| HPLC测定蒙药沏其日甘-5中栀子苷的含量 |
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| 引用本文： | 席海山.HPLC测定蒙药沏其日甘-5中栀子苷的含量[J].光谱实验室,2009,26(3):711-713. |
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| 作者姓名： | 席海山 |
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| 作者单位： | 内蒙古民族大学分析测试中心,内蒙古通辽市科尔沁区西拉木伦大街996号,028043 |
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| 摘 要： | 建立了沏其日甘-5（化痰五味散）中栀子苷的含量测定方法。采用BDS（150×4.6mm,5μm）色谱柱,以乙腈-水（15∶85）为流动相,检测波长为238nm,流速为0.8mL/min。栀子苷在1.3—6.5μg范围内具有良好的线性关系,r=0.9998。
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| 关 键 词： | 沏其日甘-5 栀子苷 高效液相色谱法 |
Determination of Geniposide in Qiqirigan-5 by HPLC |
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| XI Hai-Shan.Determination of Geniposide in Qiqirigan-5 by HPLC[J].Chinese Journal of Spectroscopy Laboratory,2009,26(3):711-713. |
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| Authors: | XI Hai-Shan |
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| Institution: | Analytical and Testing Center of Innermongolia University for Nationalitie;Tongliao;Innermongoli 028043;P.R.China |
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| Abstract: | The content of geniposide in Mongolian medicine qiqirigan-5 was determined by HPLC on BDS（150 × 4. 6mm, 5μm） column and the mobile phase of a mixture of water and acetonitrile（85 ： 15） at a flow rate of 0.8mL/min at 30℃. The detecting wavelength was 238nm. The linear range of Geniposide was 1.3-6.5μg,r=0. 9998. The mean recovery was 101.09% （RSD= 1. 48%,n=5）. |
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| Keywords: | Qiqirigan-5 Geniposide HPLC |
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