萃取-催化电势动力学法测定生物样品中痕量钼的研究

选H_2O_2-KI作为指示反应体系,以碘离子选择电极作跟踪体系电位变化的监测器,通过系统性实验,建立了生物样品中痕量钼的催化电势动力学分析法。该法可对试液中5×10~(-8)M以上,宽达3个数量级的Mo(Ⅵ)进行测定。对于生物样品中共存离子的干扰,采用萃取一掩蔽法排除。以乙酸乙酯代替惯用的毒性溶剂氯仿,取得满意的效果,对鳗饵及人发进行了实际分析及标准回收实验,回收率93.3～110.0%(n=2-3),相对平均偏差≤4.8%。     

用于散裂中子源直线加速器超导段相速度设计分析

对用于散裂中子源的质子直线加速器的超导加速段进行了初步设计,其中,包括加速腔腔形的设计和优化、超导加速段的结构布局.另外,对超导加速腔的加速单元数的选择及设计值β_G的确定、加速腔的优化原则及束流的动力学性质进行了讨论.     

一种新型可协调绿色荧光材料BaAl2Si2O8∶Tb3+,Ce3+的发光性质与能量传递

采用高温固相法制备了BaAl2Si2O8∶Tb3+,Ce3+系列的荧光材料,讨论了Tb3+,Ce3+单掺及Tb3+,Ce3+共掺样品的光谱性质及发光机理,分析了Ce3+与Tb3+之间的能量传递过程.通过对样品进行XRD,荧光光谱,色坐标等测试.结果表明,Tb3+,Ce3+的掺杂没有改变BaAl2Si2O8晶体的结构.BaAl2Si2O8∶Tb3+发出明亮的绿光,发光峰分别位于487,545,583和621 nm对应于Tb3+的5D4→7FJ(J=6,5,4,3)特征发射.Ce3+的掺入没有改变BaAl2Si2O8∶Tb3+发射光谱的位置,但使其激发谱由窄带激发变成了宽带激发增加了谱带多样性,发光强度有了明显的增强,而且颜色也具有一定的协调性,使其在实际运用方面具有更大的灵活性.发光强度增强的原因不仅仅是因为Ce3+的敏化作用,还与Ce3+和Tb3+之间存在能量传递有密切关系.通过猝灭法计算了,Ce3+与Tb3+之间的能量传递的临界距离为15.345 nm,并且证明了能量传递是由偶极-偶极相互作用产生的.通过计算得到能量传递效率最高达到了76.04%.     

强流AVF型Hui旋加速器中的空间电荷效应和束晕

详细推导了AVF型Hui旋加速器中束团粒子在曲线坐标系中的动力学方程（考虑和不考虑空间电荷相互作用力两种情况）,在假定动力学方程中各参值的前提条件下,用Lunge-Kutta方法对考虑空间电荷时的动力学方程进行了数值计算,结果表明,束晕的形成和发展同样也是强流Hui旋加速器中束流损失的一个主要原因,但束晕形成的机制不同于直线加速器的情况,它不是由共振和混沌引起,而是由于粒子的排斥运动和束团内粒子的涡流运动引起的。     

基于聚焦物镜与PSD的激光对中测量方法研究

针对传统激光对中方法数学模型复杂、求解困难的不足,提出一种基于聚焦物镜与PSD的激光对中测量方法。该方法利用光学系统中视场与焦距的关系以及相似三角形的原理得到不对中的角度偏差和平行偏差,测量原理简单,求解方便。实验结果表明,当平行偏量和角度偏量的测量范围分别为0.5 mm~1.5 mm,0.047 7°~0.143 2°时,平行偏量测量误差范围为0.035 mm~0.207 mm,角度测量误差范围为0.000 2°~0.012 8°。最后对系统测量误差进行分析并提出一种消除安装误差影响的方法,给出了计算公式。     

ATPF—a dedicated proton therapy facility

A proton therapy facility based on a linac injector and a slow-cycling synchrotron is proposed. To obtain good treatments for different cancer types, both the spot scanning method and the double-scattering method are adopted in the facility, whereas the nozzles include both gantry and fixed beam types. The proton accelerator chain includes a synchrotron of 250 MeV in maximum energy, an injector of 7 MeV consisting of an RFQ and a DTL linac, with a repetition rate of 0.5 Hz. The slow extraction using the third-order resonance and together with the RFKO method is considered to be a good method to obtain a stable and more-or-less homogenous beam spill. To benefit the spot scanning 200 between 60 MeV and 230 MeV. A new method method, the extraction energy can be as many as about - the emittance balancing technique of using a solenoid or a quadrupole rotator is proposed to solve the problem of unequal emittance in the two transverse planes with a beam slowly extracted from a synchrotron. The facility has been designed to keep the potential to be upgraded to include the carbon therapy in the future.     

Slim Discs with Varying Accretion Rates

It was revealed in our previous studies that there exists a maximal possible accretion rate for slim discs with constant accretion rates because the correctly calculated vertical gravitational force can only gather some limited amount of accreted matter. Here we show that when the accretion rate is not constant and instead decreases with decreasing radius because of outflows, such that the amount of accreted matter is adjusted to be within the allowed limit, global slim disc solutions can be constructed even for the case that accretion rates at large radii apparently exceed the maximal possible value. This result further demonstrates that outflows seem to be unavoidable for accretion flows with large accretion rates at large radii.     

真空紫外-紫外光激发下的Na2SO4:TbF3的发光性质

在空气中900℃温度下,对纯天然无水芒硝(Na2SO4)和TbF3的混合粉末加热20min,制备了Na2SO4:TbF3发光材料。并测量了在室温中真空紫外-紫外光下的发射和激发光谱。发射光谱有一系列由于Tb3+离子的5D4→7FJ(J=6,5,4,3,2)和5D3→7FJ(J=6,5,4,3,2)跃迁发射峰。通过监测542nm处发光得到的激发光谱,分别由Tb3+离子4fn→4fn-15d跃迁(187,193,218nm),基质吸收(165,200,240nm)引起的强激发谱和禁戒的f-f跃迁产生的弱激发谱组成。在TbF3的掺杂量在0.3%～2%范围内,随着Tb3+离子掺杂量的增加,真空紫外区的激发谱相应地逐渐增强。     

RF power coupling for the CSNS DTL

The China Spallation Neutron Source (CSNS) drift tube linac (DTL) consists of four tanks and each tank is fed by a 2.5 MW klystron. Accurate predication of RF coupling between the RF cavity and ports is very important for DTL RF coupler design. An iris-type coupler is chosen to couple the RF power to the DTL accelerating cavity. The physical design of the DTL coupler and the calculations of RF coupling between the cavity and coupler are carried out. The results from the numerical simulations are in excellent agreement with the analytical results.