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微波等离子体炬发射光谱法去溶系统性能的研究
引用本文:周建光,彭增辉,郇延富,于爱民,金钦汉,周翔,刘梅.微波等离子体炬发射光谱法去溶系统性能的研究[J].高等学校化学学报,2002,23(7):1273-1276.
作者姓名:周建光  彭增辉  郇延富  于爱民  金钦汉  周翔  刘梅
作者单位:1. 吉林大学化学学院分析科学研究所,长春,130023
2. 济源钢铁厂质管处,焦作,454650
基金项目:国家自然科学基金 (批准号 :2 973 5 160 ),国家“九五”科技攻关项目 (批准号 :96-A2 3 -0 2 -0 1),吉林省科技发展项目 (批 准号 :93 10 0 8)
摘    要:用微波等离子体矩(MPT)作激发光源,等离子体的工作气体为氩气,研究了气动雾化进样去溶系统的工作参数对分析性能的影响,探讨了水冷凝与浓硫酸吸收二者协同去溶的相关性,结果表明,OH (Q1带,带头谱线为308.520nm)的发射强度即可判别样品去溶效果。

关 键 词:性能  微波等离子体矩  原子发射光谱  去溶系统  气动雾化进样
文章编号:0251-0790(2002)07-1273-04

An Investigation on Effect of Desolvation System on Analytical Performance of MPT-AES
ZHOU Jian Guang,PENG Zeng Hui,HUAN Yan Fu,YU Ai Min,JIN Qin Han.An Investigation on Effect of Desolvation System on Analytical Performance of MPT-AES[J].Chemical Research In Chinese Universities,2002,23(7):1273-1276.
Authors:ZHOU Jian Guang  PENG Zeng Hui  HUAN Yan Fu  YU Ai Min  JIN Qin Han
Institution:ZHOU Jian Guang,PENG Zeng Hui,HUAN Yan Fu,YU Ai Min,JIN Qin Han *
Abstract:A pneumatic nebulizer(PN) was utilized as a sample introduction device for the microwave plasma torch atomic emission spectrometry(MPT AES) in an attempt to study the relationship between analytical performance and desolvation system. The desovation system consists of a condenser and a cell with concentrated H 2SO 4. Some parameters were studied and discussed in this work. The optimized conditions for the MPT AES were obtained.
Keywords:Microwave plasma torch  Atomic emission spectrometry  Desovation system
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