高强度钢手工焊接后过程的声发射实时监测研究

本针对实际工艺中使用的高强度钢，重点对手工焊接的冷却过程利用声发射技术进行实时监测。本次试验是和先前在不同型号的钢板在手工焊接过程中所产生的声发射信号进行比较的基础上进行的，主要目的是寻找高强度钢在手工焊接的冷却中所产生的活性裂纹在冷却阶段的声信号特征。     

不锈钢焊接件不等强度激光冲击与应力腐蚀试验研究

针对不锈钢焊接接头应力及组织分布不均匀,容易导致应力腐蚀开裂的问题,采用不等强度激光冲击波对316奥氏体不锈钢焊接接头进行处理。通过应力腐蚀试验、残余应力测试及微观组织分析,研究了激光冲击强化对焊接接头应力腐蚀抗性的影响及其作用机理。试验结果表明：激光冲击强化将焊接件的应力腐蚀断裂时间提高了33.48%。激光冲击波的作用,在焊接接头部位引入了高数值的残余压应力,一方面消除了热影响导致的残余拉应力,同时抵消了拉伸工作载荷的作用,降低局部应力梯度,从而延缓表面钝化膜的破裂;另一方面,激光冲击使焊接接头不同区域之间的微观组织均匀和细化,提高了微裂纹萌生的条件,降低了金属发生阳极溶解的可能性。两种因素的共同作用,使得不锈钢焊接接头的抗应力腐蚀性能显著增强。     

Cohesive zone modelling of anodic dissolution stress corrosion cracking induced by corrosion product films

Damage mechanics based on the cohesive zone model were applied to study the anodic dissolution stress corrosion cracking (SCC) in flat and U-shaped edge-notched specimens. The simulation results show that corrosion product films (CPFs) facilitate crack initiation in SCC due to the CPF-induced stress and CPF rupture. In the flat specimen, SCC susceptibility increases with the CPF thickness and CPF Young’s modulus, while it decreases with CPF fracture strength. For the U-shaped edge-notched specimen, the normalised threshold stress intensity factor K_ISCC/K_IC decreases with the CPF thickness and notch depth.     

Role of hydrogen in stress corrosion cracking of austenitic stainless steels

Effects of hydrogen charging on the stress corrosion cracking (SCC) behavior of 304 and 310 stainless steels under sustained load were investigated in boiling 42% MgCl₂ solution. The cracking was accelerated by the incorporation of hydrogen into the steel without altering the crack growth mechanism. The fact that the active dissolution is almost unaffected by the hydrogen charging and tensile stress indicates that the phenomenon of hydrogen-promoted SCC is unlikely a result of hydrogen-facilitated active dissolution. In contrast, hydrogen significantly promotes anodic dissolution in the potential range where the active-to-passive transition occurs. The electrochemical noise detected in the SCC process implies that the crack propagation process is discontinuous and hydrogen charging can raise the frequency of film breakdown at the crack tip. These observations suggest that the hydrogen-promoted SCC may result from the hydrogen-induced passivity degradation.     

Mechanical behavior and acoustic emission technique for detecting damage in sandwich structures

The present study investigates the mechanical behavior under static and dynamic loadings and assesses damage by the acoustic emission method of two types of sandwich composite materials. The sandwich structures under study are both made of cross-ply laminates as skins and PVC closed-cell as foam with different densities: 60 kg m⁻³ and 100 kg m⁻³. The mechanical behavior tests were conducted in static and cyclic fatigue loadings under 4-point bending. The sandwich structures considered in fatigue tests were damaged by a various number of shear damages in the foam. Static tests were performed to determine the failure parameters and characteristics used in fatigue tests. The damage density effect on the stiffness, hysteresis loops, dissipated energy and damping of sandwich structures, were studied for various numbers of cycles during cyclic fatigue tests. The acoustic emission method was used to identify and characterize the local damage in both types of sandwich materials under static 4-point bending tests.     

Stress corrosion cracking of alloy C-22 and Ti Gr-12 using double-cantilever-beam technique

Susceptibility to stress corrosion cracking (SCC) of two candidate alloys for the inner container of the multi-barrier nuclear waste package was evaluated by using wedge-loaded precracked double-cantilever-beam (DCB) specimens in deaerated acidic brine (pH≈2.70) at 90°C. Materials tested included Alloy C-22 and Ti Grade-12. Duplicate samples of each material were loaded at different initial stress intensity factor (K_I) values ranging between 22 and 43 MPa√m. Both metallography and the compliance methods were used to determine the final crack length. The final stress intensity for SCC (K_f) was computed from the measured final wedge load and the average crack length. The results indicate that, in general, the final crack lengths measured by metallography and compliance agreed well with one another, thus, providing very similar K_f values. The alloy C-22 showed higher susceptibility to SCC than Ti Grade-12 in terms of the average crack growth. Fractographic evaluation by scanning electron microscopy (SEM) of broken DCB specimens revealed three distinct regions showing the characteristics of fatigue precrack, SCC, and fast fracture.     

声发射技术在铁路系统检测中的研究和应用

高速铁路的快速发展,给我国经济和社会发展带来了巨大的推动作用,同时对铁路系统的安全性提出了更高的要求。针对声发射技术在铁路系统安全检测中的研究和应用,介绍了声发射技术及其在检测应用中的优点,综述了目前国内外声发射技术在铁路系统检测研究中的情况,包括钢轨伤损检测、车轮伤损检测、轮轴轴承伤损检测、铁路结构安全监测以及车体材料安全监测等,特别针对钢轨裂纹伤损引起的钢轨断裂这一铁路安全中的主要事故,着重分析了声发射技术在钢轨裂纹伤损检测研究中的情况,并介绍了在高速铁路方面的应用探索。最后在上述分析总结的基础上,指出了声发射技术在铁路系统特别是高速铁路检测研究中的前景及研究难点。     

Low-energy EDX – A novel approach to study stress corrosion cracking in SUS304 stainless steel via scanning electron microscopy

Intergranular stress corrosion cracking (IGSCC) in type SUS304 stainless steels, tested under pressurized water reactor (PWR) primary water conditions, has been characterized with unprecedented spatial resolution using scanning electron microscopy (SEM) and novel low-energy (∼3 kV) energy dispersive X-ray spectroscopy (EDX). An advancement of the large area silicon drift detector (SDD) has enhanced its sensitivity for X-rays in the low-energy part of the atomic spectrum. Therefore, it was possible to operate the SEM at lower accelerating voltages in order to reduce the interaction volume of the beam with the material and achieve higher spatial resolution and better signal-to-noise ratio. In addition to studying the oxide chemistry at the surface of intergranular stress corrosion cracks, the technique has proven capable of resolving Ni enrichment ahead of some crack tips. Active cracks could be distinguished from inactive ones due to the presence of oxides in the open crack and Ni-rich regions ahead of the crack tip. Furthermore, it has been established that SCC features can be better resolved with low-energy (3 kV) than high-energy (12 kV) EDX. The low effort in sample preparation, execution and data analysis makes SEM the ideal tool for initial characterization and selection of the most important SCC features such as dominant cracks and interesting crack tips, later to be studied by transmission electron microscopy (TEM) and atom probe tomography (APT).     

基于声发射技术的钢丝绳断丝模式识别

基于大量实验及波形分析,给出钢丝绳断丝事件的声发射（ＡＥ）定量化表征形式．采用类内类间距离和二维图示方法综合选择ＡＥ特征,并根据其分布情况建立起基干Ｆｉｓｈｅｒ准则的分段线性分类器,以实现断丝事件的自动检测．     

Rate effect on mechanical properties of hydraulic concrete flexural-tensile specimens under low loading rates using acoustic emission technique

Acoustic emission (AE) waveform is generated by dislocation, microcracking and other irreversible changes in a concrete material. Based on the AE technique (AET), this paper focuses on strain rate effect on physical mechanisms of hydraulic concrete specimens during the entire fracture process of three point bending (TPB) flexural tests at quasi-static levels. More emphasis is placed on the influence of strain rate on AE hit rate and AE source location around peak stress. Under low strain rates, namely 0.77 × 10⁻⁷ s⁻¹, 1 × 10⁻⁷ s⁻¹ to 1 × 10⁻⁶ s⁻¹ respectively, the results show that the tensile strength increases as the strain rate increases while the peak AE hit rate decreases. Meanwhile, the specimen under a relatively higher strain rate shows a relatively wider intrinsic process zone in a more diffuser manner, lots of distributed microcracks relatively decrease stress intensity, thus delay both microcracking localization and macrocrack propagation. These phenomena can be attributed to Stéfan effect. In addition, further tests, namely the combination of AE monitoring and strain measuring systems was designed to understand the correlation between AE event activity and microfracture (i.e., microcracking and microcracking localization). The relative variation trend of cumulative AE events accords well with that of the load-deformation curve.     

Application of signal processing to acoustic emission signals emitted by steel specimens during tensile tests

We show that time and spectral properties of ae signals emitted by steel specimens during a tensile test depend, in a large part, on the characteristics of the acquisition set-up. Then we apply signal processing techniques (FFT, normalized energy, etc) to ae signals and we make here a comparative study between the acoustic emissions of different types of steel used in nuclear reactor technology.     

早龄期荷载及低温作用下的混凝土声发射特征试验研究*

井壁混凝土由于施工与环境特殊性导致其裂缝扩展情况异常,本文通过对不同早龄期荷载、低温条件下混凝土轴压破坏过程的声发射检测,分析井壁施工环境对混凝土内部裂缝产生、发展的影响。研究表明,早龄期荷载、低温单独作用时,与标养混凝土主要差异在轴压过程中的声发射初始阶段,对混凝土内部的原有收缩裂缝有所影响。当两者耦合作用时,早龄期荷载影响比低温作用显著,并且在早龄期荷载较大时会出现声发射信号"倒置"现象。     

正交异性钢桥面板声发射波三维谱元法模拟及损伤定位*

针对大跨度桥梁正交异性钢桥面板的疲劳损伤评估与结构健康监测需求,开展基于声发射波场谱元法模拟的大型复杂板类结构损伤定位研究。采用Legendre高阶插值三维时域谱元法模拟声发射波在正交异性钢桥面板中的传播过程,验证了其内部显著的反射、衍射和频散现象,并代替人工预断铅实测试验获得大量声发射数据。然后,利用赤池信息准则判定声发射波到达各传感器的时间,通过高斯过程回归建立到达时差与声发射源位置的关系模型,用于未知损伤的定位监测。数值模型实验结果表明,赤池信息准则和高斯过程回归改进的时差图法在正交异性钢桥面板中的平均定位误差为37.3 mm(25 dB信噪比工况),平板的定位精度高于U肋。谱元法模拟有望代替繁琐的预断铅实测试验,提升声发射时差图系列损伤定位方法的实用性。     

超声双折射法测试铝合金的内部应力

声各向同性的金属材料在应力作用下表现出声各向异性,这是用声弹性法分析材料内部应力的基础。本文用偏振方向平行或垂直于应力方向的超声纯横波对LY11型铝合金进行测试。实验结果表明:材料在拉、压单轴应力作用下,偏振方向平行和垂直于应力方向的超声纯横波的声速都发生了变化。实验在分析材料声各向异性的基础上计算材料声弹性双折射系数,得到测试LY11型铝合金内部应力的理论公式,并对其内部的残余应力进行评估。实验中利用双换能器回振法测量声速,时间测试精确度可达10^-11s,可精确测量声速的微小变化量。     

Guided ultrasonic waves for non-destructive monitoring of the stress levels in prestressed steel strands

The safety of prestressed civil structures such as bridges, dams, nuclear power plants, etc. directly involves the security of both environment and users. Health monitoring of the tensioning components, such as strands, tendons, bars, anchorage bolts, etc. is an important research topic and a challenging task bringing together the non-destructive evaluation (NDE) and civil engineering communities. This paper deals with a guided ultrasonic wave procedure for monitoring the stress levels in seven-wire steel strands (15.7 mm in diameter). The mechanical and geometrical characteristics of the prestressed strands were taken into account for optimizing the measurement configuration and then the choice of the guided ultrasonic mode at a suitable frequency. Simplified acoustoelastic formulations were derived from the acoustoelasticity theory according to either calibration test or in situ measurement. The results from acoustoelastic measurements on the seven-wire steel strands are presented and discussed in the case of calibration tests and industrially prestressed strands. They show the potential and the suitability of the proposed guided wave method for evaluating the stress levels in the tested seven-wire steel strands.     

Using transmission Kikuchi diffraction to study intergranular stress corrosion cracking in type 316 stainless steels

Transmission Kikuchi diffraction (TKD), also known as transmission-electron backscatter diffraction (t-EBSD) is a novel method for orientation mapping of electron transparent transmission electron microscopy specimen in the scanning electron microscope and has been utilized for stress corrosion cracking characterization of type 316 stainless steels. The main advantage of TKD is a significantly higher spatial resolution compared to the conventional EBSD due to the smaller interaction volume of the incident beam with the specimen.Two 316 stainless steel specimen, tested for stress corrosion cracking in hydrogenated and oxygenated pressurized water reactor chemistry, were characterized via TKD. The results include inverse pole figure (IPFZ) maps, image quality maps and misorientation maps, all acquired in very short time (<60 min) and with remarkable spatial resolution (up to 5 nm step size possible). They have been used in order to determine the location of the open crack with respect to the grain boundary, deformation bands, twinning and slip. Furthermore, TKD has been used to measure the grain boundary misorientation and establish a gauge for quantifying plastic deformation at the crack tip and other regions in the surrounding matrix. Both grain boundary migration and slip transfer have been detected as well.     

Corrosion behavior of X-70 pipe steel in near-neutral pH solution

The mechanism of near-neutral pH stress corrosion cracking (SCC) of natural gas pipelines has not been well-established since the first accident was found in the 1980s. In particular, the role of hydrogen in near-neutral pH SCC has remained unknown. In this work, cyclic voltammetry was used to comprehensively investigate the fundamentals of the electrochemical corrosion reactions occurring at the steel/solution interface in diluted, 5% CO₂/N₂-purged, near-neutral pH bicarbonate solutions. It is shown that there is no stable oxide film formed on the steel surface in near-neutral pH solution. The dissolution-based cracking mechanism does not apply for near-neutral pH SCC of pipelines. The formation of a metastable Fe(OH)₂ deposit layer shows a catalytic activity on hydrogen evolution reaction, indicating that a significant amount of hydrogen could be generated under near-neutral pH condition. The presence of corrosive anions in the soil electrolyte enhances both the anodic polarization of the steel and the cathodic hydrogen evolution reaction, resulting in an increased hydrogen evolution rate. The introduction of oxygen could form a stable oxide film on the surface of steel, resulting in the loss of the surface catalytic effect on hydrogen evolution reaction. Thus, a hydrogen-based mechanism does not apply for SCC in the presence of oxygen.     

Holographic interferometry as electrochemical emission spectroscopy of carbon steel in seawater with low concentration of RA-41 corrosion inhibitor

In the present investigation, holographic interferometry was utilized for the first time to determine the rate change of the number of the fringe evolutions during the corrosion test of carbon steel in blank seawater and with seawater with different concentrations of a corrosion inhibitor. In other words, the anodic dissolution behaviors (corrosion) of the carbon steel were determined simultaneously by holographic interferometry, an electromagnetic method, and by the electrochemical impedance (EI) spectroscopy, an electronic method. So, the abrupt rate change of the number of the fringe evolutions during corrosion test (EI) spectroscopy, of the carbon steel is called electrochemical emission spectroscopy. The corrosion process of the steel samples was carried out in blank seawater and seawater with different concentrations, 5–20 ppm, of RA-41 corrosion inhibitor using the EI spectroscopy method, at room temperature. The electrochemical emission spectra of the carbon steel in different solutions represent a detailed picture of the rate change of the anodic dissolution of the steel throughout the corrosion processes. Furthermore, the optical interferometry data of the carbon steel were compared to the data, which were obtained from the EI spectroscopy. Consequently, holographic interferometric is found very useful for monitoring the anodic dissolution behaviors of metals, in which the number of the fringe evolutions of the steel samples can be determined in situ.     

Investigation of failure mechanisms in polymer composites by simultaneous measurement of ultra-small-angle scattering and acoustic emission during the deformation. I. Method

Failure mechanisms in polymer composites were investigated with the method of ultra-small-angle X-ray scattering using synchrotron radiation and acoustic emission analysis simultaneously. The composites were prepared from polystyrene filled with glass beads with different coatings. The two-dimensional scattering patterns were analyzed by means of a cylinder model, while the curves of the acoustic emission signals per stress or amplitude interval were calculated and fitted by a Weibull distribution function.     

Real time NDE of laser shock processing with time-of-flight of laser induced plasma shock wave in air by acoustic emission sensor

Acoustic emission sensor is used to research the time-of-flight of the shock wave induced by laser-plasma in air for real time nondestructive evaluation (NDE) of laser shock processing. The time-of-flight of the shock wave propagating from the source to the sensor declines nonlinearly and similarly at the different distances for different laser energies. The velocity of the shock wave at the distance of 30 mm increases faster than that of the distance of 35 mm. The relationship between the laser energy and the distance is almost linearly when the signal with distortion is measured by acoustic emission sensor. Finally, Taylor solution is used to analyze the experimental results, and the empirical formula between the energy of the shock wave and the laser energy is established, which will provide a theoretical basis for real time NDE of laser shock processing.