| 微波辐射下的1,4-二甲基咔唑-9-羧酸的快速合成 |
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| 引用本文： | 劳文剑,尤进茂,孙学军,孔祥鹤,欧庆瑜.微波辐射下的1,4-二甲基咔唑-9-羧酸的快速合成[J].合成化学,2000,8(1):6-8. |
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| 作者姓名： | 劳文剑 尤进茂 孙学军 孔祥鹤 欧庆瑜 |
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| 作者单位： | 1. 中国科学院兰州化学物理研究所,兰州,730000
2. 曲阜师范大学化学系,曲阜,273165 |
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| 摘 要： | 以ＤＭＦ为溶剂，在微波辐射下由１，４－二甲基咔唑和相应的溴酯快速合成了两种１，４－二甲基咔唑－９－羧酸化合物，在最佳反应条件下，产率分别为８５．２％和８３．１％。
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| 关 键 词： | 羧酸 微波辐射 1 4－二甲基咔唑 合成 |
Rapid Preparation of 1,4-Dimethyl-carbazole-9-carboxylic acid under Microwave Irradiation |
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| Abstract.Rapid Preparation of 1,4-Dimethyl-carbazole-9-carboxylic acid under Microwave Irradiation[J].Chinese Journal of Synthetic Chemistry,2000,8(1):6-8. |
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| Authors: | Abstract |
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| Abstract: | Two 1,4- dimethyl- carbazole- 9- carboxylic acid compounds were synthesizedrapidly from 1,4-dimethyl carbazole and corresponding bromo-esters under microwaveirradiation using DMF as a solvent. The optimum reaction yields were 85. 1% and 83. 1%respectively. |
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| Keywords: | 1 4-Dimethyl- carbazole- 9- carboxylic acid Microwave irradiation Bromo-ester 1 4-Dimethyl-carbazole |
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