| 单萜/顺丁烯二酸酐加成物及其酯类衍生物的气相色谱法分析 |
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| 引用本文： | 常东亮,哈成勇.单萜/顺丁烯二酸酐加成物及其酯类衍生物的气相色谱法分析[J].色谱,1999,17(6):576-577. |
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| 作者姓名： | 常东亮 哈成勇 |
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| 作者单位： | 中国科学院广州化学研究所 |
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| 摘 要： | 摘要：研究了单萜/顺酐加成物及其酯化衍生物在OV-17和SE-30柱上的某些色谱性能和定量分析的线性相应关系。结果表明，这两种化合物在涂渍量为5％～10％的OV-17和SE-30柱上均能正常出峰；在峰形对称性和出峰时间上，OV-17柱具有优势。260℃以后，色谱峰面积与汽化温度无关。
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| 关 键 词： | TMA 松节油 增塑剂 萜烯 顺丁烯二酸酐 加成物 |
Analysis of terpene/maleic anhydride adduct and its derivatives by GC] |
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| D L Chang,C Y Ha.Analysis of terpene/maleic anhydride adduct and its derivatives by GC][J].Chinese Journal of Chromatography,1999,17(6):576-577. |
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| Authors: | D L Chang C Y Ha |
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| Institution: | Guangzhou Institute of Chemistry, Chinese Academy of Sciences, Guangzhou 510650, China. |
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| Abstract: | The retention behaviors of terpene/maleic anhydride adduct(TMA, 1) and its esterification derivatres(2) on OV-17 and SE-30 columns has been studied. The relationships between adjusted retention time and column temperature for the two compounds were linear. The shape of both peaks was more symmetrical on OV-17 column than on SE-30 column. It was found that the peak area was unaffected when the temperature of injector was higher than 260 degrees C. |
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