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Titanium and aluminum nitride synthesis via layer by layer LA-CVD
Authors:I Shishkovsky  Yu Morozov
Institution:a Samara State Technical University, Molodogvardeiskaja st. 244, 443110 Samara, Russia
b Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences, Institutskaya str., 8, Chernogolovka, Moscow Region, 142432, Russia
c Ecole Nationale d’Ingénieurs de Saint-Étienne (ENISE), DIPI Laboratory, 58 rue Jean Parot, 42023 Saint Etienne, France
Abstract:The possibility of the layer-by-layer synthesis of 3D parts from nitrides of titanium or aluminum by selective laser sintering/melting is discussed. The relationship between laser processing parameters and structure and phase content of sintered/melted samples are studied by means of optical metallography, X-ray diffraction, scanning electron microscopy and energy dispersive X-ray analysis. Optimal parameters of SLM process for AlN and TiN synthesis are determined. Solid 3D parts containing a TiN phase are produced from Ti powder. Distortion of the crystalline lattice of AlN and TiN phases is observed with the laser energy input.
Keywords:42  62  &minus  b  64  70  dj  81  05  Rm  81  20  Ev
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