INVESTIGATION ON FATIGUE HYSTERESIS LOOPS MODELS OF FIBRE-REINFORCED CERAMIC-MATRIX COMPOSITES

纤维增强陶瓷基复合材料初始加载到疲劳峰值应力时, 基体出现裂纹, 纤维/基体界面发生脱粘. 在疲劳载荷作用下, 纤维相对基体在界面脱粘区往复滑移使得陶瓷基复合材料出现疲劳迟滞现象. 建立了纤维陶瓷基复合材料疲劳迟滞回线细观力学模型, 采用断裂力学方法确定了初始加载纤维/基体界面脱粘长度、卸载界面反向滑移长度与重新加载新界面滑移长度, 分析了4种不同界面滑移情况的疲劳迟滞回线. 假设正交铺设与编织陶瓷基复合材料疲劳迟滞回线主要受0°铺层、轴向纱线内纤维/基体界面滑移的影响, 预测了单向、正交铺设与编织陶瓷基复合材料在不同峰值应力与不同循环的疲劳迟滞回线, 与试验结果吻合.     

纤维增强陶瓷基复合材料疲劳迟滞回线模型研究

纤维增强陶瓷基复合材料初始加载到疲劳峰值应力时, 基体出现裂纹, 纤维/基体界面发生脱粘. 在疲劳载荷作用下, 纤维相对基体在界面脱粘区往复滑移使得陶瓷基复合材料出现疲劳迟滞现象. 建立了纤维陶瓷基复合材料疲劳迟滞回线细观力学模型, 采用断裂力学方法确定了初始加载纤维/基体界面脱粘长度、卸载界面反向滑移长度与重新加载新界面滑移长度, 分析了4种不同界面滑移情况的疲劳迟滞回线. 假设正交铺设与编织陶瓷基复合材料疲劳迟滞回线主要受0°铺层、轴向纱线内纤维/基体界面滑移的影响, 预测了单向、正交铺设与编织陶瓷基复合材料在不同峰值应力与不同循环的疲劳迟滞回线, 与试验结果吻合.      

A percolation-type fracture criterion for composites with randomly oriented fibres

A fracture model is built up for a solid composed of brittle fibres randomly oriented in the matrix volume. The fracture process includes a stable growth of microcracks caused by fibre breaking under the load and formation of an infinite cluster of the microcracks. Both upper and lower bounds for ultimate stress in a fibre system are found as functions of the fibre volume fraction. The calculation of the ultimate stresses are performed by using the percolation theory and the theory of branching processes. At the present stage of the theory under consideration, only two types of the microcracks are appraised, namely that of a delamination type which corresponds to a weak fibre/matrix interface, and that of a penny shape which corresponds to a strong fibre/matrix interface. A particular solid contains only one type of the microcracks. In both cases, non-linear dependencies of the ultimate composite strength on fibre volume fraction are obtained.     

A theoretical model for electroelastic analysis in piezoelectric fibre push-out test

A theoretical model is presented to study the elastic deformation process and frictional sliding behavior in single piezoelectric fibre push-out tests. Based on the theoretical model and some necessary simplifications, stress and electric fields are obtained for push-out tests of a circular piezoelectric fibre embedded in an elastic matrix. Numerical results of a piezoelectric fibre/expoxy matrix system are presented to verify the proposed formulation. The study shows that there is a significant effect of the piezoelectric parameter and embedded fibre length on stress transfer, electric field distribution and load-displacement curve of the frictional sliding process. This study also indicates that the piezoelectric effect has a distinct influence on the mechanical behavior and properties of the interface in a fibre/matrix system.     

单纤维实验技术的现状和展望

本文综述了目前流行的测量纤维／树脂界面力学性能的单纤维实验技术。重点介绍了三种单纤维实验技术——单纤维拔出法、单纤维段埋入法和单纤维压出法的基本原理。讨论了三种单纤维实验技术在理论和应用上的发展重点     

纤维压出实验双向脱粘现象的数值研究

本文利用轴对称边界元程序，对影响纤维同界面剪面应力分布的材料和几何参数；纤维与基体的弹性模量比，纤维体积分数，试件厚度和支撑孔尺寸进行了数值分析工作，找出了纤维压出实验中导致界面双向脱粘的主要影响参数，给出了关于性暮一经和纤维体积分数的两界面端初始剪切脱粘的发生区域。     

Slip, stick, and reverse slip characteristics during dynamic fibre pullout

Inertial effects in the mechanism of fibre pullout (or push-in) are examined, with emphasis on how the rate of propagation of stress waves along the fibre, and thence the pullout dynamics, are governed by friction and the propagation of companion waves excited in the matrix. With a simple shear lag model (assuming zero debond energy at the fibre/matrix interface), the effect of uniform frictional coupling between the fibre and the matrix is accounted for in a straightforward way. Analytical solutions are derived when the pullout load increases linearly in time. The process zone of activated material is generally divided into two or three domains along the axis of the fibre. Within these domains, slip in the sense implied by the load, slip in the opposite sense (reverse slip), and stick may be observed. The attainable combinations define three regimes of behavior, which are realized for different material parameter values. The elastodynamic problem is also solved more accurately using a plane stress finite element method, with friction represented by an interfacial cohesive zone. The predictions of the shear lag theory are broadly confirmed.     

模型复合材料弹塑性界面应力分析

由纤维增强弹塑性基体所产生的界面具有弹塑性力学行为。考虑到一般材料的塑性变形都遵循幂硬化规律,对模型复合材料的界面进行弹性和应变硬化状态下的变形规律及其应力分析。以纤维拔出试验为研究模型,将界面分成弹性区和塑性区。利用界面应力剪滞理论,分别建立弹性区和塑性区的界面力学基本方程。选择适当的位移函数满足基本方程及埋入纤维的边界条件,再按位移函数求出弹性区和塑性区的界面剪应力。推导出平均界面剪应力与纤维     

基于弹性-塑性内聚力模型的纤维拔出界面宏观行为分析

用解析法分析了单纤维从聚合物基体中的拔出过程,采用弹性—塑性内聚力模型模拟裂纹的扩展和界面失效,确定了临界纤维埋入长度,该值区分两种不同长度的纤维拔出过程. 在纤维拔出过程,界面经历不同的阶段. 纤维埋长小于临界长度时,界面的脱粘载荷与纤维的埋长成正比;超过临界长度后,界面的脱粘载荷近似为常数. 分析了界面参数对脱粘载荷的影响:增加界面的剪切强度和界面的断裂韧性,或减小界面裂纹萌生位移,均能提高界面的脱粘载荷;界面脱粘后无界面摩擦应力时,拔出载荷—位移曲线的峰值载荷等于界面的脱粘载荷;界面摩擦应力存在时,使峰值载荷大于脱粘载荷,需要较长的纤维埋入长度和较大的界面摩擦应力.      

Analytical study of the load transfer in fibre-reinforced 2D composite materials

The phenomenon of the load diffusion from a fibre to a surrounding matrix is analysed for the 2D case. We use an approximate analytical approach based on the asymptotic reduction of the governing biharmonic problem into two harmonic problems. The comparison of the obtained solutions with known results of other authors shows an acceptable accuracy of the proposed asymptotic simplifications. All solutions are obtained in closed analytical form.The case of perfect bonding between fibre and matrix for a single fibre and for a periodic system of fibres is firstly considered. Then we study the influence of the interface stiffness. In the case when only a single fibre is loaded, the influence of all other fibres is predicted by means of a three-phase model. The proposed approach gives a possibility to solve the problems for a broken fibre and for a broken matrix, as well as for partly debonded fibres. The important problem of infinite matrix cracks is also solved in the present paper.The obtained results can be used for the calculation of pull-out and push-out tests, as well as for the investigation of the fracture of composite materials.     

Theoretical model of piezoelectric fibre pull-out

A theoretical model of a single piezoelectric fibre pull-out is developed to study the interaction between fibre deformation, pull-out stress and corresponding electrical field. Computer simulation of the stress–displacement curve of the fibre pull-out process is presented. Numerical examples show that the piezoelectric fibre pull-out behaviour can be both described and affected by its electrical field. Therefore, the interactions between the mechanical and electric fields of the fibre/matrix system can be employed to monitor and control the fracture behaviour of active fibre composites.     

Crack paths formed by multiple debonds in LFRP composites

Onset and growth of debonds at fibre-matrix interfaces in a bundle of fibres subjected to transverse loads are studied numerically. In particular, the crack path formed by debonded neighbour fibres is analysed. The Linear Elastic–Brittle Interface Model (LEBIM) is used to model the fibre-matrix interface behaviour. This simple model of a Long Fibre Reinfoced Polymer (LFRP) composite includes ten parallel fibres embedded in a matrix cell whose external dimensions are much larger than the fibre radius. The advantage of the present LEBIM formulation of the so-called matrix cracking lies in its ability to make quantitative predictions about the concurrent fibre-matrix debond onset and mixed-mode interface crack growth in a fibre bundle. The numerical analysis predicts failure loads producing the first and subsequent debond onsets, leading to a crack path. A discussion on the position where debond occurs is also included. Finally, the effect of the load biaxiality on the crack path is studied in detail.     

Progress in shakedown analysis with applications to composites

This paper reports on recent developments in the field of direct methods, in particular shakedown analysis (SA) from theoretical and numerical points of view. Emphasis is placed on problems connected with the failure of fibre-reinforced periodic composites under variable loads where special attention is paid to the problem of interface debonding between fibre and matrix materials. The approach is based on a local SA in a representative volume element of the composite and the use of averaging techniques to study the influence of each component (matrix, fibre and interface) on the macroscopic response of such composite. For numerical applications, the interior-point difference-of-convex-functions algorithm (IPDCA) is proposed as an efficient method for solving large-scale problems.     

Stress analysis of notched anisotropic finite plates under mechanical and hygrothermal loads

Summary Notch-induced stress concentrations in anisotropic composite materials depend on their directional material properties, especially for uniaxially reinforced composites with high-modulus fibres. The design of notched high-performance composites requires therefore a special proof of their notched strength, which includes the structural parameters of the fibre/matrix combination, fibre orientation and layer arrangement. The assessment of the effects of the finite outer boundary is of practical importance when dimensioning critical notched regions. An anisotropic plate with finite dimensions and a hole in its center will be used here to model stress concentrations. The calculation is based on conformal mappings combined with complex-valued stress functions. The outer boundary is described using point-matching and the least-squares method. The solutions are conducive to the assessment of the essential influencing factors of material properties, geometry and loads. Notched finite plates made of fibre/matrix composites, mainly carbon-fibre reinforced polymers, will be presented as illustrations. Received 29 June 1998; accepted for publication 22 October 1998     

<Emphasis Type="Italic">In-situ</Emphasis> Full Field Measurements During Inter-Facial Debonding in Single Fiber Composite Under Transverse Load

The fibre/matrix interfacial damage mechanisms of fiber-reinforced composites (FRCs) are investigated for single-fiber composites under transverse load. A stereo microscope setup is used for 3D digital image correlation during in-situ quasi-static tests of single-fiber standard dog-bone specimens. Macro-fibers (0.9 mm diameter) with radically different interfacial bonding with the epoxy matrix are used. Damage appears to initiate with fiber debonding at the free surface along the tensile direction. The crack then propagates around the interface while slightly growing along the fiber until a lateral crack initiates on the debonded free surface, provoking specimen failure. The final failure mechanisms appears to be different for strong and weak fiber/matrix bonding. 3D DIC is used to provide precise measurements of displacements, strains, and out-of-plane displacement during the whole test. Quantitative differences in the displacement fields are measured in the cases of strong and weak bonding between the fiber and matrix. 3D DIC with macro-fibers is shown to be a promising technique to provide a better understanding of the damage mechanisms in a single-fiber composite and to determine interfacial toughness of a specific fibre/matrix couple in order to perform accurate modeling of damage in FRCs. Displacement, strain, and confidence field results for each pixel from each experiment and at each time step are also provided for detailed comparison with simulation results.     

金属基复合材料和强度与损伤分析

用观察计算力学的方法分析了金属基复合材料（ＭＭＣ）多重损伤与强度的关系,采用唯象的内聚力模型模拟纤维／基体界面的脱粘和采用Ｇ－Ｔ模型描述韧性基体的损伤。并用上述模型分析了长纤维增强ＭＭＣ在横向荷载作用下损伤演化的规律,讨论了不同界面性质与材料强度及损伤、破坏模式之间的关系。     

Investigation of the Effects of Environmental Fatigue on the Mechanical Properties of GFRP Composite Constituents Using Nanoindentation

Background

Fatigue failure criteria for fibre reinforced polymer composites used in the design of marine structures are based on the micromechanical behaviour (e.g. stiffness properties) of their constituents. In the literature, there is a lack of information regarding the stiffness degradation of fibres, polymer matrix and fibre/matrix interface regions affected by environmental fatigue.

Objective

The aim of present study is to characterize the stiffness properties of composite constituents using the nanoindentation technique when fatigue failure of composites is due to the combined effect of sea water exposure and cyclic mechanical loads.

Methods

In the present study, the nanoindentation technique was used to characterize the stiffness properties of composite constituents where the effects of neighbouring phases, material pile up and viscoplasticity properties of the polymer matrix are corrected by finite element simulation.

Results

The use of finite element simulation in conjunction with nanoindentation test data, results in more accurate estimation of projected indented area which is required for measuring the properties of composite constituents. In addition, finite element simulation provides a greater understanding of the stress transfer between composite constituents during the nanoindentation process.

Conclusions

Results of nanoindentation testing on the composite microstructure of environmentally fatigue failed composite test coupons establish a strong link to the stiffness degradation of the fiber/matrix interface regions, verifying the degradation of composite constituents identified by scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX) analysis.

     

Micromechanical analysis of polymer composites reinforced by unidirectional fibres: Part II – Micromechanical analyses

This paper presents the application of a new constitutive damage model for an epoxy matrix on micromechanical analyses of polymer composite materials. Different representative volume elements (RVEs) are developed with a random distribution of fibres. Upon application of periodic boundary conditions (PBCs) on the RVEs, different loading scenarios are applied and the mechanical response of the composite studied. Focus is given to the influence of the interface between fibre and matrix, as well as to the influence of the epoxy matrix, on the strength properties of the composite, damage initiation and propagation under different loading conditions.