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分光光度法测定食盐中的碘
引用本文:杨兵,彭传友,夏兰.分光光度法测定食盐中的碘[J].光谱实验室,2011,28(4):1778-1781.
作者姓名:杨兵  彭传友  夏兰
作者单位:1. 重庆化工职业学院应用化学系 重庆市江北区嘉陵四村100号400020
2. 重庆市水产技术推广站 重庆市渝北区龙溪街道金龙路64号-3 400030
摘    要:采用分光光度法对食盐中碘含量进行定量分析.对反应条件进行试验及优化,得最佳测定条件为:测定波长565nm,0.5mol/L盐酸2.00mL、3%双氧水3.00mL、10g/L淀粉1.00mL,显色时间10min.在此条件下测得碘含量为29.32mg/kg,符合国家标准.本方法操作简便,可靠,重现性好,专属性强,具有广泛...

关 键 词:  分光光度法  食盐  双氧水

Determination of Iodine in Salt by Spectrophotometry
YANG Bing,PENG Chuan-You,XIA Lan.Determination of Iodine in Salt by Spectrophotometry[J].Chinese Journal of Spectroscopy Laboratory,2011,28(4):1778-1781.
Authors:YANG Bing  PENG Chuan-You  XIA Lan
Institution:a(Department of Applied Chemistry,Chongqing Chemical Industry Vocational College,Chongqing 400020,P.R.China)a(Aquaculture Technology Extension Station in Chongqing,Chongqing 400030,P.R.China)
Abstract:The content of iodine in salt was quantitatively analyzed by spectrophotometry.The reaction conditions were tested and optimized,and optimal reaction conditions were obtained as follows:detection wavelength of 565nm,0.5mol/L HCl dosage of 2.00mL,3% hydrogen peroxide dosage of 3.00mL,10g/L starch dosage of 1.00mL,coloration time of 10min and the iodine content of 29.32mg/kg under the conditions,that met national standard.The method is convenient,accurate,practicable,and has good reproducibility and good specificity,that has same advantages and practical significance.
Keywords:Iodine  Spectrophotometry  Salt  Hydrogen Peroxide
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