| 流动注射一超声雾化器一电感耦合等离子体-原子发射光谱(FI-UN-ICP-AES)同时测定头发中多种元素条件的优化 |
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| 引用本文： | 覃事栋,杨成隆,姚俊,张永康,杨芃原,王小如.流动注射一超声雾化器一电感耦合等离子体-原子发射光谱(FI-UN-ICP-AES)同时测定头发中多种元素条件的优化[J].光谱实验室,1997(6). |
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| 作者姓名： | 覃事栋 杨成隆 姚俊 张永康 杨芃原 王小如 |
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| 作者单位： | 吉首大学化学系!湖南省吉首市沙子坳，416000，厦门大学化学系!福建省厦门市，361005，吉首大学化学系!湖南省吉首市沙子坳，416000，吉首大学化学系!湖南省吉首市沙子坳，416000，厦门大学化学系!福建省厦门市，361005，厦门大学化学系!福建省厦门市，361005 |
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| 基金项目： | 国家自然科学基金!29235110-Ⅱ |
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| 摘 要： | 建立了FI－UN－ICP－AES联用技术，用所发展技术进行了头发中多种微量元素的同时测定，对载流流速、积分时间、进样体积等进行了优化。多次注射测定的再现性（RSD）在0.6％一5．0％范围内，标准加入回收率为90％一101％。
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| 关 键 词： | 人发 流动注射 超声雾化器 电感耦合等离子体原子发射光谱 |
The Optimization of Conditions for Simultaneous Determination of Multi-Element in Human Hair by FI-Ultrasonic Nebulization Coupled with ICP-AES |
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| QIN Shidong, YANG Chenglong, YAo Jun, ZHANG Yongkang, YANG Pengyuan, WANG Xiaoru.The Optimization of Conditions for Simultaneous Determination of Multi-Element in Human Hair by FI-Ultrasonic Nebulization Coupled with ICP-AES[J].Chinese Journal of Spectroscopy Laboratory,1997(6). |
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| Authors: | QIN Shidong YANG Chenglong YAo Jun ZHANG Yongkang YANG Pengyuan WANG Xiaoru |
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| Abstract: | The hyphenated technique of flow injection (FI)-ultrasonic nebulhation (UN ) and inductivelycoupled pthema atomic emission spectroscopy(ICP-AES) has been established in the present work,which was applied to the simultaneous determination of multi-element in human hair, The carrier flowrate, the integrate thoe and the sample injection volume were optimized. The repeatabilities of themulti injection(RSD) are in the range of 0. 6 % to 5%' The recoveries from the standard addition tothe sample ranged from 90% to 1Ol %. |
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| Keywords: | Human Hair Flow Injection Ultrasonic Nebulizer ICP-AES |
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