实现材料高应变率拉伸加载的爆炸膨胀环技术

设计了新型的爆炸膨胀环实验加载装置,加载装置中采用爆炸丝线起爆方式,避免了传统装置中对碰爆轰波加载时的应力不均匀性。利用新型的爆炸膨胀环实验技术研究了无氧铜材料的动态性能,利用激光位移干涉仪测量了试样环的径向速度历史,处理数据获得了无氧铜材料的流动应力-塑性应变-应变率的关系,为进一步利用爆炸膨胀环实验技术研究材料在高应变率拉伸加载时的本构关系奠定了基础。     

膨胀环受力历史对应力应变关系的影响

利用两类实验装置开展了无氧铜TU1膨胀环实验研究,发现:电磁膨胀环在加载阶段,样品受体力作用,满足均匀变形的假定;而爆炸膨胀环在加载阶段,样品内壁受面力冲击作用,不满足均匀变形的假定。针对这个差异,发展了一种考虑冲击阶段变形不均匀性的新方法,利用回收样品几何变形,将冲击阶段试样环内轴向塑性应变、径向塑性应变纳入等效塑性应变的计算中,通过修正后的方法更准确地获得了材料的应力应变关系。     

爆炸膨胀环的截面尺寸效应

利用爆炸膨胀环实验数据修正了无氧铜的J-C本构模型参数,计算获得的速度历史与实验测试结 果吻合。通过数值模拟研究了膨胀环宽度对速度历史、应力状态的影响,发现:对厚度1mm 的膨胀环,加载 速度峰值随着膨胀环宽度的增加而增加,当宽度超过8mm 后速度峰值不再变化;膨胀环宽度不超过2mm 时,能较好满足1维应力状态的假定。膨胀环的应力状态在一定范围内具有明显的尺寸效应,可为爆炸膨胀 环的试样尺寸设计提供参考。     

爆炸膨胀环实验技术初步研究

为避免对碰爆轰波加载时的应力不均匀性,初步建立了爆炸丝线起爆方式的爆炸膨胀环实验技术。长度为200mm、直径为0．175mm的铜丝爆炸同步性小于0．2μs,基本实现了同步起爆粉末泰安炸药,通过膨胀环实验初步获得无氧铜试样环的膨胀速度历史,为进一步利用爆炸膨胀环实验研究材料的高应变率拉伸加载时的本构关系奠定了基础。     

液压膨胀环恒应变率加载技术

膨胀环实验技术主要包括爆炸膨胀环实验技术和电磁膨胀环实验技术,实验过程中膨胀环的加载应变率在达到峰值后会随着圆环的膨胀而迅速降低,给研究应变率敏感材料的拉伸碎裂带来极大的不便。在前期提出的液压膨胀环实验技术的基础上,发展了一种恒应变率加载技术。首先,从理论上获得了实现金属圆环恒应变率膨胀所需的液压加载曲线的近似表达式;然后,采用有限元流固耦合数值模拟了液压膨胀环装置中1060-O铝环的膨胀碎裂过程,在给定液压加载曲线下,膨胀环的环向应变率在应变率稳定阶段上下波动范围最大不超过20%;并进一步研究了加载曲线对碎裂过程中应变率的影响规律。在液压膨胀环实验装置上对1060-O铝环开展了膨胀环实验,验证了恒应变率加载技术的可行性。     

Y态TU1环的动态脆性碎裂特性

针对膨胀环的碎裂问题,以Mott碎裂理论和Grady能量平衡理论为基础,利用裂纹张开位移碎裂模型（crack opening displacement model,COD）描述脆性无氧铜环的碎裂特性,并推导了碎片尺寸和数目表达式。利用电磁膨胀环加载技术,完成了不同应变率的脆性无氧铜（TU1）环碎裂实验,实验结果与理论计算结果符合较好,可为脆性金属环膨胀碎裂特性描述提供参考。     

爆炸与电磁加载下无氧铜环、柱壳的断裂模式转变

考虑断面收缩率、局域断裂应变以及平均断裂应变,并基于电磁膨胀环、爆炸膨胀环(柱壳)实验平台,研究了高纯无氧铜(TU1)环及柱壳在高应变率载荷下的膨胀断裂行为。采用高速摄影技术拍摄柱壳外壁的膨胀断裂形貌演化过程,用于确定柱壳平均断裂应变;利用激光干涉测速技术获得样品径向膨胀速度历史,用于确定加载应变率;利用样品的全回收测量及微观表征,确定了无氧铜环、柱壳的局域断裂应变及断裂模式。实验表明,随着应变率的增加,TU1材料的平均断裂应变增加,断面的收缩程度加剧,并在应变率约为1.0×104 s-1附近会出现明显的断裂模式转变,断面收缩率出现量级上的跳跃,从100变化至约103,局域断裂应变呈现明显的分区现象。     

一维快速拉伸下无氧铜的动态断裂与破碎

利用电磁膨胀环技术对无氧铜环进行了不同加载电压下的动态拉伸实验。对无氧铜在破碎前出现塑性失稳多重颈缩进行了初步分析,利用能量平衡的破碎理论给出了无氧铜环的破碎分布。三维数值模拟结果表明,颈缩区温升比非颈缩区高,且多重颈缩在环周上的分布服从泊松分布。     

PBX炸药本构关系的实验研究

在SHPB装置上开展了某典型PBX炸药的单轴压缩、间接拉伸实验。利用入射波整形技术,结合 半导体应变片和石英晶体联合测试的方法,实现了PBX炸药的应力平衡和恒应变率加载,得到了不同应变率 下某PBX炸药的压缩应力应变曲线,初步建立了该炸药的修正Sargin唯象模型;开展了3种PBX炸药的动 态巴西实验,通过高速摄影获得了炸药的破坏过程,结合数字相关技术,获得了试样裂纹附近的应变场分布, 初步建立了描述3种炸药动态拉伸行为的修正Johnson-Cook模型。模型曲线与实验结果符合较好。     

玻纤增强复合材料高应变率拉伸实验研究

利用爆炸膨胀环实验技术,对玻璃纤维增强复合材料(GFRC)进行了高应变率(104s-1)下力学性能研究。实验中使用铜丝汽化引爆装药的方法对驱动环进行能量加载,并采用激光速度干涉仪(VISAR)测量试样环自由膨胀的质点速度,实现了玻璃纤维增强复合材料在104应变率下的一维拉伸破坏,并获取了该材料的速度时间曲线。经过计算得到了材料的应力应变关系,最后与该材料在准静态下、中高应变率下实验得到的数据进行了比较。     

(Q)SAR modelling of nanomaterial toxicity: A critical review

There is increasing recognition that some nanomaterials may pose a risk to human health and the environment. Moreover, the industrial use of the novel engineered nanomaterials (ENMs) increases at a higher rate than data generation for hazard assessment; consequently, many of them remain untested. The large number of nanomaterials and their variants (e.g., different sizes and coatings) requiring testing and the ethical pressure towards nonanimal testing means that in a first instance, expensive animal bioassays are precluded, and the use of (quantitative) structure–activity relationships ((Q)SARs) models as an alternative source of (screening) hazard information should be explored. (Q)SAR modelling can be applied to contribute towards filling important knowledge gaps by making best use of existing data, prioritizing the physicochemical parameters driving toxicity, and providing practical solutions for the risk assessment problems caused by the diversity of ENMs. This paper covers the core components required for successful application of (Q)SAR methods to ENM toxicity prediction, summarizes the published nano-(Q)SAR studies, and outlines the challenges ahead for nano-(Q)SAR modelling. It provides a critical review of (1) the present availability of ENM characterization/toxicity data, (2) the characterization of nanostructures that meet the requirements for (Q)SAR analysis, (3) published nano-(Q)SAR studies and their limitations, (4) in silico tools for (Q)SAR screening of nanotoxicity, and (5) prospective directions for the development of nano-(Q)SAR models.     

流变学研究的若干问题

本文综述了1988年8月第10届国际流变学会议部分大会邀请报告及分组报告的下列几个领域内容:①分子动力学;②光学流变测量;⑧血液的动态测量;④数值仿真;⑤钻探油井;⑥强化采油;⑦减阻;⑧聚合物挤压成形加工;⑨食品流变学.     

On the boundedness and the stability properties of solution of certain fourth order differential equations

This paper investigates equation(1)in two cases:(i)P≡0,(ii)P(≠O)satisfies|P(t,x,y,z,ω)|≤(A |y| |z| |ω|)q(t),where q(t)is a nonnegative function of t.For case(i)the asymptotic stability in the large of the trivial solution x=0 is investigatedand for case(ii)the boundedness result is obtained for solutions of equation(1).Theseresults improve and include several well-known results.     

Overview of Identification Methods of Mechanical Parameters Based on Full-field Measurements

This article reviews recently developed methods for constitutive parameter identification based on kinematic full-field measurements, namely the finite element model updating method (FEMU), the constitutive equation gap method (CEGM), the virtual fields method (VFM), the equilibrium gap method (EGM) and the reciprocity gap method (RGM). Their formulation and underlying principles are presented and discussed. These identification techniques are then applied to full-field experimental data obtained on four different experiments, namely (i) a tensile test, (ii) the Brazilian test, (iii) a shear-flexural test, and (iv) a biaxial test. Test (iv) features a non-uniform damage field, and hence non-uniform equivalent elastic properties, while tests (i), (ii) and (iii) deal with the identification of uniform anisotropic elastic properties. Tests (ii), (iii) and (iv) involve non-uniform strain fields in the region of interest. Working group “Identification” of the French CNRS research network (GDR 2519) “Mesures de champs et identification en Mécanique des Solides / Full-field Measurements and Identification in Solid Mechanics”.     

国内非牛顿流体力学进展

非牛顿流体;;本构方程;;流变测量;;流动稳定性;;收缩流动;;聚合物加工;;石油工业;;生物流体力学     

On (g, f)-factorizations of graphs

I.IntroductionLetGbeafinitegraph(withoutloops),V(G)andE(G)bethevenicessetandedgesset,respectively.Foreachxos(G),wedenotebydo(x)thedegreeofxinG.Letg,fbetwononnegativeinteger-valuedfunctionsdefinedonV(G)andg相似文献   

Synthesis of submicron-sized composite particles with unique morphology by emulsifier-free seeded emulsion copolymerization

Polystyrene （PSt） microspheres with diameter of 375 nm to be used as the seeds for seeded emulsion polymerization were prepared via emulsion polymerization using potassium persulfate （KPS） as initiator in ethanol-water mixed solvents. Emulsifier-free seeded emulsion copolymerization of styrene （St） with acrylonitrile （AN） was carried out in the presence of poly（ethylene glycol） monomethoxymonomethacrylate （PEGm） macromonomer as reactive stabilizer and 2,2＇-azobisisobutyronitrile （AIBN） as initiator to obtain submicron-sized PEGm graft poly（styrene-coacrylonitrile） （PEGm-g-PSAN） composite particles with unique morphology. Scanning electron microscopy （SEM） indicated that St and AN together contributed to forming the unusual morphology. The concentration of St and AN, total monomer concentration, initiator type and the monomer adding method remarkably affected the morphology of the composite polymer particles.     

Computerized Developments in Design,Generation, Simulation of Meshing,and Stress Analysis of Gear Drives

The paper represents new computerized developments in design, generation, simulation of meshing, and stress analysis of gear drives. The main contents of the paper are: (i) application of a predesigned parabolic function of transmission errors for reduction of noise, (ii) computerized simulation of noise caused by transmission errors, (iii) modification of the basic algorithm of tooth contact analysis, and (iv) application of approaches developed for enhanced design and simulation of meshing of the following gear drives: (a) spiral bevel gear drives, (b) face-gear drives (including an approach for grinding), and (c) modified helical gear drives. The developed theory is illustrated with numerical examples.     

Synthesis of submicron-sized composite particles with unique morphology by emulsifier-free seeded emulsion copolymerization

Polystyrene (PSt) microspheres with diameter of 375 nm to be used as the seeds for seeded emulsion polymerization were prepared via emulsion polymerization using potassium persulfate (KPS) as initiator in ethanol-water mixed solvents.Emulsifier-free seeded emulsion copolymerization of styrene (St) with acrylonitrile (AN) was carried out in the presence of poly(ethylene glycol) monomethoxymonomethacrylate (PEGm)macromonomer as reactive stabilizer and 2,2'-azobisisobutyronitrile (AIBN) as initiator to obtain submicron-sized PEGm graft poly(styrene-co-acrylonitrile) (PEGm-g-PSAN) composite particles with unique morphology.Scanning electron microscopy (SEM) indicated that St and AN together contributed to forming the unusual morphology.The concentration of St and AN,total monomer concentration,initiator type and the monomer adding method remarkably affected the morphology of the composite polymer particles.     

An analytical model for the critical shell thickness in core/shell nanowires based on crystallographic slip

Employing crystal plasticity theory and micromechanics inclusion theory, we developed a full-strain relaxation model under isotropic assumption of materials properties to predict the dependence of the critical shell thickness (CST) for defect-free core/shell nanowires (NWs) on their growth direction. Unlike prior models, we consider three important factors in the energetic analysis (1) the self-energy of a dislocation loop in a finite domain, (2) the three-dimensional mismatch strains that develop in core/shell NWs (axial, radial and tangential directions) as a result of the finite NW geometry and the lattice mismatch between the core and shell materials, and (3) the three-dimensional plastic strains from misfit dislocations that nucleate to relax the mismatch strains. With these, the full-relaxation model is able to reveal that (i) the variation of the CST with growth direction depends on the core radius, (ii) misfit dislocations will not nucleate when the core radius falls below a critical value, (iii) the CST tends to a constant as the core radius increases, and (iv) the CST predicted by prior uniaxial-strain relaxation models is a lower bound.