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纯钛与Ti6Al7Nb合金氮离子注入层在小牛血清溶液中的扭动微动磨损试验研究
引用本文:朱永奎,蔡振兵,张广安,彭金方,沈明学,沈火明,朱旻昊.纯钛与Ti6Al7Nb合金氮离子注入层在小牛血清溶液中的扭动微动磨损试验研究[J].摩擦学学报,2013,33(2):196-201.
作者姓名:朱永奎  蔡振兵  张广安  彭金方  沈明学  沈火明  朱旻昊
作者单位:1. 西南交通大学材料先进技术教育部重点实验室摩擦学研究所,四川成都,610031
2. 西南交通大学材料先进技术教育部重点实验室摩擦学研究所,四川成都610031;中国科学院兰州化学物理研究所固体润滑国家实验室,甘肃兰州730000
3. 中国科学院兰州化学物理研究所固体润滑国家实验室,甘肃兰州,730000
4. 西南交通大学力学与工程学院,四川成都,610031
基金项目:国家自然科学基金项目(51005192, 11172250),教育部博士点基金(20100184120002),固体润滑国家重点实验室2009年度开放基金(0903)资助.
摘    要:文中主要研究了纯钛、Ti6A17Nb基体以及经过氮离子注入后的改性层的扭动微动磨损行为.氮离子注入采用高能离子注入机及增强沉积系统,加速电压为50 kV,注入剂量分别为1×l017、5×1017和9×1017cm-2.采用球/平面接触模式,对纯钛和Ti6Al7Nb合金/(Zr2O球(直径为25.2 mm),接触副在小牛血清介质条件下进行了纯钛和Ti6Al7Nb合金及其改性层的了扭动微动磨损试验.借助X衍射仪(XRD)、拉曼光谱(Raman)、三维形貌仪(3D)和扫描电镜(SEM)分析了两种材料及其改性层的化学成分、微动磨损磨痕形貌和微观组织结构,探讨了纯钛和Ti6Al7Nb合金基材和改性层的扭动微动运行行为和损伤机制.研究结果表明:用氮离子注入方法处理钛及其合金,生成的氮化物层能够改善材料表面的综合性能,提高其扭动微动磨损的耐磨性.纯钛和Ti6Al7Nb基体的磨损现象为氧化和剥落,其离子注入层的磨损现象为犁沟.

关 键 词:离子注入  扭动微动  摩擦磨损
修稿时间:9/4/2012 12:00:00 AM

Comparison on the Torsional Fretting Wear of Nitrogen Ion Implanted Pure Titanium and Ti6Al7Nb Alloys in Bovine Serum
ZHU Yong-kui,CAI Zhen-bing,ZHANG Guang-an,PENG Jin-fang,SHEN Ming-xue,SHEN Huo-ming and ZHU Min-hao.Comparison on the Torsional Fretting Wear of Nitrogen Ion Implanted Pure Titanium and Ti6Al7Nb Alloys in Bovine Serum[J].Tribology,2013,33(2):196-201.
Authors:ZHU Yong-kui  CAI Zhen-bing  ZHANG Guang-an  PENG Jin-fang  SHEN Ming-xue  SHEN Huo-ming and ZHU Min-hao
Institution:Key Lab of Advanced Technologies of Materials (Ministry of Education), Tribology Research Institute, Southwest Jiaotong University, Chengdu Sichuan 610031, China;1. Key Lab of Advanced Technologies of Materials (Ministry of Education), Tribology Research Institute, Southwest Jiaotong University, Chengdu Sichuan 610031, China;2. State Key Laboratory of Solid Lubrication, LanZhou Institute of Chemical Physics, Chinese Academy of Sciences, LanZhou 730000, China;State Key Laboratory of Solid Lubrication, LanZhou Institute of Chemical Physics, Chinese Academy of Sciences, LanZhou 730000, China;Key Lab of Advanced Technologies of Materials (Ministry of Education), Tribology Research Institute, Southwest Jiaotong University, Chengdu Sichuan 610031, China;Key Lab of Advanced Technologies of Materials (Ministry of Education), Tribology Research Institute, Southwest Jiaotong University, Chengdu Sichuan 610031, China;School of Mechanics and Engineering, Southwest Jiaotong University, Chengdu 610031, China;Key Lab of Advanced Technologies of Materials (Ministry of Education), Tribology Research Institute, Southwest Jiaotong University, Chengdu Sichuan 610031, China
Abstract:Pure titanium and Ti6Al7Nb alloys alloys were implanted by 50 keV N+ ions with different implanting dosage in high energy ion implantation and enhanced deposition system. Torsional fretting wear of un-treated and plasma implantation nitride titanium alloys flats against ZrO2 ball (with a diameter of 25.2 mm) were carried out under a simulated physiological condition. With analyses of the frictional kinetics behaviors, the X-ray diffraction, Raman spectroscopy, 3-D profiler,SEM morphologies, the damage characteristics of the surface modification layer and its substrate were discussed in detail.The results show that the plasma implantation nitride can improve its surface properties and the resistance of torsional fretting wear can be improved obviously.The wear mechanism of the pure titanium and Ti6Al7Nb were oxidation wear and delaminlation, the ploughing of the modification layers.
Keywords:torsional fretting  fretting wear  ion implantation
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