准分子激光辐照K9玻璃的热力效应分析

基于传热学理论, 利用有限元法对KrF准分子激光辐照K9玻璃样品中的热力效应进行了数值分析, 并比较了脉冲数目和重频对损伤效果的影响。研究表明, 较低的准分子激光能量就能够使K9玻璃在表面和体内产生热应力损伤, 热应力损伤在光斑区域内主要由压缩热应力控制, 在光斑边缘和材料内部则主要由拉伸热应力控制。在激光脉冲结束时刻, 产生的温度和热应力最大, 且热应力以热冲击波的形式在材料内传播, 随时间变化而来回振荡, 逐渐减弱。这种热应力的反复冲击会对材料产生持续的损伤增长效应, 增加了材料的损伤时间, 并使材料更容易断裂。脉冲数目和重复频率对损伤效果有着较大影响, 在高重复频率下, 损伤累积效应明显。     

高重复频率激光脉冲光束大小对吸收玻璃损伤特征的影响

针对高重复频率对吸收性滤光片损伤问题,研究了高重复频率(kHz量级)激光脉冲的光束半径大小对吸收玻璃的形貌特征和损伤机理.研究发现在总的激光作用个数、单脉冲能量和脉冲作用频率固定时,吸收玻璃的损伤特性发生很大变化:在光束半径较大时,激光能量分散,主要损伤形貌是熔化破坏;随着光束半径的减小,激光脉冲能量变得集中,热量的累积效果变得明显,逐渐变成熔化破坏和气化破坏;当激光光束半径小到一定程度,则会由于光强过大使得介质表面发生击穿而产生激光等离子体冲击波,同时由于热量沉积的集中使光束作用中心处产生超热液体,当满足相爆炸发生的条件时,气化物、液滴和固体颗粒的混合物会向外飞溅,在损伤凹陷的周围形成气化物、液滴的冷凝区和固体颗粒溅射区. 关键词： 激光诱导损伤 高重复激光脉冲 吸收玻璃 相爆炸     

二次彩虹法测量高折射率玻璃微珠折射率研究

基于米氏散射理论解释了激光照明下玻璃微珠的二次彩虹精细结构的成因,发现折射率的差异将直接影响二次彩虹精细结构的位置.对于实验中玻璃微珠半径变化引起二次彩虹精细结构间距变化的现象亦用米氏散射理论进行了模拟分析和实验研究.利用米氏散射的近似理论——艾里理论对玻璃微珠的折射率进行了测量.在对玻璃微珠二次彩虹精细结构所计算得到的折射率的统计分析基础上,通过校正测量误差后得到了玻璃微珠折射率的准确数据.     

多脉冲激光对K9玻璃的表面损伤实验研究

 实验研究了波长为1 064 nm、脉宽为10 ns、重复频率为1 Hz的激光脉冲对K9玻璃的表面损伤特点,给出了脉冲透过能量随激光脉冲作用次数变化的规律。采用3维立体显微镜对损伤形貌进行观察,发现K9玻璃的损伤表面呈环状分布,分为烧蚀区、微裂纹区和断裂区。随着激光脉冲个数的增加,损伤由点状破坏演变为损伤区,微裂纹逐渐增长,损伤面积逐渐增大。基于激光支持的爆轰波理论分析,激光与脆性材料的相互作用可引起微裂纹的大量增长。在多脉冲激光的作用下,K9玻璃损伤的累积效应明显,表面损伤阈值明显降低,表面裂纹增长明显,损伤面积逐渐增大;但随着激光脉冲的继续增加,这种损伤趋于稳定。     

Laser cleaving on glass sheets with multiple laser beams

A multiple laser system consisting of CO₂ line-shaped and Nd-YAG pulsed lasers was applied to cleave a soda-lime glass substrate in this study. Due to an increase of absorption coefficient of the wavelength of 1.06 μm for Nd-YAG laser on the soda-lime glass at high temperatures, the glass sheets were preheated by the CO₂ line-shaped laser and followed with the pulsed Nd-YAG laser to generate a mixture fracture mode on the substrate. The stress distribution on the glass substrate cleaved by the multiple laser beams has been analyzed. An uncoupled thermal–elastic analysis based on the finite-element method (FEM) was made. The numerical results show that the stress field of the fracture region is caused by a complex stress state and the cleavages are significantly affected by the pulsed laser. A clean cut of the soda-lime glass substrate could be obtained due to a large shear stress state on the cutting direction with the pulsed laser radiated on the glass substrate.     

Development of XUV lasers at the RAL Central Laser Facility

Recent progress in the development of XUV lasers by research teams using high-power and ultrashort-pulse Nd: glass and KrF laser facilities at the Rutherford Appleton Laboratory is reviewed. Injector-amplifier operation and prepulse enhanced output of the Ge XXIII collisional laser driven by a kilojoule glass laser, enhanced gain in CVI recombination with picosecond CPA drive pulses from a glass laser, and optical field ionization and XUV harmonic generation with a KrF CPA laser are described.     

Features of Laser Through-Cutting of Silicate Glass by a Fiber Ytterbium Laser

Some principal aspects of silicate glass cutting by controlled laser through thermal cleavage are considered. In particular, it is shown that the cutting speed in the case of ytterbium fiber laser radiation with a wavelength of 1.065 μm lying in fact in the glass transmission range (more precisely, in the low absorption region) depends linearly on the laser power. It is shown that the glass end face takes various geometrical shapes under various conditions of bulk heating and cooling. Therefore, to obtain a homogeneous end face, it is required to stabilize both the laser radiation power and the laser beam speed at a corresponding laser beam geometry in the cut region. Methods for obtaining various cross section shapes of the glass end face and methods for obtaining blunt edges of end faces are presented.     

Temperature prediction for CO2 laser heating of moving glass rods

This paper presents a heat transfer model to calculate the temperature field in moving glass rods heated by a CO₂ laser. Conduction and radiation heat transfer in radial and axial directions are taken into account in the current model. The Rosseland diffusion approximation is incorporated to analyze the radiation heat transfer in the glass rod. A two-band model is used to simulate the spectral property of the glass. Results of the simulation show that glass rods of sufficiently large optical thickness should be treated as a semitransparent medium for radiative transfer, and it is reasonably accurate to assume it to be opaque to CO₂ laser irradiation. It has been shown that the resulting temperature profile is strongly dependent on the laser parameters, i.e., the size of laser beam and the power of the laser. The diameter and speed of the moving glass rod are also important in determining the temperature field although the convective heat transfer coefficient between the glass rod and the environment has little effect.     

多普勒振镜正弦调制多光束激光外差测量玻璃厚度的方法

本文提出了一种多普勒振镜正弦调制多光束激光外差测量玻璃厚度的新方法. 基于激光外差技术和多普勒效应, 通过做简谐振动的多普勒振镜对不同时刻入射光的频率进行正弦调制, 把待测厚度信息加载到外差信号的频率差中, 通过快速傅里叶变换对外差信号解调后可以同时得到多个待测玻璃厚度值, 经加权平均处理可以提高待测厚度的测量精度. 利用这种新方法, 通过MATLAB仿真测量了不同玻璃厚度值, 结果表明：该测量结果的最大相对误差小于0.008%.     

基于ANSYS的脉冲激光辐照石英玻璃的温度场数值模拟

采用有限元仿真软件ANSYS 12.0对脉冲功率激光辐照石英玻璃建立了热力学模型,对其表面温度场进行了数值模拟,得到了在不同激光功率密度下的瞬态温度场分布,并对模拟结果进行了分析和研究,为激光辐照石英玻璃实验提供依据.     

大口径激光玻璃光学加工的质量控制

大口径激光玻璃光学加工的特点是加工指标要求高、难度大,加工周期长,而质量控制是保障大口径激光玻璃光学加工质量满足要求和促进工艺进步的管理手段。从质量控制和质量管理的角度出发,阐述了在大口径激光玻璃光学加工中质量控制的特点和质量控制的方法,其目的是通过流程检验和控制,人员、设备、物料管理,环境管理,以及先进的质量控制和分析方法的应用来提高加工的质量稳定性和合格率。实践证明:在大口径激光玻璃光学加工中推行质量管理,产品的合格率和加工效率得到了较为显著的提高。     

Effect of thermal stresses on chip-free diode laser cutting of glass

In laser cleaving of brittle materials using controlled fracture technique, thermal stresses are used to induce a crack and the material is separated along the cutting path by extending this crack. In this study, a glass sheet is stressed thermally using a 808-940 nm diode laser radiation. One of the problems in laser cutting of glass with controlled fracture technique is the cut deviation at the leading and the trailing edges of the glass sheet. In order to avoid this damage it is necessary to understand the stress distributions which control crack propagation. A study is conducted here to analyse the cut deviation problem of glass by examining the stress fields during diode laser cutting of soda-lime glass sheets. Optical microscope photographs of the breaking surface are obtained to examine the surface quality and cut path deviation while the latter is explained from the results of the stress fields which are obtained from a finite element simulation.     

Fifty percent internal slope efficiency femtosecond direct-written Tm³⁺:ZBLAN waveguide laser

We report a 790 nm pumped, Tm3? doped ZBLAN glass buried waveguide laser that produces 47 mW at 1880 nm, with a 50% internal slope efficiency and an M2 of 1.7. The waveguide cladding is defined by two overlapping rings created by femtosecond direct-writing of the glass, which results in the formation of a tubular depressed-index-cladding structure, and the laser resonator is defined by external dielectric mirrors. This is, to the best of our knowledge, the most efficient laser created in a glass host via femtosecond waveguide writing.     

Experimental and numerical study of mechanism of glass modification process by continuous-wave laser backside irradiation (CW-LBI)

The modification of transparent materials using a femtosecond laser has been studied. We previously proposed a new method of modifying glass using a continuous-wave laser, named continuous-wave laser backside irradiation (CW-LBI), in which CW laser illumination induces a change in the refractive index without cracking the glass. In this study, we investigated the process of glass modification by CW-LBI using time-lapsed imaging and by calculation of the temperature. First, the modification of glass was observed by the shadowgraph method, and it was found that thermal radiation was included in the phenomena that occurred when the glass was modified. Second, the time-lapsed temperature distribution was calculated. The temperature distribution was roughly in accordance with the shape of the modified area observed in the shadowgraphs. We concluded that the radius of the modified area is dependent on the temperature reached in the glass.     

Fabrication of glass micro-prisms using ultra-fast laser pulses with chemical etching process

In this study, a new process of glass micro-prism structures is investigated by an ultra-fast laser irradiation with chemical etching process. The ultra-fast laser is employed by an all-in-one femtosecond laser (FS-laser) system with the amplifier as an excitation source for patterning the structures. Here, the center wavelength of laser is frequency-doubled to 517 nm. Besides, the repetition rate and pulse width of laser are 100 kHz and 350 fs, respectively. First, the embedded gratings of glass with different pitches can be fabricated using a FS-laser process. Afterwards, the glass samples are placed in the hydrofluoric acid (HF) solution for 15 min to develop structures. Finally, the results of this study demonstrated that the V-cut micro-prisms are successfully formed by controlling etching concentration between intrinsic glass material and modified areas.     

Excimer laser-assisted annealing of silicate glass with ion-synthesized silver nanoparticles

The effect of KrF excimer laser radiation on a composite layer consisting of sodium-potassium silicate glass with silver nanoparticles is studied as a function of the number of laser nanosecond pulses. The silver nanoparticles are synthesized by ion implantation. The measured optical absorption of the composite layer demonstrates that the silver nanoparticle size decreases monotonically as the number of laser pulses increases. Rutherford backscattering shows that laser annealing is accompanied by silver diffusion into the bulk of the glass and partial metal evaporation from the sample surface. The detected decrease in the silver nanoparticle size is discussed in terms of simultaneous melting of silver nanoparticles and the glass matrix due to the absorption of laser radiation.     

Fabrication of an integrated Raman sensor by selective surface metallization using a femtosecond laser oscillator

We demonstrate that a Raman sensor integrated with a micro-heater, a microfluidic chamber, and a surface-enhanced Raman scattering (SERS) substrate can be fabricated in a glass chip by femtosecond laser micromachining. The micro-heater and the SERS substrate are fabricated by selective metallization on the glass surface using a femtosecond laser oscillator, whereas the microfluidic chamber embedded in the glass sample is fabricated by femtosecond laser ablation using a femtosecond laser amplifier. We believed that this new strategy for fabricating multifunctional integrated microchips has great potential application for lab-on-a-chips.     

Internal modification of glass by ultrashort laser pulse and its application to microwelding

Internal modification process of glass by ultrashort laser pulse (USLP) and its applications to microwelding of glass are presented. A simulation model is developed, which can determine intensity distribution of absorbed laser energy, nonlinear absorptivity and temperature distribution at different pulse repetition rates and pulse energies in internal modification of bulk glass with fs- and ps-laser pulses from experimental modified structure. The formation process of the dual-structured internal modification is clarified, which consists of a teardrop-shaped inner structure and an elliptical outer structure, corresponding to the laser-absorbing region and heat-affected molten region, respectively. Nonlinear absorptivity at high pulse repetition rates increases due to the increase in the thermally excited free electron density for avalanche ionization. USLP enables crack-free welding of glass because the shrinkage stress is suppressed by producing embedded molten pool by nonlinear absorption process, in contrast to conventional continuous wave laser welding where cracks cannot be avoided due to shrinkage stress produced in cooling process. Microwelding techniques of glass by USLP have been developed to join glass/glass and Si/glass using optically contacted sample pairs. The strength of the weld joint as high as that of base material is obtained without pre- and post-heating in glass/glass welding. In Si/glass welding, excellent joint performances competitive with anodic bonding in terms of joint strength and process throughput have been attained.     

Aluminum thin film enhanced IR nanosecond laser-induced frontside etching of transparent materials

Laser processing of glass is of significant commercial interest for microfabrication of precision optical engineering devices. In this work, a laser ablation enhancement mechanism for microstructuring of glass materials is presented. The method consists of depositing a thin film of aluminum on the front surface of the glass material to be etched. The laser beam modifies the glass material by being incident on this front-side. The influence of ablation fluence in the nanosecond regime, in combination with the deposition of the aluminum layer of various thicknesses, is investigated by determining the ablation threshold for different glass materials including soda-lime, borosilicate, fused silica and sapphire. Experiments are performed using single laser pulse per shot in an air environment. The best enhancement in terms of threshold fluence reduction is obtained for a 16 nm thick aluminum layer where a reduction of two orders of magnitude in the ablation threshold fluence is observed for all the glass samples investigated in this work.     

Glass modification by continuous-wave laser backside irradiation (CW-LBI)

We report on a permanent change in the physical properties inside glass that is rapidly heated and quenched with a continuous-wave (CW) laser beam. The absorption of the glass was enhanced by laser heating, and the heated spot moved by thermal radiation and conduction. To trigger the heating, an absorbent material was placed on the backside of a glass plate and irradiated through the glass. The laser beam can modify borosilicate glass with a high aspect ratio (∼100:1) at a rate of ∼130 mm/s. The modified zone consists of two concentric cylindrical zones and is crack-free.