| 毛细管气相色谱法分离分析苯酚和水杨醛 |
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| 引用本文： | 陈连文,刘敬兰.毛细管气相色谱法分离分析苯酚和水杨醛[J].化学分析计量,2003,12(6):41-42. |
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| 作者姓名： | 陈连文 刘敬兰 |
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| 作者单位： | 1. 河北经贸大学生物工程系,石家庄,050061
2. 河北师范大学实验中心,石家庄,050016 |
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| 摘 要： | 采用毛细管气相色谱法对由苯酚和甲醛为原料合成的水杨醛及反应物苯酚进行了分离分析。研究了水杨醛与苯酚分离的最佳条件，用正十四烷作内标物进行定量，水杨醛、苯酚在0．5～6．0g／L内有良好的线性，加标平均回收率分别为97、3％、99、0％，测定结果的相对标准偏差小于5％。
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| 关 键 词： | 毛细管气相色谱法 分离 化学分析 苯酚 水杨醛 |
| 修稿时间： | 2003年5月27日 |
SEPARATION AND ANALYSIS OF PHENOL AND SALICYLIC ALDEHYDE BY CAPILLARY GAS CHROMATOGRAPHY |
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| Chen Lianwen.SEPARATION AND ANALYSIS OF PHENOL AND SALICYLIC ALDEHYDE BY CAPILLARY GAS CHROMATOGRAPHY[J].Chemical Analysis And Meterage,2003,12(6):41-42. |
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| Authors: | Chen Lianwen |
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| Abstract: | A method for separation and analysis of salicylic aldehyde and phenol by capillary gas chromatography was developed. The optimum separation conditions of salicylic aldehyde and phenol were studied. The quantitative analysis was carried out with internal standard of tetradecance. A good linear relation was in the range of 0. 5 -6.0 g/L for them. The recovery was 97. 3% and 99. 0% respectively and the RSD of the determinated results was less than 5% . |
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| Keywords: | capillary gas chromatography phenol salicylic aldehyde separation analysis |
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