| 具有潜在抗菌活性的环丙沙星衍生物的NMR谱研究 |
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| 引用本文： | 李英俊,刘素娜,靳焜,彭勤纪,孙淑琴,许永廷,王营.具有潜在抗菌活性的环丙沙星衍生物的NMR谱研究[J].波谱学杂志,2004,21(3):317-321. |
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| 作者姓名： | 李英俊 刘素娜 靳焜 彭勤纪 孙淑琴 许永廷 王营 |
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| 作者单位： | 辽宁师范大学,化学化工学院,辽宁,大连,116029;大连理工大学,精细化学化工重点实验室,辽宁,大连,116012 |
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| 摘 要： | 利用核磁共振谱，通过1H-1]H COSY, gHMBC and APT (Attached Proton Test)实验对所合成的新化合物1环丙基-6-氟-7-（4-苯乙酰氨基硫代甲酰基-1-哌嗪基）-1,4-二氢-4-氧代喹啉-3-羧酸的NMR谱进行了分析，并对其谱峰进行了详细归属.
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| 关 键 词： | NMR 归属 2D NMR 1-环丙基-6-氟-7-(4-苯乙酰氨基硫代甲酰基-1-哌嗪基)-1 4-二氢-4-氧代喹啉-3-羧酸 环丙沙星 |
| 收稿时间： | 2004-03-01 |
AN NMR STUDY OF A NOVEL CIPROFLOXACIN DERIVATIVE:A POTENTIAL ANTIBACTERIAL AGENT |
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| Abstract.AN NMR STUDY OF A NOVEL CIPROFLOXACIN DERIVATIVE:A POTENTIAL ANTIBACTERIAL AGENT[J].Chinese Journal of Magnetic Resonance,2004,21(3):317-321. |
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| Authors: | Abstract |
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| Institution: | 1.School of Chemical Engineering, Liaoning Normal University, Dalian 116029, China; ;
2.State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012, China |
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| Abstract: | NMR spectroscopy was used to study a potential antibacterial agent, 1-cyclopropyl-
6-fluoro-1, 4-dihydro-4-oxo-7- (4-phenylacetylamino-thiocarbamoyl-1-piperazinyl)-3-quinoline-
carboxylic acid. The ~1H and ~(13)C NMR chemical shifts of the compound were assigned using~1
H-~1 H COSY, gHMBC and attached proton test (APT) experiments. |
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| Keywords: | NMR 2D NMR NMR assignment 2D NMR 1-cyclopropyl-6-fluoro-7-(4-phenylacetylamino-thiocarbamoyl-1-piperazinyl)-1 4-dihydro-4-oxo-3-quinolinecarboxylic acid ciprofloxacin |
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