Due to their different structures, the bicrystals Σ33, Σ11 and Σ9 show an increasing propensity for Bi segregated concentration. So under the action of external force, Σ33, Σ11 and Σ9 show transgranular ductile, intergranular tearing and intergranular brittle fracture modes, respectively. The subject supported by the Chinese Academy of Sciences and National Natural Science Foundation of China     

An experimental study of dynamic tensile properties of glass fiber at low-temperatures

Tensile impact experiments of EC8.0−24×7 glass fiber bundles at different low temperaturesT(14°C, −40°C and −10°C) and strain rates ɛ were carried out, and complete stress-strain curves were obtained. Within the range of the experiment temperatures and strain rates, it is found that the initial modulusE, the ultimate strength σ_max and the unstable strain ɛ _b of the glass fiber bundles all increase with ɛ at an identicalT. At an identical ɛ, with the decrease ofT, E and σ_max increase; but ɛ _b increases when 10°C>T>−40°C and decreases when −40°C>T>−100°C. The strain-rate- and temperature-dependent bimodal Weibull statistical constitutive theory was adopted for the statistical analysis of the experimental results, and the Weibull parameters of single fiber were obtained. The results show that the bimodal Weibull distribution function is suitable to represent the strength distribution of the glass fiber at low temperature and different strain rates. The differences in the mechanical properties between EC8.0−24×7 and EC5.5−12 ×14 glass fiber bundles were also discussed. Project supported by the National Natural Science Foundation of China (No. 19772058).     

A crystallographic model for the orientation dependence of low cyclic fatigue property of a nickel-base single crystal superalloy

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Failure resistance of intermetallic matrix reinforced by wires

Composite materials with brittle matrices such as ceramics and intermetallic compounds have gained increased importance in application. Ceramics and intermetallic compounds possess unique heat-resistance at high temperatures. They are, however, vulnerable to brittle fracture. This problem can be overcome by reinforcing the intermetallic compounds with wires. NiAl-tungsten composite wire was manufactured by hot diffusion welding of alternate layers of the matrix and wires. These specimens were subjected to a three-point bending in the temperature range from 20° to 1000°C. Temperature dependence of the bending strength exhibited brittle to ductile transition behavior. At room temperature, unstable failure by bending is terminated in a stable fashion. Brittle fracture of the matrix and wire were observed. For text temperatures of 300°, 500° and 700°C, subcritical crack growth occurred where the matrix and wire showed brittle and ductile fracture, respectively. A pronounced necking of the specimen was observed as the temperature is increased. Substantial plastic deformation occurred when the test is performed at 1000°C. The critical stress intensity factor K_1c and specific work of fracture were measured and found to be two to three times larger than the intermetallic compounds without wire reinforcement.     

Random-fuzzy model for the ductile/brittle transition

IntroductionTheductile brittletransition (DBT )ofsteelalloysisinfluencedbythematerialmicrostructureandtestingtemperature[1].Availablereferencesrangingfromanalyticalapproachtoempiricaltestsaretoonumeroustolist.Mostofthesemodesaredeterministic ,whichdidnottaketherandomnessoftheparametersandman_madeerrorintoconsideration .Thebasicproposesofthispaperistounderstandthetransitionbyanewrandom_fuzzymodel.Theductile brittletransitioninvolvestheductilefracture ,brittlefractureandthetransition .Inacerta…     

The effect of brittle interfacial compounds on deformation and fracture of molybdenum-aluminum fiber composites

The effect of brittle intermetallic compounds at the fiber-matrix interface on the deformation characteristics of molybdenum-aluminum fiber composites was investigated. If the filament is ductile and notch-insensitive, then composite strength degradation is relatively minor and composite strength can be predicted by a modified mixture-rule which neglects the strength contribution of the brittle compound. For the case of notch-sensitive filaments, severe filament degradation occurs upon compound formation. The degradation was shown to result from cracks formed during deformation at the roots of compound nodules. The presence of 10 per cent compound by volume results in a 50 per cent decrease in tensile strength, but larger amounts of compound cause little additional strength reduction. At filament volume fractions of 25 and 34 per cent and compound volume fractions less than 10 per cent, composite fracture occurs by the statistical accumulation of fiber necks or fractures depending on the notch sensitivity of the fiber. At high fiber or compound volume fractions, composite failure occurs upon the first or the second filament fracture.     

Thin-layer drying characteristics of sweet potato slices and mathematical modelling

The effect of blanching and drying temperature (50, 60 and 70°C) on drying kinetics and rehydration ratio of sweet potatoes was investigated. It was observed that both the drying temperature and blanching affected the drying time and rehydration ratio. The logarithmic model showed the best fit to experimental drying data. The values of effective moisture diffusivity and activation energy ranged from 9.32 × 10⁻¹¹ to 1.75 × 10⁻¹⁰ m²/s, and 22.7–23.2 kJ/mol, respectively.     

Maximum density effects on convective instability of horizontal plane poiseuille flows in the thermal entrance region

A linear stability analysis is used to study the conditions marking the onset of secondary flow in the form of longitudinal vortices for plane Poiseuille flow of water in the thermal entrance region of a horizontal parallel-plate channel by a numerical method. The water temperature range under consideration is 0∼30°C and the maximum density effect at 4°C is of primary interest. The basic flow solution for temperature includes axial heat conduction effect and the entrance temperature is taken to be uniform at far upstream location jackie=−∞ to allow for the upstream heat penetration through thermal entrance jackie=0. Numerical results for critical Rayleigh number are obtained for Peclet numbers 1, 10, 50 and thermal condition parameters (λ ₁, λ ₂) in the range of −2.0≤λ ₁≤−0.5 and −1.0≤λ ₂≤1.4. The analysis is motivated by a desire to determine the free convection effect on freezing or thawing in channel flow of water.     

Tensile-shear transition in mixed mode I/III fracture

The propensity of the transition of fracture type in either brittle or ductile cracked solid under mixed-mode I and III loading conditions is investigated. A fracture criterion based on the competition of the maximum normal stress and maximum shear stress is utilized. The prediction of the fracture type is determined by comparing τ_max/σ_max at a critical distance from the crack tip to the material strength ratio τ_C/σ_C, i.e., (τ_max/σ_max)<(τ_C/σ_C) for tensile fracture and (τ_max/σ_max)>(τ_C/σ_C) for shear fracture, where σ_C (τ_C) is the fracture strength of materials in tension (shear). Mixed mode I/III fracture tests were performed using circumferentially notched cylindrical bars made of PMMA and 7050 aluminum alloy. Fracture surface morphology of the specimens reveals that: (1) for the brittle material, PMMA, only tensile type of fracture occurs, and (2) for the ductile material, 7050 aluminum alloy, either tensile or shear type of fracture occurs depending on the mode mixity. The transition (in ductile material) or non-transition (in brittle material) of the fracture type and the fracture path observed in experiments were properly predicted by the theory. Additional test data from open literature are also included to validate the proposed theory.     

Search for conditions of compressive fracture of hard brittle ceramics at impact loading

In this paper we discuss three different experimental configurations to diagnosing the modes of inelastic deformation and to evaluating the failure thresholds at shock compression of hard brittle solids. One of the manifestations of brittle material response is the failure wave phenomenon, which has been previously observed in shock-compressed glasses. However, based on the measurements from our “theory critical” experiments, both alumina and boron carbide did not exhibit this phenomenon. In experiments with free and pre-stressed ceramics, while the Hugoniot elastic limit (HEL) in high-density B₄C ceramic was found to be very sensitive to the transverse stress, it was found relatively less sensitive in Al₂O₃, implying brittle response of the boron carbide and ductile behavior of alumina. To further investigate the effects of stress states on the shock response of brittle materials, a “divergent flow or spherical shock wave” based plate impact experimental technique was employed to vary the ratio of longitudinal and transversal stresses and to probe conditions for compressive fracture thresholds. Two different experimental approaches were considered to generate both longitudinal and shear waves in the target through the impact of convex flyer plates. In the ceramic target plates, the shear wave separates a region of highly divergent flow behind the decaying spherical longitudinal shock wave and a region of low-divergent flow. Experiments with divergent shock loading of alumina and boron carbide ceramic plates coupled with computer simulations demonstrated the validity of these experimental approaches to develop a better understanding of fracture phenomena.     

加载速率对40Cr钢Ⅱ型动态断裂特性的影响

采用新型Ⅱ型动态断裂测试技术,对高强钢40Cr在高加载速率下的Ⅱ型动态断裂特性进行了测试研究。基于新设计的Ⅱ型动态断裂试样和分离式霍普金森压杆（split Hopkinson pressure bar, SHPB）技术,通过实验-数值方法确定了裂尖在加载过程中的应力强度因子曲线。采用应变片法确定了试样的起裂时间,最终得到40Cr的Ⅱ型动态断裂韧性值,并对其加载速率相关性和材料的失效机理进行了研究。结果表明,在1.08～5.53 TPa·m1/2/s的加载速率范围内,40Cr的Ⅱ型动态断裂韧性基本表现为与加载速率成正相关的变化趋势。通过对试样断口形貌的分析,确定了材料的失效模式及机理,发现随着加载速率的增加,存在拉伸型失效向绝热剪切型失效模式转变的现象。     

Modeling of water transport in roof tiles by removal of moisture at isothermal conditions

The main objective of this article is to describe the drying process of ceramic roof tiles, shaped from red clay, using diffusion models. Samples of the product with initial moisture content of 0.24 (db) were placed inside an oven in the temperatures of 55.6, 69.7, 82.7 and 98.6°C; and the data of the drying kinetics were obtained. The analytical solutions of the diffusion equation for the parallelepiped with boundary conditions of the first and third kinds were used to describe the drying processes. The process parameters were determined using an optimization algorithm based on inverse method coupled to the analytical solutions. The analysis of the results makes it possible to affirm that the boundary condition of the third kind satisfactorily describes the drying processes. The values obtained for the convective mass transfer coefficient were between 8.25 × 10⁻⁷ and 1.64 × 10⁻⁶ m s⁻¹, and for the effective water diffusivity were between 9.21 × 10⁻⁹ and 1.80 × 10⁻⁸ m² s⁻¹.     

Effect of constraint on fracture controlled by stress or strain

To interpret fracture of solids, an appropriate fracture criterion is required. It is often believed that the level of strain ahead of a crack tip controls the fracture event for materials exhibiting high ductility, e.g. ductile fracture of A533B steel in the upper shelf regime. And the level of stress ahead of a crack tip controls the brittle fracture event, e.g. cleavage fracture of A533B steel in the lower shelf regime. Within each regime (ductile or brittle), the level of constraint of a specimen or structure determines the magnitude of the apparent fracture toughness. In this paper, we address the difference in the effect of constraint on the stress- or strain-controlled fracture. It is found that the constraint plays an opposite role to the apparent fracture toughness values for strain-controlled vs. stress-controlled fracture.     

Simulation of voids effect on ductile fracture of metallic alloys

Most commerical alloys have inclusions which reduce their ductility and toughness. Ductile fracture of perforated mild steel sheet was investigated in order to simulate the fracture of metallic alloys containing a second phase or inclusions. The growth of the holes during tensile straining has been studied. The results indicate that fracture of the specimens did not result from the coalescence of growing holes, but from the initiation of a shear crack at a side of the hole after the strain of the matrix close to that hole reached a critical value.Theories of ductile fracture^1–4 were examined using experimental data obtained using mild steel sheet and ductile cast iron. It was found that these theories can be used to predict the experimental results within some limitations.     

The influence of oil on nucleate pool boiling heat transfer

The influence of various oil contents in R134a is investigated for nucleate pool boiling on copper tubes either sandblasted or with enhanced heating surfaces (GEWA-B tube). Polyolester oils (POE) (Reniso Triton) with medium viscosity 55 cSt (SE55) and high viscosity 170 cSt (SE170) were used. Heat transfer coefficients were obtained for boiling temperatures between −28.6 and +20.1°C. The oil content varied from 0 to 5% mass fraction. For the sandblasted tube and the SE55 oil the heat transfer coefficients for the refrigerant/oil-mixture can be higher or lower than those for the pure refrigerant, depending on oil mass fraction, boiling temperature and heat flux. In some cases the highest heat transfer coefficients were obtained at a mass fraction of 3%. For the 170 cSt oil there is a clear decrease in heat transfer for all variations except for a heat flux 4,000 W/m² and −10.1°C at 0.5% oil content. The heat transfer coefficients are compared to those in the literature for a smooth stainless steel tube and a platinum wire. For the enhanced tube and 55 cSt oil the heat transfer coefficients are clearly below those for pure refrigerant in all cases. The experimental results for the sandblasted tube are compared with the correlation by Jensen and Jackman. The calculated values are within +20 and −40% for the medium viscosity oil and between +50% and −40% for the high viscosity oil. A correlation for predicting oil-degradation effects on enhanced surfaces does not exist.