基于永磁恒定磁场激励的起始磁化曲线测量

现有起始磁化曲线测量系统需绕制励磁线圈和感应线圈,在线应用受限.为此,本文提出了一种基于永磁恒定磁场激励的起始磁化曲线测量原理并搭建了相应测量系统.该系统采用永磁磁化器作为激励磁源,以对称磁化方法在圆柱棒状构件上激励出随轴向位置变化的恒定磁场作为激励磁场;采用阵列霍尔探头测量构件表面不同提离下的轴向和法向磁感应强度;并基于多项式外推法和磁场高斯定理外推法,推算构件与空气分界面上的轴向和法向磁感应强度;进一步地,根据分界面上的磁感应强度获取构件的起始磁化曲线.系统测量结果表明,在永磁恒定磁场激励下,无须励磁线圈和感应线圈即可方便地获取棒状构件的起始磁化曲线,测量误差小于10%,测量误差标准差小于0.01,重复性较好.该系统可为便捷地在线测量棒状构件起始磁化曲线提供新途径.     

磁熵变测量实验装置

简述了磁熵概念及磁熵变测量原理,介绍了应用于教学的磁熵变测量实验装置.利用该装置测量了金属钆在0～50℃温度范围,最大磁场为2T的等温磁化曲线,计算了不同温度下的磁熵变.     

Sm_2(TM)_17合金的磁性(自旋再取向相变)研究

本文研究了Sm_2(FeNiCoM)_(17)合金(M为非磁性组元)的磁性。样品由六角结构无序型的2∶17主相及少量FeNi合金杂相组成。在六角结构的e轴方向(易磁化方向)观察到下述异常现象:低温(273K以下)时的磁化及反磁化曲线发生明显的跃变,跃变时相应的磁场H_r随温度下降而增大;磁滞迴线是蜂腰型的,温度愈低蜂腰愈明显;升温时磁化强度随温度变化(1.5K至居里点T_C)的曲线上出现极大值,其相应的温度T_t随磁场增大而降低;降温时观察到了热磁滞后现象。但在基面(难磁化方向)上及Co含量增多(>18at％)时,样品却表现了正常的铁磁行为。本文提出用磁矩非共线结构排列的自旋再取向相变来解释上述异常现象,并给出自旋倒向所需越过的能垒高度U=9.2×10~(-15)erg,用设想磁结构的模型得到的磁化强度的计算值与实验值也符合得较好。     

Sm2(TM)17合金的磁性(自旋再取向相变)研究

本文研究了Sm₂(FeNiCoM)₁₇合金(M为非磁性组元)的磁性。样品由六角结构无序型的2∶17主相及少量FeNi合金杂相组成。在六角结构的e轴方向(易磁化方向)观察到下述异常现象:低温(273K以下)时的磁化及反磁化曲线发生明显的跃变,跃变时相应的磁场H_r随温度下降而增大;磁滞迴线是蜂腰型的,温度愈低蜂腰愈明显;升温时磁化强度随温度变化(1.5K至居里点T_C)的曲线上出现极大值,其相应的温度T_t随磁场增大而降低;降温时观察到了热磁滞后现象。但在基面(难磁化方向)上及Co含量增多(>18at％)时,样品却表现了正常的铁磁行为。本文提出用磁矩非共线结构排列的自旋再取向相变来解释上述异常现象,并给出自旋倒向所需越过的能垒高度U=9.2×10^-15erg,用设想磁结构的模型得到的磁化强度的计算值与实验值也符合得较好。 关键词：     

基于时空变换恒定磁化的起始磁化曲线推算方法

起始磁化曲线作为铁磁材料磁学特性的重要表征, 研究其获取方法具有重要意义. 现有方法采用随时间变化磁场作为激励磁场, 通过改变激励磁场大小, 逐步改变试件内的磁场及磁感应强度并进行测量以得到起始磁化曲线, 效率较低, 准备繁琐. 为此, 本文从基本的磁学物理定理出发, 提出一种基于时空变换的起始磁化曲线推算方法. 该方法以细长棒状试件或环形试件作为被测试件; 采用恒定磁化在被测试件内产生空间变化磁场作为激励磁场; 通过测量试件表面的磁场值来推算试件内磁场值, 从而获取铁磁材料起始磁化曲线. 直流线圈恒定磁化环形和棒状试件仿真实验验证了该方法的理论正确性. 进一步地, 考虑实际应用限制因素的推算结果表明了该方法在实际应用中是可行的, 可为探索新的起始磁化曲线测量方法提供理论指导.     

La2/3Ca1/3MnO3的巨磁熵效应

本文对超大磁阻材料Ｌａ２／３Ｃａ１／３ＭｎＯ３的巨磁熵效应进行了研究,通过测量不同磁场下的磁化－温度曲线,发现伴随铁磁－顺磁相变有一个大的磁熵变化,这个结果表明钙钛矿锰氧化物可以作为磁致冷技术中的工作物质。     

熔融织构YBCO的磁性

测量了熔融织构YBCO样品从1.5K到89K的磁化曲线。磁场H平行于c轴时,在1.5K,7K和10K观察到磁通跳跃,在15—83K的温度区间观察到峰值现象。详细分析了磁化曲线和磁临界电流的各向异性。讨论了晶粒之间连接的性质和主要的钉扎中心。 关键词：     

垂直磁记录薄膜实施剩余磁化测量时退磁场的补偿

对于垂直磁记录薄膜，进行剩余磁化强度的测量时，必须补偿退磁场.提出一种新方法，在直流退磁剩磁和等温剩磁测量中采用有效反向磁场来直接补偿退磁场.从而可以正确地得出垂直磁记录薄膜的ΔM曲线并评价晶粒间的磁相互作用.还采用了三种方法来确定其中的关键参数——退磁因子.结果表明，c轴垂直取向的钡铁氧体薄膜中，晶粒间的磁相互作用是交换偶合型的；而Co-Cr-Ta薄膜中，晶粒间磁相互作用是静磁相互作用. 关键词： 退磁场补偿 直流退磁剩磁(DCD) 等温剩磁(IRM) ΔM曲线     

通过磁化曲线测定金属玻璃窄带的感生磁各向异性常数

一、引 言 由于原子的非晶型排列,铁磁金属玻璃没有磁晶各向异性,但是在磁场或张力下退火,或进行冷轧之后,能够得到感生磁各向异性.这些感生各向异性都有一个特定的对称主轴(磁场轴、张力轴、辊轧轴),其各向异性能密度至少在带面内可以表示为 其中 θ为饱和磁化强度 M_g与主轴的夹角,K_(u1)和K_(u2)为前两个单轴各向异性常数. 为决定K_(u1)和K_(u2),一般要取圆片样品在转矩磁强计中测量磁转矩曲线再作傅里叶分析～[1,2].对于易磁化轴在横向或难磁化轴在纵向的窄带样品,也可以从饱和磁化功或指定磁化强度下的磁化率测量,得到笼统的有效各向…     

通过磁化曲线计算金属磁熵变

用振动样品磁强计测量金属钆的磁化曲线,采用二步最小二乘法拟合出二元函数M(H,T)的表达式,然后通过热力学关系式计算出它的磁熵变. 关键词：     

对铁磁材料居里点的测量

介绍了通过转换出分别与磁化强度和磁场强度成正比的电压信号,来定性观察与定量测量居里点的一种方法。     

Spin reorientation transition in (111) textured L10 CoPt layers

In this work, a spin reorientation transition from [001] axis to an in-plane direction occurs near Curie temperature under a small external field for (111) textured L1₀ CoPt layers in an AlN/CoPt multilayer film, indicating the dominant role of the shape anisotropy at elevated temperatures over the magnetocrystalline anisotropy. A large in-plane residual magnetization is also observed after cooling the sample from a temperature above the Curie point. The formation of magnetization during cooling is considered due to the alignment of magnetic moments along the easy axis by the small field in the spin reorientation transition temperature region. Our work reveals the importance of shape anisotropy for the formation of magnetization in the heat assisted magnetic recording process.     

All-optical magnetic recording with circularly polarized light

We experimentally demonstrate that the magnetization can be reversed in a reproducible manner by a single 40 femtosecond circularly polarized laser pulse, without any applied magnetic field. This optically induced ultrafast magnetization reversal previously believed impossible is the combined result of femtosecond laser heating of the magnetic system to just below the Curie point and circularly polarized light simultaneously acting as a magnetic field. The direction of this opto-magnetic switching is determined only by the helicity of light. This finding reveals an ultrafast and efficient pathway for writing magnetic bits at record-breaking speeds.     

A rotating probe for measuring the inhomogeneity of a magnetic field

The theory is given of a rotating probe for measuring the inhomogeneity of a magnetic field. The design of the instrument and its calibration are described, giving its sensitivity and some methods of use such as the measurement of saturation magnetization, the Curie point and hysteresis loops.     

Effect of electric field on the magnetic characteristics of a ferromagnetic nanosemiconductor

A theory is developed to describe the effect of an electric field on the magnetization of a thin ferromagnetic semiconductor plate. It is shown that the magnetic moment density is nonuniform under these conditions and that the total magnetic moment and its density depend on the electric field and the temperature. An electric field is found to increase the Curie temperature, and an inflection point is detected in the temperature dependence of the derivative of the total magnetic moment with respect to temperature.     

Gd3Co29-xCrx新相化合物的结构与磁性

制备出具有室温单轴磁晶各向异性的非间隙型Co基Gd3Co29-xCrx化合物(x=65和70)，x射线衍射和磁性测量表明所有单相化合物均属于单斜晶系，Nd3(Fe,Ti)29型结构和A2/m空间群.Gd3Co29-xCrx化合物的居里温度在x=65时为412 K，x=70时为359 K. Gd3Co29-xCrx化合物在x=65 时磁化强度随温度的变化曲线表明，在居里温度以下的某一温度处有一补偿点，在补偿点处求得晶格分子场系数nRT=33 T f.u./μB. 关键词： Gd3Co29-xCrx化合物 x射线衍射 磁晶各向异性     

Unambiguous determining the Curie point in perovskite manganite with second-order phase transition by scaling method

The accurate determination of the Curie temperature (T_C) is particularly important in describing the magnetic behavior close to the paramagnetic-ferromagnetic (PM-FM) phase transition. In this paper, we studied the magnetic phase transition and accurately predicted the Curie point of perovskite manganite La_0.825Sr_0.175MnO₃. We find the compound shows a second-order PM-FM transition and has a large magnetic entropy change (MEC) in vicinity of phase transition region. Based on the scaling law and the correlation between magnetic field and MEC, the precise and magnetic-independent Curie temperature was determined to be 281.7 K, obviously lower than 285.4 K decided from the magnetization versus temperature. The reliability of new Curie temperature can be well confirmed by the modified Arrott plot together with the critical exponents. Our results not only open up a new pathway for precise definition of Curie point but also facilitate the efficient exploitation of spontaneous magnetic bubbles in perovskite manganite.     

非均匀铁磁体自发磁化的平均场理论

从描写非均匀铁磁体的平均场近似的非线性微分方程出发,本文用分支点理论处理相变现象。指出:(1)系统的居里点由线性化方程的最大本征值决定;(2)略低于居里点时系统磁化的空间分布可用相应的本征函数描写;(3)磁化的温度关系由参数a(T)～(1-T/T_C)^1/2表示。本文最后用薄膜和一个简单的模型为例指出方法的利用。 关键词：     

Zero—field—cooled and field—cooled magnetizations and magnetic susceptibility of itinerant ferromagnet SrRuO3

Zero-field-cooled(ZFC) magnetization,field-cooled(FC) magnetization,ac magnetic susceptibility and major hysteresis loops of itinerant ferromagnet SrRuO3 have been measured at magnetic ordering temperatures ranging from 5 to 160K.An empirical model is proposed to calculate the measured ZFC magnetization.The result indicates that the calculated ZFC magnetization compares well with the measured one.Based on the generalized Preisach model.both the ZFC and FC curves are reproduced by numerical simulations.The critical temperature and critical exponents are determined by measuring the ac magnetic susceptibility in different bias magnetic fields at temperatures in the vicinity of the point of phase transition.     

Imaging magnetic responses of nanomagnets by XPEEM

The Spin-resolved Photoelectron Emission Microscope (SPEEM) is a permanently installed set-up at Helmholtz-Zentrum Berlin (HZB). Due to its specific contrast it is mainly used for magnetic imaging and micro-spectroscopy with quantitative analysis. A crucial point in magnetic imaging is the application of magnetic fields. Many experiments require observation of magnetic responses or the preparation of a certain magnetic state during the measurement. We present a dedicated magnetic sample holder combining magnetic field during imaging with additional temperature control. This set-up enables SPEEM to measure magnetization curves of individual Fe nanocubes (18 nm)³ in size. If additionally alternating magnetic fields are applied we can image the local magnetic AC susceptibility (χ_AC) as a function of temperature. The latter is ideally suited to visualize local variations of the Curie temperature (T_C) in nano- and microstructures.