Fiber laser welding of austenitic steel and commercially pure copper butt joint

The fiber laser welding of austenitic stainless steel and commercially pure copper in butt joint configuration without filler or intermediate material is presented. In order to melt stainless steel directly and melt copper via heat conduction a defocused laser beam was used with an offset to stainless steel. During mechanical tests the weld seam was more durable than heat affected zone of copper so samples without defects could be obtained. Three process variants of offset of the laser beam were applied. The following tests were conducted: tensile test of weldment, intermediate layer microhardness, optical metallography, study of the chemical composition of the intermediate layer, fractography. Measurements of electrical resistivity coefficients of stainless steel, copper and copper–stainless steel weldment were made, which can be interpreted or recalculated as the thermal conductivity coefficient. It shows that electrical resistivity coefficient of cooper–stainless steel weldment higher than that of stainless steel. The width of intermediate layer between stainless steel and commercially pure copper was 41–53 µm, microhardness was 128–170 HV_0.01.     

Investigation of the Thermal Stability of Laser Nitrided Iron and Stainless Steel by Annealing Treatments

Laser nitriding has revealed to be a very promising and effective treatment to improve the technical properties, like surface hardness and corrosion-wear resistance, of iron and steels. The high nitrogen concentration, the fastness and precision of the treatment and the easy experimental setup make this technique very suitable for applications on industrial scale. Samples of pure iron and austenitic stainless steel have been irradiated with ns laser pulses in the UV radiation range and analyzed by means of Conversion Electron Mössbauer Spectroscopy (CEMS), Resonant Nuclear Reaction Analysis (RNRA), Grazing Incidence X-Ray Diffraction (GXRD) and Microhardness. Mössbauer Spectroscopy, in particular, is capable of detecting the phase composition of the nitrided layer and therefore represents an essential tool for these kind of analysis. The thermal stability of the treated samples have been investigated by subsequent annealings at increasing temperatures in vacuum and in air. For iron samples the annealing treatment at 250°C shows a rather drastic phase transformation from phase (fcc) into (Fe₄N) while a strong depletion of N has been observed for 400°C or higher, regardless of the ambient pressure (atmospheric or vacuum). On the other hand, the stainless steel shows a very good thermal stability up to 500°C, but higher temperatures induce a gradual decrease in the nitrogen concentration which seems to be a common feature for both pure iron and stainless steel. Furthermore, annealing in air leads to the formation of a thin oxide layer on the surface of the iron sample which is easily characterized by Mössbauer spectroscopy.     

Combined bulk and laser heat treatment for optimizing the structure and phase composition of high-speed steels

The influence of laser radiation on the formation of an austenitic grain and on the alloying ability of a solid solution of high-speed cutting steels is investigated using as an example the steel R18 subjected beforehand to various bulk heat treatments. Notice is taken of the role of laser tempering during the initial stage of heating to the temperature at which an austenitic transformation with release of secondary carbides takes place, accompanied by laser action of plastic de formation with formation of a corresponding structurally stressed state. The content, in the solid solution, of the main alloying element tungsten in the R18 high-speed steel is determined from Mössbauer measurements and from x-ray phase analysis data on the degree of the dissolution of the carbide phase in laser-action zone. Determination of the carbon content in the solid solution of the zones of laser action, yields data on the degree of the carbide-phase solution and on the displacement of the diffraction -lines; these data can be attributed to anomalous diffusion of the carbon as the laser heating is accelerated.Quantum Physics Division, Kuibyshev Branch. Translation of Preprint No. 19, Lebedev Institute of Physics, Academy of Sciences of the USSR, Moscow, 1991.     

The characteristics of laser micro drilling using a Bessel beam

A Bessel beam is suitable for laser micro-fabrication because it possesses both a micron-sized focal spot and a deep focal depth. As the influence of focusing aberrations is much smaller than that of a convex lens, the generation of a Bessel beam using an axicon is very practical. In the case of laser micro drilling of austenitic stainless steel with a Bessel beam, suitable processing conditions were investigated. The threshold fluence to make a through hole increased with an increase in the sample thickness. For samples with the same thickness, the threshold fluence increased with an increase in the crossing angle. A small crossing angle Bessel beam can drill a deep hole with a small threshold fluence. A through hole with a diameter smaller than 10 μm can be made on a stainless steel sheet 20 μm thick by using a Bessel beam with a large crossing angle. The taper of the hole drilled with the Bessel beam is smaller than that with the focused beam from the convex lens. PACS 52.38.Mf; 42.62.Cf; 42.79.Bh     

Evolution of magnetic phase at low aging temperature in a heavily cold-drawn stainless steel fiber

The evolution of the magnetic phase upon aging at 300–520 °C in a heavily cold-drawn AISI 316L austenitic stainless steel fiber was studied using thermomagnetic analysis (TMA) and magnetic force microscopy with a heating stage. An increasing trend of magnetization from 50 °C to around 470 °C in the heating curves of TMA in austenitic stainless steels after a cold-drawing process was observed. No significant M_s temperature signal in the TMA curve at cooling indicated an increase in magnetization upon cooling period without significant phase transformation. A series of in situ magnetic force microscopy observations reveal a growth of the magnetic domain structure after aging at 300 °C for 2.5 h. Results show that the ferromagnetic increase during aging at lower annealing temperature resulted from the growth of martensite.     

The annealing behavior of implanted nitrogen in fcc stainless steel

Post-implantation annealing of N-implanted 304 stainless steel at 400 °C has been investigated by conversion electron Mössbauer spectroscopy, X-ray diffraction and Auger electron spectroscopy. After a 1 h anneal, the near complete dissolution of the as-implanted Fe₂N-like nitride phase results in a 9 at.% N fcc solid-solution phase. After the final anneal (64 h), N has diffused to a depth of about 2 m and remains in solid solution with an average content of 4 at.%. An average N diffusion coefficient at 400 °C is estimated to be 10^-12-10^-14 cm²/s, depending on anneal time, too small to explain the deep penetration observed in high-flux, high-dose N-implanted stainless steel. The present results provide additional evidence for beam controlled N migration where Cr plays an important role.     

Efficient multiple-longitudinally diode laser pumped Nd:YAG slab laser

The operation of an eightfold longitudinally diode laser pumped 1.06m cw Nd:YAG slab laser is demonstrated. The 809 nm diode radiation is focused through a dichroic coating into each laser channel starting from the reflection points of the 1.06m beam in the slab crystal. At an absorbed pump power in the crystal of 2830 mW a maximum cw TEM₀₀ output of 1075 mW was achieved with a corresponding slope efficiency of 42.5%.     

Alternate intensity modulation of a dual-wavelength He−Ne laser for differential absorption measurements

A simple method is demonstrated for internal intensity modulation of the 3.391 and 3.392-m emissions of a He–Ne laser with equal amplitudes and 180° out of phase to each other. A modulation amplitude of 0.7 mW peak-to-peak at 1kHz for the individual emissions has been obtained from a laser plasma tube 50 cm long while maintaining the total-intensity modulation as low as 0.25 W for a signal averaging time of 1 s. This laser source can greatly simplify the setup and improve the sensitivity of differential absorption measurements for the methane remote sensing.     

Strain Hardening and Fracture of Austenitic Steel Single Crystals with High Concentration of Interstitial Atoms

Stages in the flow curves, mechanisms of deformation (slip or twinning), evolution of the dislocation structure and fracture are studied in austenitic stainless steel single crystals alloyed with nitrogen (C _N = 0–0.7 wt. %) and Hadfield steel in relation to the orientation of the crystal axis of tension, test temperature, and atomic concentrations of nitrogen and carbon. The dislocation-structure pattern (cellular or planar) and deformation mechanisms (slip or twinning) are shown to depend on the matrix stacking-fault energy _sf, friction forces due to solid-solution hardening by interstitial atoms, and crystal orientation. An interrelation between the stages in the flow curves and the type of dislocation structure is found. The contribution of mechanical twinning to the plastic flow of steel crystals is shown to increase with increase in nitrogen and carbon concentrations. The mechanical twinning develops in the early stages of deformation and determines the strain-hardening coefficient and fracture of crystals in high-strength states for interstitial atomic concentration C 0.5–0.7 wt. %. High deforming stresses due to solid-solution strain hardening by interstitial atoms of nitrogen and carbon in combination with low _sf are found to result in twinning in the <001> orientations. The values of _sf in Hadfield steel single crystals and in austenitic stainless steel single crystals are found experimentally depending on the concentration of nitrogen atoms and test temperature.     

Measurement of the bead profile and microstructural characterization of a CO2 laser welded AISI 904 L super austenitic stainless steel

Laser welding of AISI 904 L super austenitic stainless steel using a diffusion cooled slab 3.5 kW CO₂ laser and employing two different shielding gases, namely argon and helium, was carried out. The laser weld bead profile depends on various parameters such as beam power (BP), travel speed (TS) and focal position (FP) of the laser spot. These parameters have to be selected suitably to obtain the desirable output. The cross sectioned area of the bead profiles measured using an optical microscope to determine the bead width and depth of penetration. X-ray diffraction used for phase identification confirmed that the weld structure was fully austenitic and dendritic. Hardness was observed to increase in the weld bead with respect to the parent metal and it was related to the microstructural refinement induced by a rapid cooling of the weld zone.     

Near Field Observation of a Refractive Index Grating and a Topographical Grating by an Optically-Trapped Gold Particle

We observed the near field for a refractive index grating fabricated on a planar light waveguide circuit (PLC) by scanning an optically-trapped 100 nm diameter gold particle. We demonstrate that stable trapping and scanning occur with a Gaussian laser beam at the scan velocity of 1.6 m/s and Nd:YAG laser power of 25mW. The scattered Ar laser light from the gold particle is strong at high refractive indexes of the grating with periods of 1.06 m and 0.53 m both by s and p polarized illumination. In addition, we observed the surface profile of the optical disk tracking groove with and without the gold particle. © 2004 The Optical Society of Japan     

Relativistic filamentation of laser beams in plasma

We describe the results of a numerical code which models the relativistic selffocussing of high-intensity laser beams in plasmas by the nonlinear relativistic dependence of the optical constants on laser intensity. The plasma dynamics of 10¹³ W Nd glass lasers of 30 m initial beam diameter in nearly cut-off density plasmas is followed for a few picoseconds interaction time and 25 m depth into the plasma. Rapid relativistic selffocussing down to a beam diameter of one micron in a distance of the order of the original beam diameter is observed, as well as the production of GeV ions moving against the laser light.     

Blow-off of aluminium films

The blow-off of Al targets from a transparent support by single pulses of intense laser irradiation through the support is investigated for target thicknesses up to some m. The blow-off process is theoretically described by calculations of the phase front dynamics in the target, adopted from Harrach's analytical solutions for laser heating and burnthrough of opaque solid slabs. Experimentally two laser beam sources were used: a Nd:YAG laser with a Gaussian intensity profile and a Nd:Glass-laser system with a homogenized flat-top profile. Two types of removal mechanism could be identified. In the first mode (low laser intensities and/or thin targets) the target is completely molten and can easily be blown-off by the vapor originating at the target-support interface. In the second mode (high laser intensities and/or thick targets) superheating of the liquid Al or a burst of the remaining solid layer of the target occurs. In both cases in the second mode the blow-off process is characterized by higher vapor pressures.     

飞秒激光烧蚀0Cr18Ni9不锈钢精度的影响因素

为了研究影响飞秒激光烧蚀0Cr18Ni9不锈钢精度的因素,采用飞秒激光对0Cr18Ni9不锈钢进行了切割和打孔实验。利用光学显微镜、光学金相显微镜等设备,对不锈钢烧蚀区形貌和切缝显微组织进行检测,基于烧蚀过程中CCD实时采集到的不锈钢表面的激光光斑图样,采用COMSOL Multiphysic数值模拟软件,模拟了烧蚀过程中激光束的发散传播行为,并计算了光束发散角。结果表明:当激光重复频率为5kHz时,厚度为160μm的0Cr18Ni9不锈钢切缝和孔边缘被明显烧黑,切缝处晶粒明显长大,存在热影响区;烧蚀过程中,由飞秒激光超高功率密度所致的金属-空气混合等离子体使光束沿传播方向上发生散射,发散角在6°～10°之间。热影响区的存在和混合等离子体的行为是影响飞秒激光烧蚀0Cr18Ni9不锈钢精度的主要因素。     

A diode-laser pump source with small focus diameter for end- pumped systems

A pump source with eight angular multiplexed laser diodes is built. The diode laser emission is collimated and focused using relatively inexpensive aspherical lenses. The maximum output power is 6.3W at 970nm. The overall transmittance of the beam shaping optics is T=85%. The electrical, temporal and spectral properties are studied. The variances of the spatial intensity distribution are r0x=99m and r0y=85m. The beam propagation factors are M2x=38 and M2y=112. The high intensity in the focus makes this system ideal for end pumping of solid state lasers.     

Investigation of a highly saturated soft X-ray amplification in a capillary discharge plasma waveguide

The characterization of the laser beam intensity distribution of a highly saturated 46.9-nm soft X-ray laser excited by capillary discharges is reported. The laser produces a total output energy of 300 J/pulse by amplification in plasma channels having lengths up to 0.45 m. A regime of laser amplification, which is almost free from the effect of the refraction defocusing, is experimentally determined. This regime produces a soft X-ray laser beam with an intense sub-milliradiant component. In the longer active medium the laser intensity distribution reaches the divergence of 0.6 mrad, which approaches the limit of diffraction. A comparison of the experimental results with the simulations performed with a ray-tracing code shows that the small divergence of the beam could be attributed to the effect of a weak index waveguiding of the laser beam through the long plasma channels. PACS 42.55.Vc; 42.60.Jf     

A highly efficient 5 kW peak power Nd:YAG laser with time-shared fiber optic beam delivery

Here, we report on the development of an efficient, high peak power lamp pumped Nd:YAG laser with time-shared fiber optic beam delivery. A maximum average output power of 270 W with 100 J maximum pulse energy and 5 kW peak power has been achieved with an electrical to laser conversion efficiency of 5.4%, which is on higher side for typical lamp pumped solid-state lasers. We have improved efficiency by spectral conversion and water flow optimization in the pump cavity, with a resulting beam quality comparable to commercial systems of similar power level. The resonator has been designed for stable operation from single-shot to 200 Hz repetition rate. A study of pulse-to-pulse laser energy stability for different resonator configurations has also been performed. The resonator was designed to achieve a good beam quality for the whole range of operation with a maximum beam parameter product of 15 mm mrad (M²45). A simple mechanism for time-shared fiber optic port selection has also been devised. Material processing applications such as cutting of stainless steel sheets up to 14 mm thickness and welding of metals such as carbon steel with weld depths up to 2 mm using the developed laser system has also been reported.     

Optical properties of a new IR converter for laser beam analysis

This work presents the temporal and spacial resolution of a new infrared (IR) converter based on thermal radiation emission. Using this converter, it is possible to measure the intensity distribution of laser beams with a wavelength between 1 and 20 μm. For this purpose, the laser radiation (for example, 10.6 μm) is converted into a wavelength coverage of 800–1100 nm. In the actual converter thin metal foils provide the basis of this method. The metal foils are heated to a temperature of 600–800 K. The emitted radiation of the foils defers into the near-infrared (NIR) area, thus enabling detection by camera systems based on silicate. Additional heat input of the laser results in a local temperature increase, and then the increase in radiation intensity can be measured. Typical thicknesses of converter metal foils are <5μm. Foil materials with a low thermal conductivity, good absorption of the measured laser beams, and a high melting temperature are particularly suitable. These parameters are well shown by using stainless steels, such as INOX (stainless steel 1.4310 CrNi steel). Using this material, it is possible to gain a maximum spatial resolution of 250 μm and a temporal resolution of 12.5 Hz, by a measurement range from 1 to 100 W/cm². The maximum measured intensity is 125 W/cm².     

Phase transformations induced by implantation of12C− ions into α-Fe and AISI 304 and 316 stainless steels studied by CEMS and SEM

Samples of AISI 304 and 316 stainless steels, initially in austenitic (first set) and martensitic states (second set) and -Fe (third set), were implanted with 180 keV¹²C^– to a dose of 10¹⁷ atoms/cm² at room temperature. Surfaces were examined by SEM (scanning electron microscopy) and the crystalline-phase fractions were estimated through CEMS (conversion electron Mössbauer spectroscopy). Different grades of etching were produced by sputtering during the implantations on the stainless steel samples depending on the previous crystallographic states. CEMS data reveal the transformation in the initially martensitic samples and no noticeable modifications as a result of the implantation on -Fe and austenitic samples.     

CO2 laser heating of surfaces: Melt pool formation at surface

The melt pool formation during the heating of titanium and steel surfaces by a moving CO₂ laser beam is examined. The repetitive pulses are introduced in the simulations and the Marangoni effect in the melt pool is incorporated in the model study. The influence of laser scanning speed and the laser intensity parameter on the melt pool size is also considered. The enthalpy–porosity method is adopted to account for the phase change in the irradiated spot. It is found that the influence of laser scanning speed on the melt pool size is considerable, which is more pronounced for laser beam parameter β=1. The melt pool size is smaller for stainless steel as compared to that corresponding to titanium.