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水热法制备MoO3-GQDs的三甲胺气敏性能
引用本文:Ali Akhtar,戴芃,储向峰,梁士明,何利芳.水热法制备MoO3-GQDs的三甲胺气敏性能[J].无机化学学报,2021,37(2):351-360.
作者姓名:Ali Akhtar  戴芃  储向峰  梁士明  何利芳
作者单位:安徽工业大学化学与化工学院;临沂大学材料科学与工程学院
基金项目:国家自然科学基金(No.61671019,61971003)资助。
摘    要:采用水热法制备了一系列具有不同碳量子点(GQDs)含量的MoO3?GQDs纳米复合材料,利用X射线衍射、扫描电子显微镜、透射电子显微镜、FTIR等对MoO3?GQDs复合材料进行了表征,研究了其气敏性能。结果表明,复合材料中GQDs的含量对MoO3?GQDs复合材料的气敏响应和选择性有显著影响。MoO3?GQDs纳米复合材料(S?6,GQDs悬浮液的含量为6 mL)传感器在230℃时对三甲胺(TMA)表现出高的气敏响应和好的气敏选择性;该传感器对1000μL·L^-1 TMA的响应为74.08;对1000μL·L^-1 TMA的响应时间和恢复时间分别为73和34 s;S?6复合材料气敏传感器在230℃时可以检测到1μL·L^-1的TMA。

关 键 词:水热合成法  量子点  纳米结构  材料科学
收稿时间:2020/6/11 0:00:00
修稿时间:2020/12/13 0:00:00

Trimethylamine Vapour Sensing Properties of MoO3-GQDs Prepared by Hydrothermal Method
Ali Akhtar,DAI Peng,CHU Xiang-Feng,LIANG Shi-Ming,HE Li-Fang.Trimethylamine Vapour Sensing Properties of MoO3-GQDs Prepared by Hydrothermal Method[J].Chinese Journal of Inorganic Chemistry,2021,37(2):351-360.
Authors:Ali Akhtar  DAI Peng  CHU Xiang-Feng  LIANG Shi-Ming  HE Li-Fang
Institution:(School of Chemistry and Chemical Engineering,Anhui University of Technology,Maanshan,Anhui 243002,China;School of Materials Science and Engineering,Linyi University,Linyi,Shandong 276005,China)
Abstract:A series of MoO3?GQDs nano?composites with different amounts of graphene quantum dots(GQDs)were prepared by the hydrothermal method.The as?prepared samples were characterized by X?ray diffraction,Scanning electron microscope,Transmission electron microscope,FTIR and so on.The gas sensing properties of MoO3?GQDs were investigated.It was found that the amount of GQDs in the composites had a great influence on the gas response and gas sensing selectivity of the nano?composites.The sensor based on the MoO3?GQDs nano?composite(S?6,the amount of GQDs suspension was 6.0 mL)showed high response and good gas sensing selectivity to TMA at 230℃;the response of the sensor to 1000μL·L^-1 TMA was 74.08;the response time and recovery time to 1000μL·L^-1 TMA were 73 and 34 s,respectively;the sensor based on MoO3?GQDs(S?6)composite could detect 1μL·L^-1 TMA vapor at 230℃.
Keywords:hydrothermal synthesis  quantum dots  nanostructures  materials science
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