| 一种二苯并吖啶衍生物的NMR特征 |
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| 引用本文： | 蒋虹,王倩,李团结,冯友建,屠树江.一种二苯并吖啶衍生物的NMR特征[J].波谱学杂志,2007,24(2):217-222. |
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| 作者姓名： | 蒋虹 王倩 李团结 冯友建 屠树江 |
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| 作者单位： | 徐州师范大学 江苏省药用植物生物技术重点实验室，徐州 221116 |
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| 基金项目： | 国家自然科学基金，江苏省大型科学仪器共享服务平台理事会资助项目，徐州师范大学校科研和教改项目 |
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| 摘 要： | 二苯并吖啶衍生物可作为新型的微感涂料，并作为改进的受体广泛用于配位和超分子化学的研究中. 我们应用核磁共振技术（1H NMR, 13C NMR, DEPT, HSQC, HMBC）以及质谱(MS)确定了7-(4-甲氧基苯基)-5,6,8,9-四氢二苯并c,h] 吖啶的结构，准确归属了它的1H, 13C NMR信号，为其结构鉴定提供了重要依据.
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| 关 键 词： | 核磁共振 归属 二维核磁共振 二苯并吖啶 波谱分析 |
| 文章编号： | 1000-4556（2007）02-0217-06 |
| 收稿时间： | 2006-8-11 |
| 修稿时间： | 2006-08-112006-11-06 |
NMR Characterization of a Dibenzoacridine Derivative |
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| JIANG Hong,WANG Qian,LI Tuan-jie,FENG You-jian,TU Shu-jiang.NMR Characterization of a Dibenzoacridine Derivative[J].Chinese Journal of Magnetic Resonance,2007,24(2):217-222. |
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| Authors: | JIANG Hong WANG Qian LI Tuan-jie FENG You-jian TU Shu-jiang |
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| Institution: | Jiangsu Provincial Key Laboratory of Biotechnology on Medical Plant, Xuzhou Normal University, ;Xuzhou 221116, China |
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| Abstract: | Dibenzoacridine derivatives can be used as coating materials for microsensor. They have also been widely used as improved receptors in coordination and superamolecule chemistry. In this study, NMR techniques, including 1H NMR, 13C NMR, DEPT, HSQC, HMBC, and mass spectrometry (MS) were used in combination to elucidate the structure of a dibenzoacridine derivative 7-(4-methoxy-phenyl)-5,6,8,9-tetrahydro-dibenzo \acridine. The 1H and 13C chemical shifts of the compound were assigned. |
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| Keywords: | NMR assignment 2D NMR dibenzoacridine spectroscopic analysis |
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