| 溶剂热合成法制备(Zn,Hg)S微晶和薄膜 |
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| 引用本文： | 李雪梅,杨延钊,孙思修,郭今心,钟红梅,李大枝.溶剂热合成法制备(Zn,Hg)S微晶和薄膜[J].无机化学学报,2002,18(9):961-964. |
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| 作者姓名： | 李雪梅 杨延钊 孙思修 郭今心 钟红梅 李大枝 |
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| 作者单位： | 山东大学化学与化工学院,济南,250100 |
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| 基金项目： | 国家自然科学基金资助项目(No.20171029)，山东省优秀中青年科学家科研奖励基金。 |
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| 摘 要： | 近年来，由于Ⅱ～Ⅵ族半导体纳米材料的特殊物理、化学性质及其在半导体、光学器件、激光二极管、IR探测器等方面的广泛应用，它们的制备和表征引起了人们越来越大的兴趣犤１～１１犦。现在（Zn，Hg）S微晶正被广泛而深入的研究和应用。例如：一种发蓝光的激光二极管已经设计成功，它包含一夹在两衬层间的活性层，无论是在衬层还是在活性层中都包含有（Zn，Hg）S犤５犦。Sugao也曾报道过一种以（Zn，Hg）S为基础的半导体激光器件犤６犦。Parkin曾用MCl２（M＝Zn，Cd，Hg）和Li２E（E＝O，S，Se，Te）混合热解法制备ME或MxM'yS…
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| 关 键 词： | 溶剂热合成 硫化物 微晶 薄膜 |
Preparation of (Zn,Hg)S Crystallite and Thin Film by Solvothermal Synthesis |
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| LI Xue-Mei,YANG Yan-Zhao,SUN Si-Xiu,GUO Jin-Xin,ZHONG Hong-Mei and LI Da-Zhi.Preparation of (Zn,Hg)S Crystallite and Thin Film by Solvothermal Synthesis[J].Chinese Journal of Inorganic Chemistry,2002,18(9):961-964. |
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| Authors: | LI Xue-Mei YANG Yan-Zhao SUN Si-Xiu GUO Jin-Xin ZHONG Hong-Mei and LI Da-Zhi |
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| Institution: | School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100,School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100,School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100,School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100,School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100 and School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100 |
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| Abstract: | The crystallite and thin film of (Zn,Hg)S at different solvents were prepared by thermolysis of thiocyanoto complexes. The samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The results of these studies show that the properties of solvents are im-portant in controlling the sizes and shapes of the final products. |
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| Keywords: | solvothermal synthesis sulfide crystallite thin film |
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