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1.
刘欢  徐锦绣  郑炀  熊镭 《波谱学杂志》2020,37(3):370-380
渤海J油田沙河街组储层核磁共振(NMR)测井孔隙度和岩心NMR孔隙度均低于岩心氦孔隙度,这种现象影响了NMR测井的应用效果.通过开展岩心NMR实验,对该研究区仪器采集参数、井眼环境以及储层流体性质等因素进行分析,发现造成储层NMR测井孔隙度偏低的主要原因是高矿化度泥浆滤液侵入.基于饱和不同矿化度盐水对T2谱的影响规律,确定了需要对T2谱进行形态校正的矿化度下限值,并建立了对应不同矿化度的T2谱形态校正模型及NMR孔隙度校正方法.应用结果表明,校正后的NMR测井孔隙度与岩心氦孔隙度的平均相对误差从13.56%下降至2.81%,有效提高了NMR测井孔隙度的精度.  相似文献   

2.
基于常规测井资料的体积模型和一维核磁共振(NMR)测井资料的固定截止值法,可以计算地层孔隙度,但是扩径段孔隙度计算结果偏大.本文通过川西海相雷四段岩心样品NMR实验和实测二维NMR测井资料,开展扩径段的T2T1孔隙度计算方法研究.首先总结不同孔径流体在T2谱和T1谱上的响应特征,分析钻井液流体峰截止值的分布范围和影响因素,建立钻井液流体弛豫时间截止值的计算模型;然后根据未扩径段和扩径段的粘土束缚水弛豫时间截止值确定原则,确立变粘土束缚水弛豫时间截止值的有效孔隙度计算方法.多口井的应用效果表明,基于T1谱的孔隙度计算结果精度更高、定量分析误差小,能有效解决扩径段孔隙度计算结果偏大的问题,满足储层评价的要求.  相似文献   

3.
本文对具有特定横向弛豫时间(T2)的硫酸铜溶液进行了多回波间隔(TE)的核磁共振(NMR)实验,并利用数值模拟对32组具有不同弛豫分量的模型进行了变TE模拟实验,定量研究了TE对致密油气、页岩气等低孔低渗储层NMR孔隙度的影响规律.实验结果表明,随着TE的增大,各T2弛豫组分NMR孔隙度先维持在100%左右,然后迅速衰减,当TE增加到一定数值时,趋近于0;不同T2弛豫组分NMR孔隙度开始迅速衰减及最后变为0的TE值存在显著差异.根据不同T2弛豫组分NMR孔隙度与TE的关系,将整个NMR测量分为无损测量区、快速衰减区、无效参数区和仪器盲区4个区域.对特定弛豫组分而言,在快速衰减区弛豫组分损失量与TE呈对数关系,本文还给出了该区域NMR孔隙度的校正公式及方法.  相似文献   

4.
岩心核磁共振(NMR)T2谱和毛管压力曲线都在一定程度上反映了岩石孔隙结构,理论分析表明可利用T2谱构建毛管压力曲线,由此快速获取储层孔隙结构的信息.本文对18块岩样T2分布和毛管压力曲线进行了分析,提出将T2截止值作为幂函数的分段点,采用分段幂函数方法构建岩样的NMR毛管压力曲线,并与采用不分段幂函数方法获得的毛管压力曲线进行了对比.研究结果表明,与不分段幂函数方法相比,分段幂函数方法得到的结果和压汞实验测定的毛管压力曲线吻合度更高,平均拟合度(R2)达到0.943 1,并且论证了T2截止值作为分段点进行分段幂函数法构建NMR毛管压力曲线的合理性和可靠性.T2截止值的引入提高了幂函数法构建NMR毛管压力曲线的精度,是利用NMR T2谱构建岩样毛管压力曲线的有价值探索.  相似文献   

5.
低孔低渗碳酸盐岩储层矿物成分复杂、岩石骨架参数难以确定、储集空间类型多样、孔隙结构及孔渗关系复杂、常规测井曲线响应特征不明显,使其测井评价极其困难.本文利用核磁共振测井定量评价低孔低渗碳酸盐岩储层岩心的孔隙结构、计算储层参数.利用T2谱分布曲线分析孔隙结构、计算T2截止值;在此基础上计算岩心总孔隙度、有效孔隙度、束缚水孔隙度、渗透率等储层参数,并与常规岩心实验结果进行对比分析;最后,总结出核磁共振测井在低孔低渗储层中的应用优势与局限,为核磁共振测井评价模型的建立提供基础数据.  相似文献   

6.
川西气田雷口坡组四段白云岩储层具有良好的天然气勘探开发前景,但是储层分布具有较强的非均质性,利用常规测井和一维核磁共振测井方法判断储层流体性质存在多解性.通过分析川西雷四段白云岩储层地质特征与测井响应特征,开展岩心二维核磁共振实验,明确了实验室分析与测井过程中环境、参数等影响因素,建立了岩心分析结果的校正方法,明确了钻井液、束缚流体、可动水与天然气信号在二维核磁共振测井中谱分布区间,建立了基于T2-T1T1/T2R)的白云岩储层二维核磁共振测井气水识别图版.利用图版对川西雷四段储层流体性质开展评价,二维核磁共振测井解释结论得到了实钻测试结果的验证,该气水识别方法填补了常规测井、一维核磁共振测井在评价储层气水关系中的缺陷,可有效解决白云岩储层流体性质判别难题.  相似文献   

7.
二维核磁共振(NMR)测井在储层参数计算与流体性质判别应用中的作用逐渐受到重视.然而在川西致密气藏开展二维NMR测井应用之初,遇到了现有观测模式下资料采集效率较低、测井结果与地质条件不匹配等难题.通过对比两种常用的二维NMR测井方法,开展致密气藏二维NMR测井观测模式设计方法研究,结合致密气藏实际应用效果分析,明确了横向弛豫时间-纵向弛豫时间(T2-T1)方法比横向弛豫时间-自扩散系数(T2-D)方法更适用于致密气藏,总结了一套致密气藏二维NMR测井观测模式设计流程与参数取值方法,设计出了适用于致密气藏的观测模式TGR01(tight gas reservoir 01).新设计的观测模式在致密气藏的应用效果优于现有的二维NMR测井观测模式,结合T2-T1方法可以有效识别储层中的流体信号,解决致密气藏综合评价难题.  相似文献   

8.
相比于常规储层,缝洞型油藏灰岩储具有集体结构复杂、缝洞尺度差异大、裂缝起主要沟通作用等特点,使用常规方法研究其流动特性和流体分布规律异常困难.该文采用自行研制的核磁共振(NMR)在线驱替装置对塔河奥陶系油藏15块致密基质灰岩岩芯进行了压力敏感性实验,获得了高压及流动状态下岩芯的横向弛豫时间(T2)谱变化情况.在此基础上分析了灰岩在压敏实验过程中微裂缝尺寸、孔隙度及渗透率的变化规律,并与常规测试分析结果进行了对比.结果表明:NMR在线检测技术可以定量测量岩芯孔隙及微裂缝的变化,为岩芯渗透率变化规律提供微观解释.  相似文献   

9.
本文在150~370 K温度范围内,采用固体核磁共振(NMR)测定了半晶聚-3-羟基丁酸酯(PHB),以及3-羟基戊酸酯单体质量分数分别为5%(PHBV5)和12%(PHBV12)的聚羟基丁酸戊酸酯共聚物在实验室坐标系和旋转坐标系条件下质子的自旋-晶格弛豫时间T1T1ρ.通过弛豫时间随温度变化的理论拟合,分别获得上述半晶聚合物晶区和结晶区的分子动力学参数(包括Eaτ0).这些结果从分子水平上阐述了PHB结构修饰和增强的原因.  相似文献   

10.
多孔介质渗透率的NMR测定   总被引:5,自引:1,他引:4  
介绍了利用NMR T2 弛豫数据求取岩心物性参数--渗透率的方法. 国外学者在分析了大量数据的基础上,建立了3种由T2 弛豫数据计算渗透率的模型,分别简称为SDR,Coates-cutoff和Coates-sbvi. 其中SDR模型不受束缚水计算方法的影响,但对岩心孔隙中流体的性质很灵敏,比较适合于水基泥浆地层. coates-cutoff和Coates-sbvi模型对束缚水的计算精度很敏感,可动和不可动流体孔隙体积的测定对渗透率的计算结果影响也很大. 此外,这三种模型对于低渗透率岩石的计算误差都较大. 通过对不同类型岩心的T2 弛豫特性和用常规方法测得的渗透率进行系统分析,在SDR模型的基础上所建立的渗透率测定方法(SDR-REV)有三个可调整参数,计算渗透率适用范围更大,计算的结果与常规实验值更接近. 把SDR-REV方法用于砂岩、砾岩、凝灰岩和火成岩四类岩心样品渗透率的测定,说明SDR-REV方法具有更普遍的适用性. 特别是对于中国普遍存在的低渗透岩心,测定结果更为准确.  相似文献   

11.
For a coupled partial wave with a bound state, the entire T-matrix is determined by the bound-state energy and wave function, the on-shell mixing parameter and a real symmetric matrix function σ(k2,2 k11) of the continuous momentum variables k and the discrete eigenchannel labels . The on-shell part of σ is given by the eigenphases, the arbitrariness of the T-matrix is the off-shell continuation of this phase-shift matrix σ(k2, k1) into two dimensions. Three possible techniques are suggested to go from to the entire T-matrix. This construction procedure for T avoids the usual complications of a potential fit.  相似文献   

12.
The 63Cu NMR Knight shift K and spin-lattice relaxation rate 1/T1 have been measured to study the thiospinel superconductor Cu1.5Rh1.5S4 from a microscopic viewpoint. K is negative and has a weak dependence on temperature, and the hyperfine coupling constant Hhfd is estimated to be −52.4 kOe/μB. 1/T1 is proportional to the temperature in the normal state. In the superconducting state, 1/T1 takes a coherence peak just below Tc, and decreases exponentially well below Tc, from whose temperature dependence the superconducting energy gap has been proved to be close to 2Δ = 3.52kBTc given by the BCS theory.  相似文献   

13.
The use of nuclear magnetic resonance (NMR) relaxation time measurements for characterization of abnormal cardiac tissue depends upon knowledge of variations of relaxation times of normal myocardium and determinants of these variations. We calculated in vitro NMR T1 and T2 relaxation times of canine myocardium from the four cardiac chambers, and determined hydroxyproline concentration (as a measure of collagen) and percent water content of the samples. We found both water content and T1 relaxation time of the right ventricle to be significantly greater than the left atrium (p < 0.05). T2 relaxation time of the left ventricle was found to be shorter than each of the other three chambers (p < 0.05). There were significant correlations between the spin-lattice relaxation time and both percent water content (r = 0.58) and hydroxyproline concentration (r = 0.45). A significant correlation was also found between T2 relaxation time and hydroxyproline concentration (r = 0.49). When T1 and T2 were adjusted for water and hydroxyproline content, there was no longer any evidence for significant interchamber differences for either T1 or T2. These data suggest that differences in NMR relaxation times exist among the four chambers of the normal canine heart. Furthermore, a major determinant of myocardial spin-lattice relaxation time is tissue water content while both collagen content and percent water content significantly contribute to variability in cardiac chamber T2 relaxation times.  相似文献   

14.
页岩气储层的孔隙结构复杂且非均质性较强,导致储层表征及有效性评价面临极大挑战.为了建立页岩气储层孔隙结构的定量评价方法,本文选取了鄂西宜昌地区陡山沱组二段20块岩心,采用0.069 ms的回波间隔开展饱含盐水状态下的核磁共振(NMR)实验.在此基础上,对T2谱进行了多重分形特征分析,提取了对页岩气储层孔隙结构较敏感的参数,并建立了基于最小与最大广义分维数差值(Dmin-Dmax)和谱宽(Δα)划分页岩气储层类型的方法及标准.该方法对于有效提高页岩气储层的预测精度、指导开发选层等具有重要意义.  相似文献   

15.
A thermoelectric probe has been developed in our laboratory. It consists of a thermocouple embedded in an absorbing material, such as silicone. Its response allows us to measure the ultrasonic intensity repartition in the reactor either by means of the initial rate of temperature (dT/dt)0 or by the difference between the equilibrium temperature Teq and the temperature of the medium T0T = TeqT0). It is shown that the increase of temperature of the absorbing material is linked to the absorption of ultrasound transmitted in the medium. A heat conduction model allows us to interpret the results, the convective transfer being negligible. It is found that the ultrasound propagation surprisingly seems to be sensitive to the flow regime.  相似文献   

16.
《中国物理 B》2021,30(6):67502-067502
Structural properties of the organic-inorganic hybrid(C_2H_5NH_3)_2CuCl_4 have been investigated by means of x-ray powder diffraction and Rietveld analysis. A structural phase transition from Pbca to Aba2 occurs at T_4= 240 K, which results in a paraelectric–ferroelectric phase transition. The release of the Jahn–Teller distortion with increasing temperature toward T_4 is revealed by the structural analysis.  相似文献   

17.
139La-NQR measurements have been carried out in the ternary carbide superconductor LaNiC2. The nuclear quadrupole frequency and the asymmetry parameter of 139La in LaNiC2 were estimated to be about 1.9 MHz and 0, respectively. In the normal state, the nuclear spin relaxation rate (1/T1) in the 139La NQR signal was proportional to temperature (T) in zero external field above the superconducting transition temperature (Tc) or in an external field larger than the superconducting critical field, which means the system is in the Fermi-liquid state. In the superconducting state, on the other hand, 1/T1 decreases no more linearly with T, but decreases rapidly exponentially as exp (−Δ/kBT) at low T with an appreciable enhancement just below Tc. The value of the superconducting energy gap, 2Δ, was estimated to be 3.34kBTc, compared with 3.52kBTc of the BCS-value. This result strongly suggests that the superconductivity in LaNiC2 is of a conventional BCS type.  相似文献   

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