| 氰基取代的含杂环烯酮缩胺的合成及其波谱和结构特性 |
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| 引用本文： | 王肖君,黄志镗.氰基取代的含杂环烯酮缩胺的合成及其波谱和结构特性[J].化学学报,1989,47(9):890-895. |
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| 作者姓名： | 王肖君 黄志镗 |
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| 作者单位： | 中国科学院化学研究所 |
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| 摘 要： | 由氰基乙酸酯或丙二腈先制得氰基取代的烯酮缩硫醇, 然后与二胺反应合成了氰基取代的含杂环烯酮缩胺, 测定了它们的UV、IR、^1H及^1^3C NMR等波谱, 并测定了其中两个化合物的晶体结构, 对所得的波谱和结构特性进行了讨论。
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| 关 键 词： | 紫外分光光度法 硫醇 红外分光光度法 晶体结构 质谱法 碳13核磁共振谱法 光谱分析 质子磁共振谱法 氰基 杂环化合物 |
Synthesis and spectral and structural characteristics of cyano substituted heterocyclic ketene aminals |
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| WANG XIAOJUN,HUANG ZHITANG.Synthesis and spectral and structural characteristics of cyano substituted heterocyclic ketene aminals[J].Acta Chimica Sinica,1989,47(9):890-895. |
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| Authors: | WANG XIAOJUN HUANG ZHITANG |
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| Abstract: | Cyano-substituted heterocyclic ketene aminals were synthesized by the reaction of cyano-substituted ketene mercaptals, which were prepared from cyano acetic esters or malononitrile with diamines. Their UV, IR, 1H and 13C NMR spectra were measured. The crystal structures of aminals I and II were determine |
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| Keywords: | ULTRAVIOLET SPECTROPHOTOMETRY MERCAPTAN INFRARED SPECTROPHOTOMETRY CRYSTAL STRUCTURE MASS SPECTROGRAPHY C13 NMR SPECTROMETRY SPECTROGRAPHIC ANALYSIS PROTON MAGNETIC RESONANCE SPECTROMETRY CYANO GROUP HETEROCYCLIC COMPOUNDS |
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