Manufacturing and modelling of sintered micro-porous absorption material for low frequency applications

A novel sintering based method to produce thin ultrahigh molecular weight polyethylene, UHMWPE, absorption material layer to increase absorption at low frequencies is introduced. The experimental impedance tube measurement results show that a 4 mm thick sintered sample layer increases absorption at a low frequency range below 1000 Hz compared with commercial melamine and polyester absorption foam samples. To cover a wider frequency range, multilayer structures composed of a sintered micro-porous material layer and commercial melamine and polyester foam layers are created and examined. The sintered sample layer also increases absorption in multilayer structures at low frequencies. Absorption coefficient values above 0.5 are reached starting from 200 Hz with multilayer structures. Software exploiting Biot’s theory of porous materials has been adopted to fit the experimental absorption data for sintered samples, commercial foams and multilayers. Software based on Biot’s theory was found to deliver quite good correlation with measured absorption coefficient values, with disagreements below 10% between the measured and estimated values.     

Improved sound absorption performance of three-dimensional MPP space sound absorbers by filling with porous materials

Because microperforated panels (MPPs), which can be made from various materials, provide wide-band sound absorption, they are recognized as one of the next-generation absorption materials. Although MPPs are typically placed in front of rigid walls, MPP space sound absorbers without a backing structure, including three-dimensional cylindrical MPP space absorbers (CMSAs) and rectangular MPP space absorbers (RMSAs), are proposed to extend their design flexibility and easy-to-use properties. On the other hand, improving the absorption performance by filling the back cavity of typical MPP absorbers with porous materials has been shown theoretically, and three-dimensional MPP space absorbers should display similar improvements. Herein the effects of porous materials inserted into the cavities of CMSAs and RMSAs are experimentally investigated and a numerical prediction method using the two-dimensional boundary element method is proposed. Consequently, CMSAs and RMSAs with improved absorption performances are illustrated based on the experimental results, and the applicability of the proposed prediction method as a design tool is confirmed by comparing the experimental and numerical results.     

释压法混合吸声系统中多孔材料厚度优化研究

研究释压法主被动混合吸声结构吸声性能与多孔吸声材料参数的关系,利用释压法对材料厚度敏感的特性,选择合适的多孔材料厚度提高系统的低频吸声性能。提出一种释压法主被动混合双层吸声结构,将误差传声器置入两层吸声结构之间的空气层中,分别优化各层的厚度,在较宽频带内获得较好吸声。对流阻系数为15000NSm^-4的一类典型的玻璃棉数值仿真,发现选择优化厚度分别为2.8 cm和6 cm,中间空腔长为2 cm,可使有效吸声频带向下大幅扩展。实验结果验证了所提宽带吸声结构。     

具有特定频段的左手材料构造与设计优化

为研究具有特定频段的左手材料设计方法. 首先基于传输线理论构造了一种左手材料微观构型, 采用S参数反演法进行数值仿真和等效传输线模型分析, 说明了该构型在特定的尺寸条件下具有左手特性, 并分析了尺寸参数对左手性能的影响. 进而给出了在给定频率附近具有最大带宽、较小损耗的左手材料设计优化问题的数学模型, 并给出了设计实例. 数值设计结果验证了优化模型的适用性和正确性.     

Calculation of sound absorption characteristics of porous sintered fiber metal

Focusing its attention on porous sintered fiber metal, this paper presents a simple extended acoustical model on the basis of Biot-Allard model by using the idea of convective heat transfer in metallic tube for reference in order to calculate the sound absorption characteristics of porous sintered fiber metal. The sound absorption coefficients and the specific surface acoustic impedances of one-layer porous fiber metal sheets, two-layer-assembled and three-layer-assembled porous fiber metal sheets are calculated by using the extended and Biot-Allard model and then compared with the corresponding measured values. By comparing, it is shown that the theoretical results calculated by using the extended model fit the measured ones better. Finally, those above-mentioned results are further discussed and analyzed.     

Design of metaporous supercells by genetic algorithm for absorption optimization on a wide frequency band

The optimization of acoustic absorption by metaporous materials made of complex unit cells with 2D resonant inclusions is realized using genetic algorithm. A nearly total absorption over a wide frequency band can be obtained for thin structures, even for frequencies below the quarter wavelength resonances i.e., in a sub-wavelength regime. The high absorption performances of this material are due to the interplay of usual visco-thermal losses, local resonances and trapped modes. The density of resonant and trapped modes in this dissipative porous layer, is a key parameter for broadband absorption. The best configurations and critical coupling conditions are found by genetic algorithm optimization. Several types of resonators are included gradually in the studied configurations (split-rings, Helmholtz resonators, back cavities) with increasing complexity. The optimization leads to a metaporous structure with a 2-cm sub-wavelength layer thickness, exhibiting a nearly total absorption between 1800 Hz and 7000 Hz. The influence of the incidence angle on the absorption properties is also shown.     

Use of a hybrid adaptive finite element/modal approach to assess the sound absorption of porous materials with meso-heterogeneities

The paper discusses the sound absorptive performance of a porous material with meso-perforations inserted in a rectangular waveguide using a numerical hybrid adaptive finite element-modal method. Two specific applications are investigated: (i) the improvement of porous materials noise reduction coefficient using meso-perforations (ii) the effects of lateral air gaps on the normal incidence sound absorption of mono-layer and two-layer porous materials. For the first application, a numerical design of experiments is used to optimize the sound performance of a porous material with meso-perforations with a reduced number of numerical simulation. An example in which the optimization process is carried out on the thickness and size of the perforation is presented to illustrate the relevance of the approach. For the second application, a set of twenty fibrous materials spanning a large flow resistivity range is used. Practical charts are proposed to evaluate the influence of air gaps on the average sound absorption performance of porous materials. This is helpful to both the experimenter regarding characterization of porous material based on Standing Wave Tube measurements and for the engineer to quantifying the impact of air gaps and for designing efficient absorbers.     

含空气层与多孔材料的复合结构隔声特性研究

基于高速列车减振降噪需求,本文应用Biot提出的多孔弹性介质声传播理论,采用传递矩阵法理论推导了典型分层结构的隔声量计算公式,给出了空气层与多孔材料对分层复合结构隔声特性的影响。将传递矩阵与遗传算法相结合,对特定中低频段内的复合结构隔声特性进行了优化。研究结果表明:空气层和多孔材料有助于分层复合结构隔声量的提高,特别是空气层对低频隔声有很好的促进作用,另外空气层与多孔材料的分配情况也影响着隔声效果。含有空气层的复合结构在提高隔声量的同时降低了结构的总体重量,实现了高速列车隔声材料低能耗和轻量化的设计目标。     

A network approach for analysis of silencers with/without absorbent material

The object of this work is to establish a general approach that can analyze the performance of most of the silencers with/without sound absorbent material. Under the assumption of plane wave propagation, the transfer matrices between the two ends of straight pipe and two-duct perforated section are derived and taken as the basic elements. Based on the conditions of continuity of pressure and of mass velocity, the silencer is modeled as a network formed by the two basic elements. Then the sound attenuation characteristic of the silencers can be investigated. With this scheme the multiply connected acoustic filters can also be analyzed. Further, the porous sound absorbent material is also included in this scheme. The effect of sound absorption material on the performance of silencers is analyzed and discussed.     

Investigation of industrial tea-leaf-fibre waste material for its sound absorption properties

The sound absorption of an industrial waste, developed during the processing of tea leaves has been investigated. Three different layers of tea-leaf-fibre waste materials with and without backing provided by a single layer of woven textile cloth were tested for their sound absorption properties. The experimental data indicate that a 1 cm thick tea-leaf-fibre waste material with backing, provides sound absorption which is almost equivalent to that provided by six layers of woven textile cloth. Twenty millimeters thick layers of rigidly backed tea-leaf-fibres and non-woven fibre materials exhibit almost equivalent sound absorption in the frequency range between 500 and 3200 Hz.     

Applicability of locally reacting boundary conditions to porous material layer backed by rigid wall: Wave-based numerical study in non-diffuse sound field with unevenly distributed sound absorbing surfaces

To clarify the applicability of locally reacting boundary conditions in wave-based numerical analyses of sound fields in rooms, we numerically analyzed a non-diffuse sound field in a room with unevenly distributed sound absorbing surfaces and investigated the differences between the extended and local reactions. Each absorbing surface was a porous material layer backed by a rigid wall. Simulations were performed by the fast multipole boundary element method, a highly efficient boundary element method using the fast multipole method. At low frequencies, the extended and local reactions yielded similar reverberation decay curves because of the influence of the room. However, when the random incidence absorption coefficients were small at low frequencies or frequencies were high, the difference was greater than expected from the corresponding Eyring decay lines. We conclude at high frequencies, the locally reacting boundary conditions lead to a longer reverberation time than that expected from the absorption coefficient differences between the extended and local reactions. These differences were similar in sound-pressure-level and sound-intensity-level distributions, and in the oblique incidence absorption coefficient of the absorbing surfaces, but were increased at low frequencies.     

Inverse acoustical characterization of natural jute sound absorbing material by the particle swarm optimization method

For modeling of jute as acoustic material, knowledge of its non-acoustical parameters like porosity, tortuosity, air flow resistivity, thermal and viscous characteristic lengths is a prime requisite. Measurement of these non-acoustical parameters is not straightforward and involves a dedicated measurement setup. So in order to overcome this issue, the inverse acoustical characterization can be used. In this paper, the particle swarm optimization method (PSO) is used as an optimization method. This method estimates the non-acoustical parameters of jute material in felt form by minimizing the error between experimental and theoretical sound absorption data. In this work, the impedance prediction models for fibrous materials like Johnson–Champoux–Allard model with rigid and limp frame and Garai–Pompoli model is used for sound absorption coefficient calculation by the transfer matrix method along with the PSO. The inverse estimated non-acoustical parameters for jute material are then compared with estimated and experimentally measured parameters for jute felts. Using these inversely predicted parameters, sound absorption of multilayer sound absorbers is also studied.     

Design optimization of tunneling field-effect transistor based on silicon nanowire PNPN structure and its radio frequency characteristics

Recently, a number of semiconductor devices have been widely researched in order to make breakthroughs from the short-channel effects (SCEs) and high standby power dissipation of the conventional metal-oxide-semiconductor field-effect transistors (MOSFETs). In this paper, a design optimization for the silicon nanowire tunneling field-effect transistor (SNW TFET) based on PNPN multi-junction structure and its radio frequency (RF) performances are presented by using technology computer-aided design (TCAD) simulations. The design optimization was carried out in terms of primary direct-current (DC) parameters such as on-current (I_on), off-current (I_off), current ratio (I_on/I_off), and subthreshold swing (SS). Based on the parameters from optimized DC characteristics, basic radio frequency (RF) performances such as cut-off frequency (f_T) and maximum oscillation frequency (f_max) were analyzed. The simulated device had a channel length of 60 nm and a SNW radius of 10 nm. The design variable was width of the n-doped layer. For an optimally designed PNPN SNW TFET, SS of 34 mV/dec and I_on of 35 μA/μm were obtained. For this device, f_T and f_max were 80 GHz and 800 GHz, respectively.     

小型掠入射式近边X射线吸收谱仪的设计

近边X射线吸收精细结构(NEXAFS)谱包含了吸收原子的局域结构信息,由于其适用范围广,灵敏度高,已经成为研究物质结构的重要手段之一。为了研究有机物的碳1s NEXAFS谱,本文基于气体激光等离子体X射线光源,采用具有平场特性的凹面变线距光栅作为分光元件,面阵CCD作为光谱探测器,设计了一台小型掠入射式近边X射线吸收谱仪。通过优化光栅和CCD的装配方案,得到了入射角88.6°的装配参数。利用光线追迹法分析了谱仪的分辨率,该谱仪工作波段2~5 nm,在4.4 nm处分辨率可达666。通过分析各结构参量误差对谱线半高宽的影响发现,半高宽对入射角的误差最为敏感,优化的装配方案可以实现入射角的高精度调节。利用氮气等离子体光谱测试了光谱仪的性能,结果显示分辨率达到设计指标。     

太赫兹自由电子激光波荡器的设计、测量与优化

波荡器电子轨迹中心偏移和磁场误差对CTFEL装置性能影响很大,通过前期设计和后期测量与优化将其限制在指标要求范围内。在前期设计中尽量避免引入全局性的系统误差：磁结构具有平面反对称结构,保证电子轨迹中心和波荡器磁轴重合;磁结构端部的特殊设计减弱了间隙对出口磁场二次积分的影响;机械系统的大梁和立柱具有良好的刚性,闭环控制系统保证了高的波荡器间隙控制精度,这些措施降低了间隙不一致引入的磁场误差。在后期测量与优化中削弱了磁场的残存全局系统误差和局部随机误差：利用磁场点测台测量了波荡器磁场的纵向和横向分布,通过调节标准单元组件位置对磁场进行了垫补和优化,优化后电子轨迹中心偏移、峰峰值误差、相位误差、好场区及其误差均满足指标要求。     

Design optimization of fiber optic probes for remote fluorescence spectroscopy

Fiber optic probes are designed, developed and fabricated in the laboratories for remote fluorescence spectroscopic studies in various fields such as investigation of tissues, environmental monitoring, and analysis of samples in hostile environment. Optimized probe design is very much important for efficient transport and collection of photons, which ultimately helps in quantifying resultant emission and understanding light-matter interaction. Instead of the conventional ray optics, Monte Carlo technique has been used to optimize the design of fiber optic probes, comprising only of flat tipped fibers with and without focusing lenses, for remote fluorescence measurement in three different types of target media having different optical properties. Typical probe geometry consists of one excitation fiber surrounded by a ring of collection fibers. The effects of fiber parameters like fiber diameter, numerical aperture, core-clad ratio, arrangement of collection fibers around the excitation fiber and dead space between them, and optical properties of the medium on the performance of probes have been analysed and compared with the results of previous observations, wherever the data are available. The results show a significant difference between the collected emission with and without consideration of dead space, which plays a very significant role in probe design and is dependent on the number of collection fibers in the geometry, relative dimension of collection and excitation fibers and separation between the two. Introduction of a convex lens in the probe increases the amount of fluorescence signal for a given probe arrangement.     

Application of experimental design for optimization of erbium determination by high-resolution continuum source electrothermal atomic absorption spectrometry using lanthanum as a chemical modifier

ABSTRACT

In this paper, lanthanum was used as a chemical modifier for the direct determination of erbium by high-resolution continuum source electrothermal atomic absorption spectrometry. A two-step experimental design was used for optimization, first a full factorial design was conducted for identification of significant factors, and then a central composite design was carried out for final optimization of the significant factors. The optimum parameters were obtained as follows: atomization temperature of 2500°C, pyrolysis temperature of 1600°C, and pyrolysis time of 10?s in the presence of lanthanum as a chemical modifier. Under optimum conditions, the characteristic mass, limit of detection, and limit of quantification were 29?pg, 0.71, and 2.4?µg?L^?1, respectively. The precision of the method, estimated as the relative standard deviation for 10 replicate measurements of 50?µg?L^?1 of erbium, was 1.8%. The optimized method was applied to determine erbium content in sediments and rock samples. The determined values of erbium in sediment certified reference materials were in satisfactory agreement with the certified values according to the t-test for a 95% confidence level.