TEMPERATURE EFFECT ON LOW-CYCLE FATIGUE BEHAVIOR OF NICKEL-BASED SINGLE CRYSTALLINE SUPERALLOY

The low-cycle fatigue （LCF） behavior of a nickel-based single crystal superalloy with [001] orientation was studied at an intermediate temperature of T0℃ and a higher temperature of To ＋ 250℃ under a constant low strain rate of 10^-3 s^-1 in ambient atmosphere. The superalloy exhibited cyclic tension-compression asymmetry which is dependent on the temperature and applied strain amplitude. Analysis on the fracture surfaces showed that the surface and subsurface casting micropores were the major crack initiation sites. Interior Ta-rich carbides were frequently observed in all specimens. Two distinct types of fracture were suggested by fractogaphy. One type was characterized by Mode-I cracking with a microscopically rough surface at To ＋ 250℃. Whereas the other type at lower temperature T0℃ favored either one or several of the octahedral {111} planes, in contrast to the normal Mode-I growth mode typically observed at low loading frequencies （several Hz）. The failure mechanisms for two cracking modes are shearing of γ＇ precipitates together with the matrix at T0℃ and cracking confined in the matrix and the γ/γ＇interface at To - 250℃.     

晶粒的取向和变形性质对双晶体循环变形影响的模拟研究

应用晶体细观力学方法，分析了双晶体循环变形过程中组元晶粒取向及其变形性质（Ｂａｕｓｃｈｉｎｇｅｒ效应和循环硬化）的影响，发现双晶体的反向屈服及循环硬化行为为主要由组元晶粒性质支配，晶间内应力的影响是次要的，晶粒取向对宏微观应力应变行为有重要的影响，取向对称性较弱或罗硬差别较大的双晶体晶界影响较大。     

Transient elongational viscosities of aqueous polyacrylamide solutions measured with an optical rheometer

An anionic polyacrylamide solution was characterized in elongational flow by combining laser-Doppler velocimetry to determine the strain rate in the flow direction and the two-color flow-induced birefringence method to measure the first normal stress difference along the axial centerline of a hyperbolic die. The elongational rate was constant along the axial centerline of the planar hyperbolic die as long as vortices at the die entrance did not occur. The transient elongational viscosity μ ⁺ was determined as a function of the elongational rate. The parameters varied are the Hencky strain rate and the polymer concentration. μ ⁺ showed a pronounced increase over the linear viscoelastic behavior above critical Hencky strains of 1.2 to 1.5; that is, a significant strain hardening could be observed for polyacrylamide solutions. This strain hardening is stronger the higher the elongational rate. A slight enhancement of strain hardening was found by increasing the concentration from 0.5 to 1 g/l. The stress optical coefficient was determined as 1.8 × 10⁻⁷ Pa⁻¹ (0.5 g/l) and 1.2 × 10⁻⁷ Pa⁻¹ (1 g/l).

On perfectly stress field at a mixed-mode crack tip under plane and anti-plane strain

In [1], under the condition that all the perfectly plastic stress components at a crack tip are functions of ϕ only, making use of equilibrium equations, stress-strain rate relations, compatibility equations and yield condition. Lin derived the general analytical expressions of the perfectly plastic stress field at a mixed-mode crack tip under plane and anti-plane strain. But in [1] there were several restrictions on the proportionality factor γ in the stress-strain rate relations, such as supposing that γ is independent of ϕ and supposing that γ=c or cr⁻¹. In this paper, we abolish these restrictions. The cases in [1], γ=cr^d (n=0 or-1) are the special cases of this paper.     

Torsional split Hopkinson bar tests at strain rates above 104s−1

The torsional split Hopkinson bar is used for testing materials at strain rates above 10⁴s⁻¹. This strain rate, which is an order of magnitude higher than is typical with this technique, is obtained by using very short specimens. Strain rates of 6.4×10⁴s⁻¹ have been achieved with specimens having a gage length of 0.1524 mm. Results from tests on 1100 aluminum show an increase in rate sensitivity as the strain rate increases.     

Measurements and model predictions of transient elongational rheology of polymeric nanocomposites

Transient elongational rheology of two commercial-grade polypropylene (PP) and the organoclay thermoplastic nanocomposites is investigated. A specifically designed fixture consisting of two drums (SER Universal Testing Platform) mounted on a TA Instruments ARES rotational rheometer was used to measure the transient uniaxial extensional viscosity of both polypropylene and nanoclay/PP melts. The Hencky strain rate was varied from 0.001 to 2 s^− 1, and the temperature was fixed at 180°C. The measurements show that the steady-state elongational viscosity was reached at the measured Hencky strains for the polymer and for the nanocomposites. The addition of nanoclay particles to the polymer melt was found to increase the elongation viscosity principally at low strain rates. For example, at a deformation rate of 0.3 s^− 1, the steady-state elongation viscosity for polypropylene was 1.4 × 10⁴ Pa s which was raised to 2.8 × 10⁴ and 4.5 × 10⁴ Pa s after addition of 0.5 and 1.5 vol.% nanoclay, respectively. A mesoscopic rheological model originally developed to predict the motion of ellipsoid particles in viscoelastic media was modified based on the recent developments by Eslami and Grmela (Rheol Acta 47:399–415, 2008) to take into account the polymer chain reptation. We show that the orientation states of the particles and the rheological behavior of the layered particles/thermoplastic hybrids can be quantitatively explained by the proposed model.     

Measurement of thermal expansion coefficients of composites using strain gages

The measurement of the coefficients of thermal expansion (CTEs) of composite materials using electrical resistance strain gages is addressed. Analytical expressions for the CTEs of an orthotropic lamina are derived, accounting for the effects of transverse sensitivity and possible misalignment of the gages. Experiments are performed for the characterization of the thermal expansion behavior of a fiber-glass-reinforced epoxy unidirectional lamina using an invar specimen as reference material. Preliminary training cycles are performed for the determination of an optimal heating rate for the measurements, which ensures thermal equilibrium conditions. Three measurement cycles yield the principal CTEs of the lamina α₁, α₂ and α₁₂ with repeatability within ±0.34×10⁻⁶, ±0.85×10⁻⁶ and ±2.8×10⁻⁶/°C, respectively. It is noted that inhomogeneity of the specimen and variation in thermomechanical properties of the gages can cause a noticeable spead in the measurements.     

Precursor ionization ahead of strong shock waves in argon

The mechanism of precursor ionization ahead of strong shock waves has been studied in a low density shock tube. The experimental results are illustrated with Arrhenius plots with kink points dividing them into two parts with apparent activation energy ratio 1:2, namely with the values 7.7 eV and 15.3 eV, and varying with first and third power of the density respectively. A model is proposed to interpret the facts where the process taking place in the precursor region, is a two step photo ionization accompanied with the drift flow effect of the gas relative to the shock wave or the ionization recombination effect according to whether the shock speed and initial density are low enough. The product of the A-A collision excitation cross section coefficientS ^* multiplied by the radiation cross sectionQ ^* of ArgonS ^*×Q ^*=1×10⁻³⁶ (cm⁴eV⁻¹) and the three body recombination coefficient of Argon at room temperaturek _ra =1×10⁻²⁴ (cm⁻⁶s⁻¹). The project supported by the National Natural Science Foundation of China     

Stress-strain relationships for spruce wood: Influence of strain rate,moisture content and loading direction

The influence of strain rate, moisture content and loading direction on the stress-strain relationships for spruce wood has been investigated. The strain rates were approximately 8×10⁻³ s⁻¹, 17s⁻¹ and 1000 s⁻¹, and the states of moisture content were those corresponding to oven dry, fiber saturated and fully saturated. Compressive loads were applied along the principal directions of the stem of the tree, i.e., radially, tangentially and axially. The low and medium strain-rate tests were performed with the aid of a servohydraulic testing machine, while the high strain-rate tests were carried out using the split Hopkinson pressure bar (SHPB) technique. Magnesium or steel bars were used in the different SHPB tests in order to reduce impedance mismatch for the different directions of the wood specimens. The strain rate was found to have large influence on the behavior of the wood, especially under the condition of full saturation, where water transport in the deforming specimen is of major importance.     

Simulation of cyclic deformation of bicrystals: Effects of orientation and deformation properties of constituent grains

The cyclic deformation of aluminium bicrystals was numerically simulated by using a crystalline micromechanical approach to study the effects of crystallographic orientation and deformation properties of constituent grains. Both the macro-and micro-stress-strain responses were analyzed. It was shown that the whole Bauschinger effect and cyclic hardening behavior of bicrystals is primarily controlled by the corresponding properties of the constituent grains, and that the effects of internal stresses induced by the grain boundary and the interaction between grains are secondary. The crystallographic orientation of constituent grains was also shown to have significant influence on the macro-and micro-mechanical behavior of the bicrystals. There were smaller symmetry in the orientation or greater difference in the strength between grains and more remarkable GB effects.     

A NEW CYCLIC J-INTEGRAL FOR LOW-CYCLE FATIGUE CRACK GROWTH

The constitutive equation under the low-cycle fatigue (LCF) was discussed, and a two-dimensional (2-D) model for simulating fatigue crack extension was put forward in order to propose a new cyclic J-integral. The definition, primary characteristics, physical interpretations and numerical evaluation of the new parameter were investigated in detail. Moreover, the new cyclic J-integral for LCF behaviors was validated by the compact tension (CT) specimens. Results show that the calculated values of the new parameter can correlate well with LCF crack growth rate, during constant-amplitude loading. In addition, the phenomenon of fatigue retardation was explained through the viewpoint of energy based on the concept of the new parameter.     

An experimental study of dynamic tensile properties of glass fiber at low-temperatures

Tensile impact experiments of EC8.0−24×7 glass fiber bundles at different low temperaturesT(14°C, −40°C and −10°C) and strain rates ɛ were carried out, and complete stress-strain curves were obtained. Within the range of the experiment temperatures and strain rates, it is found that the initial modulusE, the ultimate strength σ_max and the unstable strain ɛ _b of the glass fiber bundles all increase with ɛ at an identicalT. At an identical ɛ, with the decrease ofT, E and σ_max increase; but ɛ _b increases when 10°C>T>−40°C and decreases when −40°C>T>−100°C. The strain-rate- and temperature-dependent bimodal Weibull statistical constitutive theory was adopted for the statistical analysis of the experimental results, and the Weibull parameters of single fiber were obtained. The results show that the bimodal Weibull distribution function is suitable to represent the strength distribution of the glass fiber at low temperature and different strain rates. The differences in the mechanical properties between EC8.0−24×7 and EC5.5−12 ×14 glass fiber bundles were also discussed. Project supported by the National Natural Science Foundation of China (No. 19772058).     

Novel Microtensile Method for Monotonic and Cyclic Testing of Freestanding Copper Thin Films

This paper presents the results of new microtensile tests conducted to investigate the mechanical properties of submicron-thick freestanding copper films. The method, used in this study, allows the observation of materials response under uniaxial tensile loads with measurements of stress at strain rates up to 5.5 × 10⁻⁴/s. It also facilitates tension–tension fatigue experiments under a variety of mean stress conditions at cyclic loading frequencies to 20 Hz. The sample processes involve fabrication of a supporting frame with springs and alignment beams all made of electroplated nickel. Electroplating took place on top of a previously deposited sample rather than creating a structure by subtractive fabrication. Tensile sample loading is applied using a piezoelectric actuator. Load was measured using a capacitance gap sensor with a novel mechanical coupling to the sample. Tension–tension fatigue experiments were carried out with feedback to give load control. Fatigue tests were conducted on sputter-deposited 500 and 900 nm copper films with grain sizes ∼50 nm. Fatigue life reached 10⁵ cycles at low mean load, which decreased with an increase in the mean load. The results indicate decreasing plasticity with increasing mean load.     

Transfer model and kinetic characteristics of $${\rm NH}_{4}^{+}$$ –K+ ion exchange on K-zeolite

Based on the mass transfer theory, a new mass transfer model of ion-exchange process on zeolite under liquid film diffusion control is established, and the kinetic curves and the mass transfer coefficients of –K⁺ ion-exchange under different conditions were systemically determined using the shallow-bed experimental method. The results showed that the –K⁺ ion-exchange rates and transfer coefficients are directly proportional to solution flow rate and temperature, and inversely proportional to solution viscosity and the size of zeolite granules. It also showed that the transfer coefficient is not influenced by the ion concentrations. For a large ranges of operational conditions including temperatures (10 − 75°C), flow rates (0.031 m s⁻¹ −0.26 m s⁻¹), liquid viscosities (1.002 × 10⁻³ N s m⁻² − 4.44 × 10⁻³ N s m⁻²), and zeolite granular sizes (0.2 − 1.45 mm), the average mass transfer coefficients calculated by the model agree with the experimental results very well.     

Comparison of experimental data with results of some drying models for regularly shaped products

This paper presents an experimental and theoretical investigation of drying of moist slab, cylinder and spherical products to study dimensionless moisture content distributions and their comparisons. Experimental study includes the measurement of the moisture content distributions of slab and cylindrical carrot, slab and cylindrical pumpkin and spherical blueberry during drying at various temperatures (e.g., 30, 40, 50 and 60°C) at specific constant velocity (U = 1 m/s) and the relative humidity φ = 30%. In theoretical analysis, two moisture transfer models are used to determine drying process parameters (e.g., drying coefficient and lag factor) and moisture transfer parameters (e.g., moisture diffusivity and moisture transfer coefficient), and to calculate the dimensionless moisture content distributions. The calculated results are then compared with the experimental moisture data. A considerably high agreement is obtained between the calculations and experimental measurements for the cases considered. The effective diffusivity values were evaluated between 0.741 × 10⁻⁵ and 5.981 × 10⁻⁵ m²/h for slab products, 0.818 × 10⁻⁵ and 6.287 × 10⁻⁵ m²/h for cylindrical products and 1.213 × 10⁻⁷ and 7.589 × 10⁻⁷ m²/h spherical products using the Model-I and 0.316 × 10⁻⁵–5.072 × 10⁻⁵ m²/h for slab products, 0.580 × 10⁻⁵–9.587 × 10⁻⁵ m²/h for cylindrical products and 1.408 × 10⁻⁷–13.913 × 10⁻⁷ m²/h spherical products using the Model-II.     

Dynamic flight stability of a bumblebee in forward flight

The longitudinal dynamic flight stability of a bumblebee in forward flight is studied. The method of computational fluid dynamics is used to compute the aerodynamic derivatives and the techniques of eigenvalue and eigenvector analysis are employed for solving the equations of motion. The primary findings are as the following. The forward flight of the bumblebee is not dynamically stable due to the existence of one （or two） unstable or approximately neutrally stable natural modes of motion. At hovering to medium flight speed [flight speed Ue = （0-3.5）m s^-1; advance ratio J = 0-0.44], the flight is weakly unstable or approximately neutrally stable; at high speed （Ue = 4.5 m s^-1; J = 0.57）, the flight becomes strongly unstable （initial disturbance double its value in only 3.5 wingbeats）.     

镍基单晶合金多轴非比例加载低周疲劳研究

基于正交设计, 分别在680℃和850℃下进行DD3镍基单晶合金薄壁圆管试样([001]取向)拉/扭非比例加载低周疲劳试验, 研究等效应变范围、应变路径角、拉/扭载荷相位角、循环特性和温度诸因素对镍基单晶合金多轴低周疲劳寿命的影响作用. 疲劳试验数据的极差分析表明, 应变路径角、拉/扭载荷相位角和等效应变范围是影响疲劳寿命的主要因素. 将菱形应变加载路径区分为比例加载段和非比例加载段, 提出了表征非比例加载效应的等效应变参量, 并通过引入单晶应变三轴性因子反映拉/扭应变路径角对多轴疲劳寿命的影响. 用考虑非比例加载效应的等效应变范围和单晶应变三轴性因子构造循环塑性应变能损伤参量, 进行多元线性回归分析, 疲劳寿命回归模型与试验寿命具有很好的相关性, 所有试验数据都落在2.0倍的偏差分布带之内.      

A rigorous assessment of the benefits of miniaturization in the Kolsky bar system

A rigorous experimental and numerical assessment is made of the benefits and limits of miniaturization in the Kolsky bar system. The primary issues that arise in very high strain rate testing (stress equilibration, inertial effects, wave dispersion, friction, and controllability of deformations) are addressed through experiments coupled with explicit finite element analyses. A miniaturized Kolsky bar system that includes the input bar is developed, together with the use of the laser occlusive radius detector to obtain local measurements of specimen strain during the very high rate deformations. It is demonstrated that this miniaturized Kolsky bar system can be used to provide fully validated results, including the explicit determination of equilibration, over a very wide range of strain rates (1×10³ to 5×10⁴ s⁻¹). The desired high strain rate can be achieved even at low accumulated strains, and the total strain developed can be controlled very effectively. Specific conditions are developed for determining the range of utility of the technique for a given material. The technique is applied to the characterization of 6061-T651 aluminum, and the results are compared with the results obtained using a conventional Kolsky bar.     

Measurement of Strain Localization Resulting from Monotonic and Cyclic Loading at 650 <Superscript>∘</Superscript>C in Nickel Base Superalloys

A methodology is presented for the use of the oxide scale that develops in polycrystalline Ni-base superalloys at service temperature, as a speckle pattern for μm-scale resolution strain measurements. Quantitative assessment of the heterogeneous strain field at the grain scale is performed by high-resolution SEM digital image correlation under monotonic and cyclic loading in polycrystalline Ni-base superalloys up to 650 ^°C. In the René 88DT superalloy, strain localization is observed near twin boundaries during low cycle fatigue (LCF) at intermediate temperatures, correlating with activation of {111} 〈110〉 and {111} 〈112〉 slip systems. A strong correlation between the microstructural configuration that promotes strain localization during monotonic loading and crack initiation at 650 ^°C in low cycle fatigue was observed.     

Miniaturized Compression Test at Very High Strain Rates by Direct Impact

A modified miniaturized version of the Direct Impact Compression Test (DICT) technique is described in this paper. The method permits determination of the rate-sensitive plastic properties of materials up to strain rate ∼10⁵ s⁻¹. Miniaturization of the experimental setup with specimen dimensions: diameter d _S = 2.0 mm and thickness l _S = 1.0 mm, Hopkinson bar diameter 5.2 mm, with application of a novel optical arrangement in measurement of specimen strain, makes possible compression tests at strain rates from ∼10³ s⁻¹ to ∼10⁵ s⁻¹. In order to estimate the rate sensitivity of a low-alloy construction steel, quasi-static, Split Hopkinson Pressure Bar (SHPB) and DICT tests have been performed at room temperature within the rate spectrum ranging from 5*10⁻⁴ s⁻¹ to 5*10⁴ s⁻¹. Adiabatic heating and friction effects are analyzed and the final true stress versus true strain curves at different strain rates are corrected to a constant temperature and zero friction. The results have been analyzed in the form of true stress versus the logarithm of strain rate and they show two regions of a constant rate sensitivity : relatively low up to the strain rate threshold ∼50 s⁻¹, and relatively high above the threshold, up to strain rate ∼4.5*10⁴ s⁻¹.